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    Alumina agglomerates, the preparation method thereof and use of same as an absorbent or catalyst carrier
    22.
    发明申请
    Alumina agglomerates, the preparation method thereof and use of same as an absorbent or catalyst carrier 有权
    氧化铝附聚物，其制备方法和作为吸收剂或催化剂载体的用途

    公开(公告)号：US20050079126A1

    公开(公告)日：2005-04-14

    申请号：US10473938

    申请日：2002-03-27

    Applicant: Jean-Luc Le Loarer ,  Christophe Nedez

    Inventor： Jean-Luc Le Loarer ,  Christophe Nedez

    IPC: B01J20/08 ,  B01J20/28 ,  B01J20/30 ,  B01J21/04 ,  B01J35/10 ,  C01F7/02 ,  C01F7/44

    CPC classification number: B01J20/28019 ,  B01J20/08 ,  B01J20/2803 ,  B01J20/28042 ,  B01J20/28069 ,  B01J21/04 ,  B01J35/10 ,  B01J35/1042 ,  B01J35/1061 ,  B01J35/1066 ,  B01J35/1085 ,  C01F7/02 ,  C01F7/448 ,  C01P2004/50 ,  C01P2004/61 ,  C01P2006/10 ,  C01P2006/12 ,  C01P2006/14

    Abstract: The invention relates to alumina agglomerates of the type obtained by dehydrating an aluminium oxyhydroxide or hydroxide, agglomerating the alumina thus obtained, hydrothermally treating the agglomerates and calcinating same. Said agglomerates are characterised in that: the V37 Å thereof is greater than or equal to 75 ml/100 g, preferably greater than or equal to 80 ml/100 g and, better still, greater than or equal to 85 ml/100 g; the V0.1 μm thereof is less than or equal to 31 ml/100 g; and the V0.2 μm thereof is less than or equal to 20 ml/100 g, preferably less than or equal to 15 ml/100 g and, better still, less than or equal to 10 ml/100 g. The invention also relates to a catalyst carrier, an intrinsic catalyst or an absorbent, in particular for use in the petroleum and petrochemical industry, comprising such alumina agglomerates. Moreover, the invention relates to methods for preparing said agglomerates.

    Abstract translation: 本发明涉及通过使羟基氧化铝或氢氧化钠脱水得到的类型的氧化铝附聚物，使由此获得的氧化铝凝聚，热固化处理附聚物并进行煅烧。 所述附聚物的特征在于：其V 37大于或等于75ml / 100g，优选大于或等于80ml / 100g，更优选大于或等于85ml / 100g; 其V0.1mum小于或等于31ml / 100g; 并且其V0.2μm小于或等于20ml / 100g，优选小于或等于15ml / 100g，更好的是小于或等于10ml / 100g。 本发明还涉及一种催化剂载体，本征催化剂或吸收剂，特别是用于石油和石化工业中，包括这种氧化铝附聚物。 此外，本发明涉及制备所述附聚物的方法。

    Porous 4 group metal oxide and method for preparation thereof
    23.
    发明申请
    Porous 4 group metal oxide and method for preparation thereof 有权
    多孔4族金属氧化物及其制备方法

    公开(公告)号：US20040238410A1

    公开(公告)日：2004-12-02

    申请号：US10484846

    申请日：2004-01-26

    Inventor： Shinichi Inoue ,  Akihiro Mutou ,  Tateo Ono ,  Toshiji Makabe ,  Toru Takatsuka ,  Hisashi Nomura

    IPC: C10G045/04 ,  C01G027/02

    CPC classification number: B01J21/063 ,  B01J21/06 ,  B01J21/066 ,  B01J23/28 ,  B01J23/85 ,  B01J23/88 ,  B01J23/882 ,  B01J23/883 ,  B01J23/888 ,  B01J27/188 ,  B01J35/10 ,  B01J35/1014 ,  B01J35/1019 ,  B01J35/1038 ,  B01J35/1042 ,  B01J35/1085 ,  B01J37/0009 ,  B01J37/036 ,  C01G23/04 ,  C01G23/0536 ,  C01G25/02 ,  C01P2002/72 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/17 ,  C01P2006/21 ,  C01P2006/82 ,  C10G45/08

