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    High shear hydrogenation of wax and oil mixtures
    43.
    发明授权
    High shear hydrogenation of wax and oil mixtures 有权
    蜡和油混合物的高剪切加氢

    公开(公告)号：US08491777B2

    公开(公告)日：2013-07-23

    申请号：US12692092

    申请日：2010-01-22

    Applicant: Abbas Hassan ,  Gregory G. Borsinger ,  Rayford G. Anthony ,  Aziz Hassan

    Inventor： Abbas Hassan ,  Gregory G. Borsinger ,  Rayford G. Anthony ,  Aziz Hassan

    IPC: C11C5/00

    CPC classification number: B01J10/007 ,  A23D9/00 ,  B01F7/00766 ,  B01F13/1013 ,  B01F13/1016 ,  B01J8/02 ,  B01J19/0066 ,  B01J19/18 ,  B01J19/1806 ,  C09D191/06 ,  C09J191/06 ,  C11C3/12 ,  C11C5/00 ,  C11C5/008

    Abstract: Embodiments disclosed herein describe a system for producing enhanced wax alternatives. The system comprises a reactor with at least one inlet and one outlet and at least one high shear mixing device with at least one inlet and one outlet. The at least one outlet of said high shear mixing device is in fluid communication with at least one inlet of said reactor. The high shear mixing device may comprise counter rotating rotors. The high shear mixing device may also comprise at least one catalytic surface. Embodiments disclosed herein also describe a method of producing enhanced wax alternatives. The method comprises (1) providing petroleum wax and base oil; (2) mixing said petroleum wax and base oil with a hydrogen-containing gas in a high shear device to form a feedstock; and (3) hydrogenating said feedstock for a time sufficient to produce enhanced hydrogenated products.

    Abstract translation: 本文公开的实施方案描述了用于生产增强蜡替代物的系统。 该系统包括具有至少一个入口和一个出口的反应器和至少一个具有至少一个入口和一个出口的高剪切混合装置。 所述高剪切混合装置的至少一个出口与所述反应器的至少一个入口流体连通。 高剪切混合装置可以包括反向旋转的转子。 高剪切混合装置还可以包括至少一个催化表面。 本文公开的实施方案还描述了生产增强的蜡替代物的方法。 该方法包括（1）提供石油蜡和基础油; （2）在高剪切装置中将所述石油蜡和基础油与含氢气体混合以形成原料; 和（3）将所述原料氢化足以产生增强的氢化产物的时间。

    Spray Process for Selective Oxidation
    46.
    发明申请
    Spray Process for Selective Oxidation 有权
    选择氧化喷涂工艺

    公开(公告)号：US20120022287A1

    公开(公告)日：2012-01-26

    申请号：US13258159

    申请日：2010-03-23

    Applicant: Bala Subramaniam ,  Daryle H. Busch ,  Fenghul Niu

    Inventor： Bala Subramaniam ,  Daryle H. Busch ,  Fenghul Niu

    IPC: C07C51/265

    CPC classification number: C07C51/255 ,  B01J4/002 ,  B01J10/007 ,  B01J2219/00006 ,  B01J2219/00063 ,  B01J2219/00065 ,  B01J2219/00162 ,  C07C51/265 ,  C07C63/00

    Abstract: Oxidation process can include: introducing small droplets of liquid reaction mixture having oxidizable reactant, catalyst, and solvent into a reaction zone containing oxygen and diluent gas; and oxidizing the reactant with the oxygen at a suitable reaction temperature and a suitable reaction pressure to produce an oxidized product. The liquid reaction mixture can have an aromatic feedstock having an oxidizable substituent as the oxidizable reactant. The oxidized product can include an aromatic compound having at least one carboxylic acid. For example, the aromatic feedstock can include a benzene ring having at least one oxidizable alkyl substituent, furan hetero-ring having at least one oxidizable alkyl substituent, a naphthalene poly-ring having at least one oxidizable alkyl substituent, derivatives thereof, and mixtures thereof.

