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11.发明授权
公开(公告)号：US5416190A
公开(公告)日：1995-05-16
申请号：US145923
申请日：1993-10-29
摘要： Disclosed is a highly reproducible method for the molecular weight fractionation of polyhydrogen silsesquioxane that gives a very storage-stable polyhydrogen silsesquioxane having a freely selectable molecular weight. The method involves dissolving polyhydrogen silsesquioxane in active-hydrogen-free nonpolar solvent; adding an active-hydrogen-free polar solvent to the resulting solution in order to precipitate polyhydrogen silsesquioxane; and collecting the desired molecular weight fraction of polyhydrogen silsesquioxane.
摘要翻译： 公开了一种高度可重复的聚氢倍半硅氧烷分子量分级方法，其提供了具有可自由选择的分子量的非常储存稳定的聚氢倍半硅氧烷。 该方法包括将聚氢倍半硅氧烷溶解在无活性氢的非极性溶剂中; 向所得溶液中加入无活性氢的极性溶剂，以沉淀聚氢倍半硅氧烷; 并收集所需的聚氢倍半硅氧烷的分子量分数。
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公开(公告)号：US5380555A
公开(公告)日：1995-01-10
申请号：US187239
申请日：1994-01-26
CPC分类号： C04B41/87 , C03C17/23 , C04B41/009 , C04B41/5035 , C23C18/1208 , C23C18/1212 , C23C18/1279 , H01L21/316 , C03C2217/213 , C03C2218/17 , C04B2111/00844
摘要： Disclosed is a method for the formation of ceramic silicon oxide films on substrate surfaces wherein said films are thick, free of cracks and pinholes, and insoluble in organic solvents. These films are formed by coating the surface of a substrate with a silicon resin having the general formula(HR.sub.2 SiO.sub.1/2).sub.X (SiO.sub.4/2).sub.1.0wherein R is selected from the set comprising the hydrogen atom, alkyl groups, and aryl groups, and 0.1.ltoreq.X.ltoreq.2.0, and then heating the coated substrate to convert the coating into a ceramic silicon oxide film.
摘要翻译： 公开了一种在衬底表面上形成陶瓷氧化硅膜的方法，其中所述膜是厚的，没有裂纹和针孔，并且不溶于有机溶剂。 这些膜通过用具有通式（HR2SiO1 / 2）X（SiO4 / 2）1.0的硅树脂涂覆基板的表面而形成，其中R选自包含氢原子，烷基和芳基的组， 和0.1≤X≤2.0，然后加热涂覆的基底以将涂层转变成陶瓷氧化硅膜。
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公开(公告)号：US20130338265A1
公开(公告)日：2013-12-19
申请号：US13997767
申请日：2011-12-27
IPC分类号： C08K5/5419
CPC分类号： C08K5/5419 , C08G59/621 , C08G77/14 , C08G77/80 , H01L23/296 , H01L2924/0002 , C08L63/00 , C08L83/06 , H01L2924/00
摘要： To provide a curable epoxy resin composition that exhibits excellent fluidity during molding without having adverse effects on the physical properties of the cured material. A curable epoxy resin composition, containing (I) a curable epoxy resin, and (II) an epoxy functional group- and aromatic hydrocarbon group-containing organopolysiloxane having an epoxy equivalent weight of 3,000 or lower, a content of aromatic hydrocarbon groups of 45 to 80% by weight (mass), and a glass transition point of less than 0° C.
