METHOD FOR PRODUCING NICKEL POWDER
    446.
    发明申请
    METHOD FOR PRODUCING NICKEL POWDER 审中-公开
    生产镍粉的方法

    公开(公告)号:US20160368059A1

    公开(公告)日:2016-12-22

    申请号:US15117823

    申请日:2015-02-17

    Abstract: Provided is a method for producing fine nickel powder used as suitable seed crystals for producing nickel powder from a solution containing a nickel ammine sulfate complex. The method for producing nickel powder sequentially comprises: a mixing step of adding, to a solution containing a nickel ammine sulfate complex, an insoluble solid which is insoluble in the solution to form a mixed slurry; a reduction and precipitation step of charging a reaction vessel with the mixed slurry and then blowing hydrogen gas into the mixed slurry in the reaction vessel to reduce nickel complex ions contained in the mixed slurry to form nickel precipitate on a surface of the insoluble solid; and a separation step of separating the nickel precipitate on the surface of the insoluble solid from the surface of the insoluble solid to form nickel powder.

    Abstract translation: 本发明提供一种从含有硫酸镍络合物的溶液中制造用于生产镍粉的合适晶种的细镍粉的方法。 依次制备镍粉的方法包括:向含有硫酸镍络合物的溶液中加入不溶于该溶液以形成混合浆料的不溶性固体的混合步骤; 还原沉淀步骤,将反应容器装入混合浆料中,然后将氢气吹入反应容器中的混合浆液中以还原混合浆料中的镍络合物离子,以在不溶性固体的表面上形成镍沉淀物; 以及从不溶性固体的表面分离不溶性固体的表面上的镍沉淀物以形成镍粉末的分离步骤。

    METHOD FOR PREPARING ELEMENT DIFFUSION-TYPE COMPOSITE SUBSTRATE
    448.
    发明申请
    METHOD FOR PREPARING ELEMENT DIFFUSION-TYPE COMPOSITE SUBSTRATE 有权
    制备元素扩散型复合基板的方法

    公开(公告)号:US20160211437A1

    公开(公告)日:2016-07-21

    申请号:US14711541

    申请日:2015-05-13

    Abstract: A method for preparing element diffusion-type composite substrate and it belongs to the field of high-temperature coated superconducting substrate preparation. The rolled composite nickel-tungsten alloy substrate is heated and thermal insulated, meanwhile, both ends of the rolled substrate are electrified by low voltage and high current density pulse current. High-performance nickel-tungsten alloy composite substrate is obtained with the method in the present invention and sandwich-like composite substrate has low ferromagnetic performance and high strength by higher solution diffusing from inner layer to outer layer, which does not affect the formation of sharp cubic texture on the surface of substrate. On the one hand, electric pulse technology accelerate the interdiffusion effect of inter-layer elements, on the other hand, it promotes the recrystallization nucleation and reduces the recrystallization annealing temperature of the substrate, thus energy saving effect is achieved and the negative effects of annealing thermal erosion grooves among crystal boundary to subsequent coating are effectively reduced. Alloyed composite substrate prepared in this invention has the characteristics of high cubic texture content, low magnetic performance, high strength, and can be applied to large-scale industrial production.

    Abstract translation: 一种制备元素扩散型复合衬底的方法,属于高温涂层超导衬底制备领域。 轧制复合镍 - 钨合金基板被加热绝热,同时轧制基板的两端通过低电压和高电流密度脉冲电流通电。 通过本发明的方法获得高性能的镍 - 钨合金复合衬底,并且夹层复合衬底通过从内层向外层扩散的较高溶液具有低铁磁性能和高强度,其不影响尖锐的形成 在基体表面的立方结构。 一方面,电脉冲技术加速了层间元素的相互扩散效应,另一方面促进了再结晶成核,降低了基板的再结晶退火温度,达到节能效果,退火的负面效果 结晶边界到后续涂层的热蚀槽有效减少。 本发明制备的合金复合基材具有立方体结构含量高,磁性能好,强度高的特点,可应用于大规模工业化生产。

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