    Abstract translation: 氧化过程可以包括：将具有可氧化反应物，催化剂和溶剂的小液滴的液体反应混合物引入含有氧气和稀释气体的反应区; 并在合适的反应温度和合适的反应压力下用氧氧化反应物以产生氧化产物。 液体反应混合物可具有具有可氧化取代基的芳族原料作为可氧化反应物。 氧化产物可以包括具有至少一个羧酸的芳族化合物。 例如，芳族原料可以包括具有至少一个可氧化烷基取代基的苯环，具有至少一个可氧化烷基取代基的呋喃异环，具有至少一个可氧化烷基取代基的萘多环，其衍生物及其混合物 。

    Method of and apparatus for synthesizing highly oriented, aligned carbon nanotubes from an organic liquid
    48.
    发明申请
    Method of and apparatus for synthesizing highly oriented, aligned carbon nanotubes from an organic liquid 有权
    从有机液体合成高定向取向碳纳米管的方法和装置

    公开(公告)号：US20100124526A1

    公开(公告)日：2010-05-20

    申请号：US12385184

    申请日：2009-04-01

    Applicant: Toshihiro Ando ,  Mika Gamo ,  Yafei Zhang

    Inventor： Toshihiro Ando ,  Mika Gamo ,  Yafei Zhang

    IPC: D01F9/12 ,  B01J19/08 ,  C01B31/36

    CPC classification number: B82Y30/00 ,  B01J10/007 ,  B01J2219/00094 ,  B01J2219/0013 ,  B01J2219/00263 ,  B01J2219/0884 ,  B01J2219/0894 ,  B82Y40/00 ,  C01B32/162 ,  C01B32/166 ,  C01B2202/08 ,  Y10S977/844

    Abstract: A method capable of synthesizing carbon nanotubes at low cost and large quantities, an apparatus usable for carrying out the method, and carbon nanotubes densely aligned on and firmly bonded to a Si substrate over, and oriented perpendicular to, an entire surface thereof are provided. Highly oriented, aligned carbon nanotubes are synthesized from an organic liquid by forming a substrate with a buildup thereon of a thin film or fine insular particles composed of at least one metallic element; exposing the substrate (3) having the buildup to a hydrogen plasma; and heating the substrate (3) exposed to the hydrogen plasma in the organic liquid (10) to a predetermined temperature. The synthesis apparatus comprises: a liquid chamber or tank (1) for an organic liquid; a water cooling means (2) for cooling the liquid tank (1) from its outside; a substrate holder (5) for holding a substrate (3), the holder having electrodes (4) for passing an electric current through the substrate (3); a condensing means (7) comprising water cooling tubes (6) for cooling and condensing vapor made from the organic liquid by its vaporization to return it to the liquid for return into the liquid tank (1); a valve (8) through which N2 gas is introduced; and a lid (9) that carries the substrate holder (5), the condensing means (7) and the valve (8). The organic liquid (10) is thus tightly sealed in the liquid tank (1) by the lid (9). This synthesis apparatus allows carbon nanotubes to be synthesized in large quantities, at low cost and in safety. Highly coaxially and densely oriented, aligned carbon nanotubes can be synthesized in the form of a bundle thereof, which when used in a variety of products brings about various excellent effects including extremely high usability.

    Abstract translation: 提供了能够以低成本和大量合成碳纳米管的方法，可用于实施该方法的装置，以及紧密地对准并牢固地结合到Si衬底并且垂直于其整个表面的碳纳米管。 通过在其上积聚由至少一种金属元素构成的薄膜或细小岛状颗粒的基板，由有机液体合成高取向的排列碳纳米管; 将具有积聚的衬底（3）暴露于氢等离子体; 以及将暴露于有机液体（10）中的氢等离子体的衬底（3）加热至预定温度。 合成装置包括：用于有机液体的液体室或罐（1）; 用于从其外部冷却液体罐（1）的水冷装置（2）; 用于保持基板（3）的基板保持器（5），所述保持器具有用于使电流通过所述基板（3）的电极（4）; 冷凝装置（7），包括水冷却管（6），用于通过其蒸发冷却和冷凝由有机液体制成的蒸汽，以将其返回到液体以返回到液体箱（1）中; 引入N 2气体的阀（8）; 以及承载基板保持件（5），冷凝装置（7）和阀（8）的盖（9）。 有机液体（10）因此通过盖（9）紧密地密封在液体罐（1）中。 该合成装置允许以低成本和安全性大量合成碳纳米管。 高度同轴且致密定向的碳纳米管可以以其束的形式合成，当用于各种产品时，可以产生包括极高的可用性的各种优异的效果。

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