摘要翻译： 提供在成型时表现出优异的流动性而对固化材料的物理性能没有不利影响的可固化环氧树脂组合物。 一种可固化环氧树脂组合物，其包含（I）可固化环氧树脂，和（II）环氧当量为3,000以下的环氧官能团和芳香族烃基的有机聚硅氧烷，芳香族烃基的含量为45〜 80重量％（质量），玻璃化转变点小于0℃
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公开(公告)号：US08609742B2
公开(公告)日：2013-12-17
申请号：US12281158
申请日：2007-02-28
申请人： Mari Wakita , Motoshi Sasaki , Peter Cheshire Hupfield , Yasuo Itami , Kaori Ozawa , Masahiko Maeda
发明人： Mari Wakita , Motoshi Sasaki , Peter Cheshire Hupfield , Yasuo Itami , Kaori Ozawa , Masahiko Maeda
CPC分类号： C08F290/06 , C08F283/12 , C08F290/061 , C08G18/2885 , C08G18/672 , C08G18/792 , C08G65/007 , C08G2650/48 , C08K3/36 , C08L27/12 , C08L33/08 , C08L75/16 , C08L83/04 , C09D4/00 , C09D5/00 , C09D5/024 , C09D7/61 , C09D133/08 , C09D171/02 , C09D175/16 , Y10T428/249921 , C08L2666/02 , C08L2666/20
摘要： Disclosed is a high energy ray-curable composition which is excellent in storage stability before curing and enables to form a cured coating film which is excellent in hardness, property of preventing adhesion of fats and oils, property of wiping off fats and oils, abrasion resistance, transparency, water repellency, adhesion, smoothness and uniformity. Specifically disclosed is a high energy ray-curable composition containing the following components (A)-(D). (A) 100 parts by weight of a polyfunctional acrylate (B) 1-30 parts by weight of an organoalkoxysilane having an aliphatic unsaturated bond (C) 1-100 parts by weight of colloidal silica (D) 0.2-20 parts by weight of a fluorine compound having an aliphatic unsaturated bond.
摘要翻译： 本发明公开了一种能够固化前的保存稳定性优异的高能射线固化性组合物，能够形成硬度优异，防止油脂粘附性，油脂擦拭性，耐磨损性的固化涂膜 ，透明性，防水性，粘合性，平滑性和均匀性。 具体公开了含有以下成分（A） - （D）的高能射线固化性组合物。 （A）100重量份多官能丙烯酸酯（B）1-30重量份具有脂族不饱和键的有机烷氧基硅烷（C）1-100重量份胶体二氧化硅（D）0.2-20重量份 具有脂肪族不饱和键的氟化合物。
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公开(公告)号：US20100304630A1
公开(公告)日：2010-12-02
申请号：US12675514
申请日：2008-09-01
申请人： Ikutaro Morikawa , Mari Wakita , Motoshi Sasaki
发明人： Ikutaro Morikawa , Mari Wakita , Motoshi Sasaki
CPC分类号： C08F2/48 , C08F220/14 , C08F230/08 , C08F290/067 , C08K3/36 , C08K5/005 , C08K5/5425 , C08L75/04 , C08L83/04 , C09D4/00 , C09D7/61 , C09D175/04 , Y10T428/249921 , Y10T428/31507 , Y10T428/31649 , Y10T428/31678 , Y10T428/31699 , Y10T428/31906 , Y10T428/31989 , Y10T428/31993 , Y10T442/20 , C08L83/00
摘要： A photocurable resin composition is provided that exhibits an excellent storage stability, that can be easily cured by ultraviolet radiation, and that cures to form a cured film that exhibits an excellent ultraviolet absorbing performance at around the 300 nm wavelength, an excellent physical strength, an excellent stain resistance, an excellent film uniformity, and an excellent adherence by the film. This photocurable resin composition comprises the following components (A) to (E): (A) 100 weight parts of a multifunctional acrylate or a multifunctional methacrylate, (B) 1 to 100 weight parts of an aliphatically unsaturated bond-containing organoalkoxysilane, (C) 1 to 300 weight parts colloidal silica, (D) 0.01 to 20 weight parts of an ultraviolet absorber that has an absorption wavelength at 220 to 400 nm, and (E) 0.01 to 30 weight parts of a photopolymerization initiator that has an absorption wavelength at 300 to 450 nm.
