公开(公告)号：US09656865B2

公开(公告)日：2017-05-23

申请号：US12296051

申请日：2007-04-05

申请人： Thomas Ellsworth McWhorter ,  Aaron Rosenblatt ,  Madhu Anand ,  John Peter Hobbs

发明人： Thomas Ellsworth McWhorter ,  Aaron Rosenblatt ,  Madhu Anand ,  John Peter Hobbs

IPC分类号： A61L2/20 ,  C01B11/02 ,  A61L2/22

CPC分类号： C01B11/022 ,  A61L2/20 ,  A61L2/22

摘要： New methods are disclosed for decontaminating surfaces and enclosures that avoid problems such as salt deposits, corrosion and condensation that accompany the use of known methods. The methods involve the use of chlorine dioxide solutions prepared by passing dilute chlorine gas over solid granular sodium chlorite to produce chlorine dioxide gas which is then collected to form a solution with very low levels of impurities. The chlorine dioxide gas can be introduced into an enclosure and used to disinfect a portion of the contents of the enclosure.

公开(公告)号：US09045340B2

公开(公告)日：2015-06-02

申请号：US13365902

申请日：2012-02-03

申请人： Thomas Ellsworth McWhorter ,  Peter Kazlas ,  Madhu Anand ,  John Peter Hobbs ,  Aaron A. Rosenblatt ,  Robert H. Shay ,  Barzin Keramati

发明人： Thomas Ellsworth McWhorter ,  Peter Kazlas ,  Madhu Anand ,  John Peter Hobbs ,  Aaron A. Rosenblatt ,  Robert H. Shay ,  Barzin Keramati

IPC分类号： A61L2/18 ,  C01B11/02

CPC分类号： C01B11/024 ,  A01N59/00 ,  A61K33/00 ,  B65B63/00 ,  C01B11/022 ,  C01B11/028 ,  Y10T428/13 ,  Y10T428/131 ,  Y10T428/1334 ,  Y10T428/1352

摘要： The present invention is for extremely pure solutions of chlorine dioxide, methods for making such solutions and to compositions and methods for storing, shipping and using such solutions. Generally, the chlorine dioxide solutions of the invention are aqueous solutions containing about 2500 ppm or less of total impurities. The chlorine dioxide solution can be prepare by passing dilute highly pure chlorine gas through a bed of substantially solid sodium chlorite and contacting the resulting chlorine dioxide gas with a liquid.

公开(公告)号：US07955588B2

公开(公告)日：2011-06-07

申请号：US12783663

申请日：2010-05-20

申请人： Madhu Anand ,  Brian C. Dunn ,  Glenn W. Dodwell

发明人： Madhu Anand ,  Brian C. Dunn ,  Glenn W. Dodwell

IPC分类号： B01J27/04 ,  B01J27/047 ,  B01J27/051 ,  B01J37/20 ,  C07C9/04

CPC分类号： C01G39/06 ,  B01J27/04 ,  B01J27/047 ,  B01J27/051 ,  B01J37/031 ,  C01G31/00 ,  C01G41/00

摘要： Methods and apparatus relate to catalysts and preparation of the catalysts, which are defined by sulfides of a transition metal, such as one of molybdenum, tungsten, and vanadium. Precursors for the catalysts include a metal ion source compound, such as molybdenum trioxide, and a sulfide ion source compound, such as thioacetamide. Once the precursors are dissolved if solid and combined in a mixture, homogenous precipitation from the mixture forms the catalysts. Exemplary uses of the catalysts include packing for a methanation reactor that converts carbon monoxide and hydrogen into methane.