    Abstract: This invention relates to a 4 group metal oxide and to a method for preparation thereof and the 4 group metal oxide prepared by adding a particle growth inhibiter to a hydrosol a hydrogel or a dried product of a hydrous 4 group metal oxide represented by MO(2-x)(OH)2x (wherein M denotes a 4 group metal and x is a number greater than 0.1 or x>0.1) followed by drying and calcining has a specific surface area of 80 m2/g or more, a pore volume of 0.2 ml/g or more and a pore sharpness degree of 50% or more and excellent heat stability and is useful for a catalyst or a catalyst carrier in which a catalyst metal is dispersed to a high degree. This invention further relates to a porous 4 group metal oxide and to a method for preparation thereof and the 4 group metal oxide prepared by application of a pH swing operation is characterized by a large specific surface area, excellent heat stability, high dispersion of a catalyst metal and a controlled and sharp pore distribution and is useful for a catalyst or a catalyst carrier of excellent reaction selectivity.

    Abstract translation: 本发明涉及一种4组金属氧化物及其制备方法以及通过向水溶胶中添加颗粒生长抑制剂而制备的4组金属氧化物，所述水凝胶或由MO（2）表示的含水4族金属氧化物的干燥产物 -x）（OH）2×（其中M表示4组金属，x是大于0.1或x> 0.1的数），然后干燥和煅烧的比表面积为80m 2 / g以上， 孔体积为0.2ml / g以上，细孔清晰度为50％以上，热稳定性优异，可用于高催化剂分散的催化剂或催化剂载体。 本发明还涉及一种多孔4族金属氧化物及其制备方法，通过应用pH挥发操作制备的4组金属氧化物的特征在于具有大比表面积，优异的热稳定性，催化剂的高分散性 金属和可控且尖锐的孔分布，并且可用于具有优异反应选择性的催化剂或催化剂载体。

    Catalyst support
    24.
    发明申请
    Catalyst support 审中-公开
    催化剂支持

    公开(公告)号：US20040152593A1

    公开(公告)日：2004-08-05

    申请号：US10400742

    申请日：2003-03-27

    Inventor： Willard A. Cutler ,  Tinghong Tao

    IPC: B01J023/02

    CPC classification number: B01J21/14 ,  B01J35/04 ,  B01J35/10 ,  B01J35/1076 ,  B01J35/1085 ,  F01N3/0814 ,  F01N3/206 ,  F01N3/2828 ,  F01N2330/06 ,  F01N2330/48 ,  F01N2610/02

    Abstract: A catalyst support for use in technologies (i.e., SCR and NOx adsorbers) which address the reduction of NOx from exhaust emissions of diesel and GDI engines. The catalyst support has a honeycomb body composed of a porous ceramic material, and a plurality of parallel cell channels traversing the body from a frontal inlet end to an outlet end thereof. The porous ceramic material is defined by a total porosity greater than 45 vol. %, and a network of interconnected pores with a narrow pore size distribution of pores having a median pore size greater than 5 micrometers but less than 20 micrometers. The catalyst support is capable of attaining higher catalyst loadings without a pressure drop penalty.

    Abstract translation: 用于技术（即SCR和NOx吸附器）的催化剂载体，其用于减少柴油和GDI发动机废气排放中的NOx。 催化剂载体具有由多孔陶瓷材料构成的蜂窝体和从正面入口端到其出口端的多个平行的细胞通道。 多孔陶瓷材料的总孔隙率大于45体积。 ％，以及具有中孔尺寸大于5微米但小于20微米的孔的狭窄孔径分布的互连孔的网络。 催化剂载体能够获得更高的催化剂负载而没有压降损失。

    Synthetic mesoporous material with radially assembled nanotubes
    25.
    发明申请
    Synthetic mesoporous material with radially assembled nanotubes 有权
    具有径向组装的纳米管的合成介孔材料