摘要翻译： 本发明提供一种光固化性树脂组合物，它具有优异的保存稳定性，可以容易地通过紫外线照射而固化，并且可以固化形成在300nm波长附近具有优异的紫外线吸收性能的固化膜，优异的物理强度， 优异的耐污性，优异的膜均匀性，以及优异的膜附着性。 该光固化性树脂组合物包含以下成分（A）〜（E）：（A）100重量份多官能丙烯酸酯或多官能甲基丙烯酸酯，（B）1〜100重量份含脂族不饱和键的有机烷氧基硅烷，（C ）1〜300重量份胶体二氧化硅，（D）0.01〜20重量份的吸收波长为220〜400nm的紫外线吸收剂，（E）0.01〜30重量份的光聚合引发剂，其吸收波长 在300〜450nm。
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公开(公告)号：US07368500B2
公开(公告)日：2008-05-06
申请号：US10484128
申请日：2002-07-26
申请人： Hideki Kobayashi , Motoshi Sasaki , Toru Masatomi
发明人： Hideki Kobayashi , Motoshi Sasaki , Toru Masatomi
IPC分类号： C08L83/06
CPC分类号： C09D183/10 , C08G77/44
摘要： A film-forming silicone resin composition, comprising a reaction product obtained by a method comprising the step of heating (A) an alkoxysilyl-functional organopolysiloxane obtained by running an equilibration reaction with components comprising (A1) a polydiorganosiloxane and (A2) an alkylpolysilicate in the presence of (A3) an equilibration polymerization catalyst; (B) colloidal silica, aluminum oxide, antimony oxide, titanium oxide, or zirconium oxide; and (C) water, and a curable film-forming silicone resin composition, comprising above film-forming silicone resin composition and (E) a condensation reaction catalyst.
摘要翻译： 一种成膜有机硅树脂组合物，其包含通过包括以下步骤的方法获得的反应产物：（A）通过与包含（A1）聚二有机硅氧烷和（A2）聚烷基硅酸盐的组分进行平衡反应获得的烷氧基甲硅烷基官能的有机聚硅氧烷 （A3）平衡聚合催化剂的存在; （B）胶体二氧化硅，氧化铝，氧化锑，氧化钛或氧化锆; 和（C）水，以及包含上述成膜硅树脂组合物和（E）缩合反应催化剂的可固化成膜硅树脂组合物。
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17.发明授权Liquid alkoxysilyl-functional silicone resins, method for their preparation, and curable silicone resin compositions 失效液体烷氧基甲硅烷基官能的有机硅树脂，其制备方法和可固化的有机硅树脂组合物公开(公告)号：US07074874B2
公开(公告)日：2006-07-11
申请号：US10481155
申请日：2002-06-27
申请人： Hideki Kobayashi , Motoshi Sasaki , Toru Masatomi
发明人： Hideki Kobayashi , Motoshi Sasaki , Toru Masatomi
IPC分类号： C08G77/06
摘要： Liquid alkoxysilyl-functional silicone resins having excellent storage stability and a method of preparing these liquid alkoxysilyl-functional silicone resins comprising running an equilibration polymerization reaction with components comprising (A) a polydiorganosiloxane and (B) an alkyl polysilicate in the presence of (C) an equilibration polymerization catalyst. Curable silicone resin compositions comprising the aforesaid liquid alkoxy-functional silicone resins which have excellent curability and when cured form a water-repellent coating on a variety of substrate surfaces.
摘要翻译： 包括具有优异的储存稳定性的液体烷氧基甲硅烷基官能的有机硅树脂和制备这些液体烷氧基甲硅烷基官能的有机硅树脂的方法，包括在（C）存在下，使（A）聚二有机硅氧烷和（B）聚硅酸烷基酯的组分进行平衡聚合反应， 平衡聚合催化剂。 可固化的有机硅树脂组合物包含上述具有优异固化性的液体烷氧基官能的有机硅树脂，并且当固化时形成各种基材表面上的拒水涂料。
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公开(公告)号：US06214748B1
公开(公告)日：2001-04-10
申请号：US09086031
申请日：1998-05-28
IPC分类号： H01L2131
CPC分类号： H01L21/02134 , H01L21/0212 , H01L21/02126 , H01L21/02203 , H01L21/02282 , H01L21/02337 , H01L21/02351 , H01L21/312 , H01L21/31695 , H01L21/76801 , H01L21/76825 , H01L21/76828 , H01L23/5329 , H01L23/53295 , H01L2924/0002 , H01L2924/3011 , H01L2924/00
摘要： This invention pertains to a method for forming thin films on substrates wherein the films are produced by applying a solution of an electrically insulating, heat-curing resin onto the substrate, evaporating the solvent and exposing the resin to high energy radiation to cure the resin. The resin solution contains a substance selected from solvents and gas generating additives that causes the dedensification of the film during the cure of the resin. This results in a film having a dielectric constant of below 2.7. This invention also pertains to a semiconductor device having an interconnect structure comprising at least one electrically conductive layer with an interposed insulating layer having a dielectric constant of less than 2.7 wherein the insulating layer is produced by the method of this invention.
