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    Process for testing catalysts using chromatography
    1.
    发明授权
    Process for testing catalysts using chromatography 有权
    使用色谱法测试催化剂的方法

    公开(公告)号：US06623967B1

    公开(公告)日：2003-09-23

    申请号：US09612853

    申请日：2000-07-10

    申请人： Richard C. Willson, III

    发明人： Richard C. Willson, III

    IPC分类号： G01N3110

    CPC分类号： G01N31/10 ,  B01J19/0046 ,  B01J2219/00286 ,  B01J2219/00315 ,  B01J2219/00364 ,  B01J2219/00527 ,  B01J2219/00585 ,  B01J2219/00596 ,  B01J2219/00659 ,  B01J2219/00691 ,  B01J2219/00704 ,  B01J2219/00745 ,  B01J2219/00747 ,  C40B30/08 ,  C40B40/18 ,  Y10T436/214 ,  Y10T436/24

    摘要： Methods for evaluating catalysts, in which a multicell holder, e.g., a honeycomb or plate, or a collection of individual support particles, is treated with solutions/suspensions of catalyst ingredients to produce cells, spots or pellets holding each of a variety of combinations of the ingredients, is dried, calcined or treated as necessary to stabilize the ingredients in the cells, spots or pellets, then is contacted with a potentially reactive feed stream or batch, e.g., biochemical, gas oil, hydrogen plus oxygen, propylene plus oxygen, CCl2F2 and hydrogen, etc. The reaction occurring in each cell can be measured, e.g., by infrared thermography, spectroscopic detection of products or residual reactants, or by sampling, e.g., multistreaming through low volume tubing, from the vicinity of each combination, followed by analysis, e.g., spectral analysis, chromatography, etc., or by observing temperature change in the vicinity of the catalyst, e.g., by thermographic techniques, to determine the relative efficacy of the catalysts in each combination. Robotic techniques can be employed in producing the cells, spots, pellets, etc.

    摘要翻译： 用于评价催化剂的方法，其中多单元保持器例如蜂窝或板或各个支撑颗粒的集合用催化剂成分的溶液/悬浮液处理以产生保持各种各样的组合的细胞，斑点或颗粒 根据需要将成分干燥，煅烧或处理以稳定细胞，斑点或丸粒中的成分，然后与潜在的反应性进料流或批次接触，例如生化，瓦斯油，氢加氧，丙烯加氧， CCl 2 F 2和氢等。可以测量每个电池中发生的反应，例如通过红外热成像，产物或残余反应物的光谱检测，或通过采样，例如通过低体积管道从每个组合的附近进行多流式化，随后 通过分析，例如光谱分析，色谱法等，或通过观察催化剂附近的温度变化，例如通过热成像技术测定 e催化剂在每种组合中的相对功效。 机器人技术可用于生产细胞，斑点，丸粒等。

    Combinatorial process for performing catalytic chemical reactions
    4.
    发明授权
    Combinatorial process for performing catalytic chemical reactions 有权
    进行催化化学反应的组合方法

    公开(公告)号：US06368865B1

    公开(公告)日：2002-04-09

    申请号：US09464306

    申请日：1999-12-15

    申请人： Ivar M. Dahl ,  Arne Karlsson ,  Duncan E. Akporiaye ,  Rune Wendelbo ,  Kurt M. Vanden Bussche ,  Gavin P. Towler

    发明人： Ivar M. Dahl ,  Arne Karlsson ,  Duncan E. Akporiaye ,  Rune Wendelbo ,  Kurt M. Vanden Bussche ,  Gavin P. Towler

    IPC分类号： G01N3110

    CPC分类号： G01N31/10 ,  B01J19/0046 ,  Y10T436/24

    摘要： A combinatorial process for simultaneously conducting multiple catalytic chemical reactions in parallel has been developed. At least one catalyst is contained in the reaction zones of a plurality of reactors, each reactor having a reactor insert placed within a sleeve and inserted into a well, the reaction zone of each reactor being formed between a fluid permeable structure attached to the sleeve and a fluid permeable end of the corresponding reactor insert. A fluid reactant is flowed through each reactor where it is contacted with the catalyst contained in the reaction zone to form an effluent. The effluents are removed from the effluent from the reactor and are analyzed.

    摘要翻译： 已经开发了同时进行多个催化化学反应并联的组合方法。 在多个反应器的反应区域中包含至少一种催化剂，每个反应器具有置于套管内的反应器插入件并插入到井中，每个反应器的反应区域形成在附接到套筒的流体可渗透结构和 相应的反应器插入物的流体可渗透的端部。 流体反应物流过每个反应器，在那里与包含在反应区中的催化剂接触以形成流出物。 将废水从反应器的流出物中除去并进行分析。

    Process for testing catalysts using mass spectroscopy
    8.
    发明授权
    Process for testing catalysts using mass spectroscopy 有权
    使用质谱法测试催化剂的方法

    公开(公告)号：US06623969B1

    公开(公告)日：2003-09-23

    申请号：US09613082

    申请日：2000-07-10

    申请人： Richard C. Willson, III

    发明人： Richard C. Willson, III

    IPC分类号： G01N3110

    CPC分类号： G01N31/10 ,  B01J19/0046 ,  B01J2219/00286 ,  B01J2219/00315 ,  B01J2219/00364 ,  B01J2219/00527 ,  B01J2219/00585 ,  B01J2219/00596 ,  B01J2219/00659 ,  B01J2219/00691 ,  B01J2219/00704 ,  B01J2219/00745 ,  B01J2219/00747 ,  C40B30/08 ,  C40B40/18 ,  Y10T436/214 ,  Y10T436/24

    摘要： Methods for evaluating catalysts, in which a multicell holder, e.g., a honeycomb or plate, or a collection of individual support particles, is treated with solutions/suspensions of catalyst ingredients to produce cells, spots or pellets holding each of a variety of combinations of the ingredients, is dried, calcined or treated as necessary to stabilize the ingredients in the cells, spots or pellets, then is contacted with a potentially reactive feed stream or batch, e.g., biochemical, gas oil, hydrogen plus oxygen, propylene plus oxygen, CCl2F2 and hydrogen, etc. The reaction occurring in each cell can be measured, e.g., by infrared thermography, spectroscopic detection of products or residual reactants, or by sampling, e.g., multistreaming through low volume tubing, from the vicinity of each combination, followed by analysis, e.g., spectral analysis, chromatography, etc., or by observing temperature change in the vicinity of the catalyst, e.g., by thermographic techniques, to determine the relative efficacy of the catalysts in each combination. Robotic techniques can be employed in producing the cells, spots, pellets, etc.

    摘要翻译： 用于评价催化剂的方法，其中多单元保持器例如蜂窝或板或各个支撑颗粒的集合用催化剂成分的溶液/悬浮液处理以产生保持各种各样的组合的细胞，斑点或颗粒 根据需要将成分干燥，煅烧或处理以稳定细胞，斑点或丸粒中的成分，然后与潜在的反应性进料流或批次接触，例如生化，瓦斯油，氢加氧，丙烯加氧， CCl 2 F 2和氢等。可以测量每个电池中发生的反应，例如通过红外热成像，产物或残余反应物的光谱检测，或通过采样，例如通过低体积管道从每个组合的附近进行多流式化，随后 通过分析，例如光谱分析，色谱法等，或通过观察催化剂附近的温度变化，例如通过热成像技术测定 e催化剂在每种组合中的相对功效。 机器人技术可用于生产细胞，斑点，丸粒等。