    公开(公告)号：US20040052714A1

    公开(公告)日：2004-03-18

    申请号：US10620770

    申请日：2003-07-17

    Applicant: Instituto Mexicano del Petroleo

    Inventor： Eduardo Terres Rojas ,  Jose Manuel Dominguez Esquivel

    IPC: C01B033/26 ,  C01B033/18

    CPC classification number: B82Y30/00 ,  B01J20/103 ,  B01J20/28019 ,  B01J20/28057 ,  B01J20/28083 ,  B01J21/08 ,  B01J29/0308 ,  B01J29/041 ,  B01J35/1023 ,  B01J35/1028 ,  B01J35/1042 ,  B01J35/1061 ,  B01J35/1085 ,  C01B37/005 ,  C01B37/02 ,  Y10S977/778

    Abstract: This invention relates to a new composition of high surface area materials suitable for adsorption of both organic and inorganic species and as a component of catalysts useful for the transformation of hydrocarbons into a variety of products. These materials are composed by mesoporous spherical particles that have large sorption capacity, as demonstrated by the uptake of nitrogen at 78 K having a diameter of 0.1 to 1.0 microns, a mean pore diameter of 2.0 nm to 4.0 nm, a surface area of 750 to 1050 m2/g and a mean pore volume of 0.75 to 1.0 ml/g. The typical inner structure is composed of nanotubes having diameters around 3.5 nm aligned along the radius of the spherical particles, with surface areas around 1,000 m2/g, depending on the surfactant (C16H33N(CH3)3 Br) to co-solvent (CnH2nnull1OH, where nnull2,3, or CH3COCH3) molar ratio. Elliptical particles are also obtained with cylindrical pores running along or across the major axis of the particles having very high surface areas of up to 1561 m2/g and a mean pore diameter of 2.0 to 4.0 nm. The walls of the nanotubes are pure silica or a composition of silica with M(III)Ox where M is a trivalent metal such as Al, Ga, or lanthanide.

    Abstract translation: 本发明涉及适于吸附有机和无机物质的高表面积材料的新组合物，以及用于将烃转化为多种产物的催化剂组分。 这些材料由具有大吸附能力的介孔球形颗粒组成，如通过在78K下吸收直径为0.1至1.0微米的氮气，平均孔径为2.0nm至4.0nm，表面积为750至 1050m 2 / g，平均孔体积为0.75〜1.0ml / g。 典型的内部结构由直径约3.5nm的纳米管组成，沿着球形颗粒的半径排列，其表面积约为1000m 2 / g，取决于表面活性剂（C16H33N（CH3）3 Br））与共溶剂 （C n H 2n + 1OH，其中n = 2,3或CH 3 COCH 3）摩尔比。 还可以获得椭圆形颗粒，其圆柱形孔沿着或横过具有高达1561m 2 / g的非常高的表面积的颗粒的长轴或者平均孔径为2.0至4.0nm。 纳米管的壁是纯二氧化硅或具有M（III）Ox的二氧化硅的组合物，其中M是三价金属如Al，Ga或镧系元素。

    Selective hydrogenation catalyst for pyrolysis gasoline
    26.
    发明申请
    Selective hydrogenation catalyst for pyrolysis gasoline 有权
    用于热解汽油的选择性氢化催化剂

    公开(公告)号：US20010056036A1

    公开(公告)日：2001-12-27

    申请号：US09767238

    申请日：2001-01-22

    Inventor： Li Siqin ,  Men Xiaotang ,  Gensheng Liu ,  Shunqin Liang ,  Xiaogong Zhang

    IPC: B01J023/58

    CPC classification number: C10G45/40 ,  B01J21/04 ,  B01J23/58 ,  B01J35/1014 ,  B01J35/1019 ,  B01J35/1042 ,  B01J35/1061 ,  B01J35/1085