摘要翻译： 本发明涉及在基板上形成薄膜的方法，其中通过将电绝缘的热固化树脂的溶液施加到基底上，蒸发溶剂并使树脂暴露于高能量辐射以固化树脂来制备薄膜。 树脂溶液含有选自溶剂和气体发生添加剂的物质，其在树脂固化期间引起薄膜的强化。 这导致介电常数低于2.7的膜。 本发明还涉及具有互连结构的半导体器件，该互连结构包括至少一个具有介电常数小于2.7的中间绝缘层的导电层，其中通过本发明的方法制造绝缘层。
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公开(公告)号：US5372842A
公开(公告)日：1994-12-13
申请号：US146358
申请日：1993-10-29
IPC分类号： H01L21/316 , C03C17/27 , C04B41/50 , C04B41/87 , C09D183/05 , C23C18/12 , H01L21/312 , B05D5/12
CPC分类号： C04B41/87 , C03C17/27 , C04B41/009 , C04B41/5035 , C23C18/1204 , C23C18/1212 , C23C18/122 , C23C18/1275 , C23C18/1279 , C03C2217/213 , C03C2218/322 , C04B2111/00844
摘要： Disclosed is a method for the formation of a thick silicon oxide film which is insoluble in organic solvents and free of cracks and pinholes on the surface of a substrate. The method comprises forming a hydrogen silsesquioxane resin film on the surface of a substrate, converting the hydrogen silsesquioxane resin into preceramic silicon oxide by heating in an inert gas atmosphere, and converting the preceramic silicon oxide into silicon oxide ceramic by heating in an atmosphere selected from the group consisting of oxygen and oxygen mixed with an inert gas.
摘要翻译： 公开了一种形成厚的氧化硅膜的方法，其不溶于有机溶剂，并且在基板的表面上没有裂纹和针孔。 该方法包括在基板的表面上形成氢倍半硅氧烷树脂膜，在惰性气体气氛中加热，将氢倍半硅氧烷树脂转化为陶瓷氧化硅，并将该陶瓷氧化硅转化为氧化硅陶瓷， 由氧和氧组成的组与惰性气体混合。
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公开(公告)号：US06706798B2
公开(公告)日：2004-03-16
申请号：US09997749
申请日：2001-11-29
申请人： Hideki Kobayashi , Motoshi Sasaki
发明人： Hideki Kobayashi , Motoshi Sasaki
IPC分类号： C08K336
CPC分类号： C09D183/04 , C08L83/00 , C08L2666/44 , C08L2666/54
摘要： A water repellent silicone coating agent composition comprising (A) a diorganopolysiloxane having a viscosity of 20 to 20,000 mPa·s at 25° C. in which the terminal ends of the molecular chain are blocked by silanol groups or silicon-bonded hydrolyzable groups, (B) a cross-linking agent represented by general formula RaSiX4-a, in which R is a monovalent hydrocarbon group comprising 1 to 10 carbon atoms, X is a hydrolyzable group, and subscript a is an integer of 0 to 2, (C) a condensation reaction catalyst, (D) a hydrophobic surface treated dry process silica having a carbon content of 3.7 to 5% by weight and a bulk density of 40 to 99 g/L, or a hydrophobic surface treated dry process silica having a carbon content of 2.7 to 5% by weight and a bulk density of 100 to 300 g/L, (E) an organic functional silane coupling agent-based adhesion-imparting agent, (F) an organic solvent, and optionally (G) a non-reactive silicone fluid.
摘要翻译： 一种防水硅氧烷涂层剂组合物，其包含（A）在25℃下粘度为20〜20,000mPa.s的二有机聚硅氧烷，其中分子链的末端被硅烷醇基或硅键合的可水解基团封闭（ B）由通式RaSiX4-a表示的交联剂，其中R是含有1至10个碳原子的一价烃基，X是可水解基团，下标a是0-2的整数，（C） 缩合反应催化剂，（D）碳含量为3.7〜5重量％，堆积密度为40〜99g / L的疏水性表面处理的干法二氧化硅，或具有碳含量的疏水性表面处理的干法二氧化硅 （E）为有机官能硅烷偶联剂的粘合赋予剂，（F）有机溶剂和任选的（G）非离子表面活性剂， 反应性硅液。
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