Method of preparing cadmium sulfide nanocrystals emitting light at multiple wavelengths, and cadmium sulfide nanocrystals prepared by the method
    4.
    发明申请
    Method of preparing cadmium sulfide nanocrystals emitting light at multiple wavelengths, and cadmium sulfide nanocrystals prepared by the method 有权
    制备发射多波长光的硫化镉纳米晶体的方法和通过该方法制备的硫化镉纳米晶体

    公开(公告)号:US20060062720A1

    公开(公告)日:2006-03-23

    申请号:US11002490

    申请日:2004-12-03

    IPC分类号: C01G11/02

    摘要: A method for preparing cadmium sulfide nanocrystals emitting light at multiple wavelengths. The method comprises the steps of (a) mixing a cadmium precursor and a dispersant in a solvent that weakly coordinates to the cadmium precursor, and heating the mixture to obtain a cadmium precursor solution, (b) dissolving a sulfur precursor in a solvent that weakly coordinates to the sulfur precursor to obtain a sulfur precursor solution, and (c) feeding the sulfur precursor solution to the heated cadmium precursor solution maintained at a high temperature to prepare cadmium sulfide crystals, and growing the cadmium sulfide crystals. Further, cadmium sulfide nanocrystals prepared by the method. The cadmium sulfide nanocrystals have uniform size and shape and can emit light close to white light simultaneously at different wavelengths upon excitation. Due to these characteristics, the cadmium sulfide nanocrystals can be applied to white light-emitting diode devices.

    摘要翻译: 一种制备发射多波长光的硫化镉纳米晶体的方法。 该方法包括以下步骤:(a)将镉前体与分散剂混合在与镉前体轻配位的溶剂中,加热混合物得到镉前体溶液,(b)将硫前体溶于弱溶剂中 与硫前体配位以获得硫前体溶液,和(c)将硫前体溶液供给到保持在高温下的加热镉前体溶液以制备硫化镉晶体,并生长硫化镉晶体。 此外,通过该方法制备的硫化镉纳米晶体。 硫化镉纳米晶体具有均匀的尺寸和形状,并且可以在激发时以不同的波长同时发射接近白光的光。 由于这些特性,硫化镉纳米晶体可以应用于白色发光二极管器件。

    Method for manufacturing metal sulfide nanocrystals using thiol compound as sulfur precursor
    7.
    发明申请
    Method for manufacturing metal sulfide nanocrystals using thiol compound as sulfur precursor 有权
    使用硫醇化合物作为硫前体制备金属硫化物纳米晶体的方法

    公开(公告)号:US20060039850A1

    公开(公告)日:2006-02-23

    申请号:US10967238

    申请日:2004-10-19

    IPC分类号: C01B17/20

    摘要: Disclosed herein is a method for manufacturing metal sulfide nanocrystals using a thiol compound as a sulfur precursor. The method comprises reacting the thiol compound and a metal precursor in a solvent to grow metal sulfide crystals to the nanometer-scale level. Further disclosed is a method for manufacturing metal sulfide nanocrystals with a core-shell structure by reacting a metal precursor and a thiol compound in a solvent to grow a metal sulfide layer on the surface of a core. The metal sulfide nanocrystals prepared by these methods can have a uniform particle size at the nanometer-scale level, selective and desired crystal structures, and various shapes.

    摘要翻译: 本文公开了使用硫醇化合物作为硫前体制备金属硫化物纳米晶体的方法。 该方法包括使硫醇化合物和金属前体在溶剂中反应以将金属硫化物晶体生长至纳米级。 进一步公开的是通过使金属前体和硫醇化合物在溶剂中反应以在芯的表面上生长金属硫化物层来制造具有核 - 壳结构的金属硫化物纳米晶体的方法。 通过这些方法制备的金属硫化物纳米晶体可以在纳米级具有均匀的粒度,选择性和期望的晶体结构以及各种形状。