摘要翻译： 方法和装置涉及催化剂和制备催化剂，其由过渡金属的硫化物如钼，钨和钒中的一种所定义。 催化剂的前体包括金属离子源化合物，例如三氧化钼，以及硫化物离子源化合物，例如硫代乙酰胺。 一旦前体溶解如果固体并在混合物中组合，则从混合物中均匀沉淀形成催化剂。 催化剂的示例性用途包括将一氧化碳和氢气转化为甲烷的甲烷化反应器的填料。

公开(公告)号：US20070243716A1

公开(公告)日：2007-10-18

申请号：US11237601

申请日：2005-09-27

申请人： Christopher Roberts ,  Marshall McLeod ,  Madhu Anand

发明人： Christopher Roberts ,  Marshall McLeod ,  Madhu Anand

IPC分类号： H01L21/31

CPC分类号： C30B7/00 ,  B05D1/18 ,  B05D2401/32 ,  B05D2401/90 ,  B82Y30/00 ,  C30B7/005 ,  C30B29/605 ,  Y10S977/70 ,  Y10S977/773

摘要： A method for size selection of nanostructures comprising utilizing a gas-expanded liquids (GEL) and controlled pressure to precipitate desired size populations of nanostructures, e.g., monodisperse. The GEL can comprise CO2 antisolvent and an organic solvent. The method can be carried out in an apparatus comprising a first open vessel configured to allow movement of a liquid/particle solution to specific desired locations within the vessel, a second pressure vessel, a location controller for controlling location of the particles and solution within the first vessel, a inlet for addition of antisolvent to the first vessel, and a device for measuring the amount of antisolvent added. Also disclosed is a method for forming nanoparticle thin films comprising utilizing a GEL containing a substrate, pressurizing the solution to precipitate and deposit nanoparticles onto the substrate, removing the solvent thereby leaving a thin nanoparticle film, removing the solvent and antisolvent, and drying the film.

摘要翻译： 纳米结构尺寸选择的方法包括利用气体膨胀液体（GEL）和受控压力来沉淀所需尺寸的纳米结构体，例如单分散。 GEL可以包含CO 2反溶剂和有机溶剂。 该方法可以在包括构造成允许液体/颗粒溶液移动到容器内的特定所需位置的第一开放容器的设备中进行，第二压力容器，位置控制器，用于控制颗粒和溶液的位置 第一容器，用于向第一容器添加抗溶剂的入口，以及用于测量加入的抗溶剂量的装置。 还公开了一种用于形成纳米颗粒薄膜的方法，其包括使用含有底物的GEL，将溶液加压沉淀并将纳米颗粒沉积到基底上，除去溶剂从而留下薄的纳米颗粒膜，除去溶剂和反溶剂，并干燥该膜 。

公开(公告)号：US06303092B1

公开(公告)日：2001-10-16

申请号：US08419317

申请日：1995-04-10

申请人： Madhu Anand ,  Shivaji Sircar ,  Brian Thomas Carvill

发明人： Madhu Anand ,  Shivaji Sircar ,  Brian Thomas Carvill

IPC分类号： C01B3118

CPC分类号： C01B3/56 ,  B01D53/02 ,  B01D2257/504 ,  B01D2259/402 ,  B01J8/0005 ,  B01J8/008 ,  B01J8/04 ,  B01J19/0006 ,  B01J20/02 ,  B01J20/0211 ,  B01J20/0225 ,  B01J20/0233 ,  B01J20/0237 ,  B01J20/041 ,  B01J20/06 ,  B01J20/08 ,  B01J20/103 ,  B01J20/18 ,  B01J20/3204 ,  B01J20/3236 ,  B01J2208/00132 ,  B01J2208/00141 ,  B01J2208/00274 ,  B01J2208/00309 ,  B01J2208/0053 ,  B01J2208/00539 ,  B01J2208/0061 ,  C01B3/38 ,  C01B32/40 ,  C01B2203/02 ,  C01B2203/0233 ,  C01B2203/0238 ,  C01B2203/0283 ,  C01B2203/0405 ,  C01B2203/042 ,  C01B2203/043 ,  C01B2203/047 ,  C01B2203/0475 ,  C01B2203/0495 ,  C01B2203/0883 ,  C01B2203/1058 ,  C01B2203/1064 ,  C01B2203/1082 ,  C01B2203/1241 ,  C01B2203/147 ,  C01B2203/148 ,  C01B2203/80 ,  Y02C10/08 ,  Y02P20/152 ,  Y02P20/52

摘要： The present invention is a process for operating equilibrium controlled reactions in continuous mode wherein a feedstock is reacted in a plurality of reactors containing an admixture of a desired process catalyst and an adsorbent to form a product which is selectively adsorbed by the adsorbent and an admixture containing a product which is withdrawn from the reactor. A series of separation steps is used to desorb the product which is selectively adsorbed by the adsorbent and to prepare the reactor for a subsequent process cycle. The process utilizes a novel series of adsorption and desorption steps to collect the less selectively adsorbed product in substantially pure form under relatively constant flow rate at feedstock pressure.