    Abstract: The present invention is related to a selective hydrogenation catalyst for pyrolysis gasoline, wherein the catalyst mainly consists of a support of null, null mixed alumina covered by palladium as active component, promoter as co-active component and alkali metal and/or alkaline-earth metal. Said palladium is distributed like egg shell on the support surface. Said support has 0.5null0.9 ml/g of specific pore volume, wherein 40null200 null pores account for more than 85% of the total pore volume, preferably 100null200 null pore volume accounts for 65%null80% of the said total pore volume in catalyst support. The specific surface area is about 70null140 m2/g , and a crystal type in the alumina support is about 0.1null5% based on the weight percentage of null, null mixed alumina support, said catalyst contains promoter having selected from a group of the VIB or IB elements in the periodical table of elements. The ratio of promoter and palladium by weight is about 0.2null2:1. The alkali metal and/or alkaline-earth metal is added in amount of 0.05null2.0 wt %.

    Abstract translation: 本发明涉及用于热解汽油的选择性氢化催化剂，其中催化剂主要由作为活性组分的钯覆盖的δ，α混合氧化铝的载体，作为共活性组分的助催化剂和碱金属和/或碱土 金属。 所述钯在蛋壳上分布在支撑表面上。 所述载体具有0.5〜0.9ml / g的比孔体积，其中40〜200埃的孔占总孔体积的85％以上，优选孔径为100〜200埃，占总孔隙体积的65％〜80％ 催化剂载体中的孔体积。 比表面积为约70〜140m2 / g，氧化铝载体中的晶体类型以δ，α混合氧化铝载体的重量百分数为约0.1〜5％，所述催化剂含有选自以下组分的促进剂： 元素周期表中的VIB或IB元素。 助催化剂和钯的重量比约为0.2〜2：1。 碱金属和/或碱土金属的添加量为0.05〜2.0重量％。

    Shaped articles based on pyrogenically produced titanium dioxide, method of their production and their use
    29.
    发明授权
    Shaped articles based on pyrogenically produced titanium dioxide, method of their production and their use 失效
    基于热解产生的二氧化钛的成型制品，其生产方法及其用途

    公开(公告)号：US5231067A

    公开(公告)日：1993-07-27

    申请号：US773504

    申请日：1991-10-09

    Applicant: Klaus Deller ,  Bertrand Despeyroux ,  Helmfried Krause

    Inventor： Klaus Deller ,  Bertrand Despeyroux ,  Helmfried Krause

    IPC: B01J21/06 ,  B01J35/10 ,  B01J37/00 ,  C04B35/46 ,  C04B38/00

    CPC classification number: B01J21/063 ,  B01J35/023 ,  B01J35/1009 ,  B01J35/1038 ,  B01J35/1061 ,  B01J35/1085 ,  B01J37/0009 ,  C04B35/46 ,  C04B38/009 ,  Y10S502/509

    Abstract: Pressed parts based on pyrogenically produced titanium dioxide with the following physico-chemical characteristics:______________________________________ Outer diameter 0.8-15 mm BET surface according 99.5% TiO.sub.2 ______________________________________ They are produced by mixing pyrogenically produced titanium dioxide with urea, graphite and water, compacting the mixture, optionally drying the resulting mass at 80.degree. C. to 120.degree. C. comminuting, subsequently extruding or tabletting to produce pressed parts and tempering the pressed parts at a temperature of 710.degree. C. to 1000.degree. C. for a period of 0.5 to 6 hours.The pressed parts can be used as catalyst or catalytic carrier.

    Abstract translation: 基于热解产生的二氧化钛的压制零件，具有以下物理化学特性：-Out直径0.8-15mm -BET表面，根据<1-20m2 / g-至DIN 66131-孔体积0.01-0.29cm 3 / g - 孔 分布无孔<10nm - 至少90％的孔 - 在10-80nm的范围内 - 增强强度30-500N /压制部分-TiO 2相金红石100％ - 复合> 99.5％TiO 2 - 它们由 将热解产生的二氧化钛与尿素，石墨和水混合，将混合物压实，任选地将所得物质在80℃至120℃干燥，粉碎，随后挤出或压片以产生压制部件，并在 710℃至1000℃，时间为0.5至6小时。 压制零件可用作催化剂或催化载体。

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