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    Process for manufacturing molecular sieve of MFS framework type and its use
    11.
    发明授权
    Process for manufacturing molecular sieve of MFS framework type and its use 有权
    制造MFS框架型分子筛的工艺及其应用

    公开(公告)号：US08187569B2

    公开(公告)日：2012-05-29

    申请号：US11699166

    申请日：2007-01-29

    申请人： Machteld M. Mertens ,  An Verberckmoes ,  Ivy D. Johnson

    发明人： Machteld M. Mertens ,  An Verberckmoes ,  Ivy D. Johnson

    IPC分类号： C01F7/00 ,  C01B33/36 ,  C01B39/00 ,  C01B39/02 ,  C01B39/04

    CPC分类号： B01J29/7026 ,  C01B39/48 ,  C07C2/12 ,  C10G49/08 ,  C10G2400/20 ,  C10G2400/22 ,  C07C11/02

    摘要： A method of making a crystalline molecular sieve of MFS framework type, said method comprising the steps of (a) adding at least one source of ions of tetravalent element (Y), at least one source of ions of trivalent element (X), at least one hydroxide source (OH−), at least one structure-directing-agent (R), at least one seed source (Seed), and water (H2O) to form a mixture having the following mole composition (expressed in term of oxide): YO2:(n)X2O3:(x)OH−:(y)R:(z)H2O+(m)Seed wherein the m is in the range of from about 10 wtppm to about 2 wt. % (based on total weight of the synthesis mixture), the n is in the range of from about 0.005 to 0.05, the x is in the range of from about 0.01 to about 0.3, the y is in the range of from about 0.03 to about 2; and the z is in the range of from about 3 to about 30; and (b) treating said mixture under crystallization conditions to form said crystalline molecular sieve substantially free of non-MFS material, wherein said crystallization conditions comprise a temperature in the range of from about 150° C. to about 250° C., and crystallization time less than 100 hr, the weight hourly throughput is at least 0.001 hr−1.

    摘要翻译： 一种制备MFS框架型结晶分子筛的方法，所述方法包括以下步骤：（a）将至少一种四价元素（Y）的离子的至少一种源，至少一种三价元素（X）的离子源加入 至少一种氢氧化物源（OH-），至少一种结构导向剂（R），至少一种种子源（Seed）和水（H 2 O），以形成具有以下摩尔组成的混合物 ）：YO 2：（n）X 2 O 3：（x）OH - :( y）R：（z）H 2 O +（m）其中m为约10重量ppm至约2重量％ ％（基于合成混合物的总重量），n在约0.005至0.05的范围内，x在约0.01至约0.3的范围内，y在约0.03至 约2; 并且z在约3至约30的范围内; 和（b）在结晶条件下处理所述混合物以形成基本上不含非MFS材料的所述结晶分子筛，其中所述结晶条件包括在约150℃至约250℃范围内的温度和结晶 时间小于100小时，重量小时产量至少为0.001小时-1。

    Method for preparing diarylalkanes
    19.
    发明授权
    Method for preparing diarylalkanes 失效
    二芳基烷烃的制备方法

    公开(公告)号：US5073655A

    公开(公告)日：1991-12-17

    申请号：US559242

    申请日：1990-07-27

    申请人： Philip J. Angevine ,  Ivy D. Johnson ,  David O. Marler ,  John P. McWilliams

    发明人： Philip J. Angevine ,  Ivy D. Johnson ,  David O. Marler ,  John P. McWilliams

    IPC分类号： B01J29/04 ,  C07C2/12

    CPC分类号： B01J29/04 ,  C07C2/12 ,  C07C2529/70

    摘要： Diarylalkanes are prepared by alkylating an aromatic hydrocarbon with an aromatic alkylation agent in the presence of a synthetic porous crystalline material catalyst composition. The aromatic hydrocarbon can be, for example, benzene, toluene, naphthalene, etc. The aromatic alkylating agent can be an aromatic compound with a hydroxy group, such as phenol, or benzyl alcohol, or an aromatic halide, aldehyde, ether, or an aromatic olefin such as styrene.

    摘要翻译： 二芳基烷烃通过在合成的多孔结晶材料催化剂组合物的存在下用芳族烷基化剂烷基化芳族烃来制备。 芳族烃可以是例如苯，甲苯，萘等。芳族烷基化剂可以是具有羟基的芳香族化合物，例如苯酚或苄醇，或芳族卤化物，醛，醚或 芳族烯烃如苯乙烯。