摘要翻译： 本发明是一种在连续模式下操作平衡控制反应的方法，其中原料在含有所需工艺催化剂和吸附剂的混合物的多个反应器中反应以形成被吸附剂选择性吸附的产物和含有 从反应器中取出的产物。 一系列分离步骤用于解吸吸附剂选择性吸附的产物，并为随后的工艺循环制备反应器。 该方法利用新的一系列吸附和解吸步骤，以在原料压力下以相对恒定的流速收集基本上纯的形式的较少选择性吸附的产物。

公开(公告)号：US5013338A

公开(公告)日：1991-05-07

申请号：US403261

申请日：1989-09-01

申请人： Madhu Anand ,  Christine A. Costello ,  Keith D. Campbell

发明人： Madhu Anand ,  Christine A. Costello ,  Keith D. Campbell

IPC分类号： B01D69/12 ,  B01D71/44 ,  B05D7/24 ,  C08F8/42 ,  C08J7/18

CPC分类号： B05D1/62 ,  B01D69/127 ,  B01D71/44 ,  C08F8/42 ,  C08J7/18 ,  B05D2201/00

摘要： A composite of a rigid, glassy, permeable membrane of a silyl or germyl-containing polyacetylene and a thin surface layer of a plasma polymerized monomer having pendant nitrogen heterocycles is provided; the composite has high flux and selectivity and is particularly useful for separating gas mixtures containing at least two components having different permeabilities through the composite structure.

摘要翻译： 提供了具有含甲硅烷基或含锗基的聚乙炔的刚性，玻璃状，可渗透的膜和具有侧氮杂环的等离子体聚合单体的薄表面层的复合物。 该复合材料具有高通量和选择性，并且特别适用于通过复合结构分离含有至少两种具有不同渗透性的组分的气体混合物。

公开(公告)号：US4404256A

公开(公告)日：1983-09-13

申请号：US211488

申请日：1980-12-01

申请人： Madhu Anand ,  Raymond F. Baddour ,  Robert E. Cohen

发明人： Madhu Anand ,  Raymond F. Baddour ,  Robert E. Cohen

IPC分类号： B01J19/12 ,  C08F8/20 ,  C08J7/12 ,  C08F8/22

CPC分类号： B01J19/12 ,  B01J19/129 ,  C08F8/20 ,  C08J7/126 ,  B01J2219/0847 ,  B01J2219/0896 ,  Y10T428/2967 ,  Y10T428/2969 ,  Y10T428/31 ,  Y10T428/31544

摘要： Polymers having a substantially completely fluorinated surface of low surface energy and substantially free of oxygen and having a thickness up to about 200 Angstroms, the remainder of the polymer comprising a non-fluorinated polymer.

摘要翻译： 聚合物具有基本上完全氟化的表面能低表面能并且基本上不含氧并具有高达约200埃的厚度，其余的聚合物包含非氟化聚合物。

公开(公告)号：US08450545B2

公开(公告)日：2013-05-28

申请号：US12509253

申请日：2009-07-24

申请人： Glenn W. Dodwell ,  Joe D. Allison ,  Shetian Liu ,  Scott McQueen ,  Dennis G. Schultz ,  Byron G. Johnson ,  Madhu Anand ,  Melinda L. Johnson ,  Larry E. Reed ,  Brian C. Dunn

发明人： Glenn W. Dodwell ,  Joe D. Allison ,  Shetian Liu ,  Scott McQueen ,  Dennis G. Schultz ,  Byron G. Johnson ,  Madhu Anand ,  Melinda L. Johnson ,  Larry E. Reed ,  Brian C. Dunn

IPC分类号： C07C1/20

CPC分类号： B01J29/40 ,  B01J29/06 ,  B01J29/076 ,  B01J29/48 ,  B01J2229/123 ,  B01J2229/186 ,  B01J2229/32 ,  C10G3/44 ,  C10G3/49 ,  C10G2300/1011 ,  C10G2300/305 ,  C10G2400/02 ,  C10L1/06 ,  Y02P30/20

摘要： A process of modifying a zeolite catalyst to produce a modified zeolite catalyst wherein the modified zeolite catalyst has blocked pore sites. An oxygenated feed is flowed over the modified zeolite catalyst, wherein the oxygenated feed comprises hydrocarbons, methanol and dimethyl ether or a mixture thereof. The hydrocarbons, methanol and dimethyl ether in the oxygenated feed react with the modified zeolite catalyst to produce cyclic hydrocarbons, wherein the cyclic hydrocarbons produced has less than 10% durene and a median carbon number is C8.

摘要翻译： 一种改性沸石催化剂以制备改性沸石催化剂的方法，其中改性沸石催化剂具有阻塞的孔隙位点。 氧化进料流过改性沸石催化剂，其中含氧进料包括烃，甲醇和二甲醚或其混合物。 含氧进料中的烃，甲醇和二甲醚与改性沸石催化剂反应生成环状烃，其中产生的环状烃具有小于10％的杜烯，中位碳数为C8。

公开(公告)号：US08420564B2

公开(公告)日：2013-04-16

申请号：US13236326

申请日：2011-09-19

申请人： Madhu Anand ,  Joe D. Allison

发明人： Madhu Anand ,  Joe D. Allison

IPC分类号： B01J27/051 ,  B01J37/00 ,  C01G39/06

CPC分类号： C01G39/06 ,  B01J21/066 ,  B01J27/051 ,  B01J35/1014 ,  B01J35/1019 ,  B01J37/0203 ,  B01J37/088 ,  B01J37/10 ,  B01J37/18 ,  B01J37/20

摘要： A method of producing a MoS2 catalyst. The method begins by the decomposition of ammonium tetrathiomolybdate in an organic solvent. This decomposition is done in the presence of a solution comprising: a solvent and a promoter, and done under gaseous pressure.

摘要翻译： 一种制备MoS 2催化剂的方法。 该方法开始于有机溶剂中四硫代钼酸铵的分解。 这种分解是在包含溶剂和促进剂的溶液的存在下进行的，并在气压下进行。

公开(公告)号：US5770135A

公开(公告)日：1998-06-23

申请号：US673989

申请日：1996-07-01

申请人： John Peter Hobbs ,  James Francis DeiTos ,  Madhu Anand

发明人： John Peter Hobbs ,  James Francis DeiTos ,  Madhu Anand

IPC分类号： B29C49/04 ,  B29C49/46 ,  C08J7/12

CPC分类号： C08J7/126 ,  B29C49/46 ,  B29C49/04 ,  B29K2023/06 ,  B29K2023/12 ,  B29K2025/00

摘要： The present invention discloses an improved process for producing plastic containers with excellent resistance to permeation by solvents such as hydrocarbons, hydrocarbon fuels, and hydrocarbon fuels with organic additives including lower alkanols and ethers consistently and reliably. The process is related to a treatment of plastic containers in a controlled manner with fluorine containing gases while blow molding them. In the process of the present invention, an article of manufacture, a container, is formed and subjected to fluorination by exposure to a fluorination gas. After the fluorination, the container is quenched by exposing the container to a fluorine reactive gas to react with the fluorine, thereby converting the fluorine to a less reactive gas.

摘要翻译： 本发明公开了一种改进的生产塑料容器的方法，该方法具有优异的抗渗透性，通过诸如烃类，烃类燃料和烃类燃料的渗透性，并且可以一致地可靠地使用含有低级烷醇和醚的有机添加剂。 该方法涉及在吹塑它们时以含氟气体的受控方式处理塑料容器。 在本发明的方法中，形成制品，容器，并通过暴露于氟化气体进行氟化。 氟化后，通过将容器暴露于氟反应性气体以与氟反应而使容器淬火，从而将氟转化为较少反应性的气体。