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公开(公告)号:US20200083039A1
公开(公告)日:2020-03-12
申请号:US16614016
申请日:2018-04-03
发明人: Tsubasa HONKE , Kyoko OKITA
IPC分类号: H01L21/02 , C30B29/36 , H01L21/304
摘要: A TTV of the silicon carbide substrate is less than or equal to 3 μm. The first main surface includes a first central region surrounded by a square having each side of 90 mm. An intersection of diagonal lines of the first central region coincides with a center of the first main surface. The first central region is constituted of nine square regions each having each side of 30 mm. A maximum LTV among the nine square regions is less than or equal to 1 μm. An arithmetic mean roughness Sa in a second central region is less than or equal to 0.1 nm, the second central region being surrounded by a square centering on the intersection and having each side of 250 μm.
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12.
公开(公告)号:US20190242014A1
公开(公告)日:2019-08-08
申请号:US16340007
申请日:2018-07-20
发明人: Kenji KANBARA , Takaya MIYASE , Tsubasa HONKE
IPC分类号: C23C16/42 , C30B25/02 , C30B29/36 , H01L21/205 , H01L29/16
摘要: A silicon carbide epitaxial film has a plurality of arc-shaped or annular basal plane dislocations and a plurality of threading dislocations. The plurality of threading dislocations have a first threading dislocation which is surrounded by the plurality of basal plane dislocations and a second threading dislocation which is not surrounded by the plurality of basal plane dislocations, when viewed from a direction perpendicular to a main surface. The plurality of basal plane dislocations and the first threading dislocation constitute an annular defect. An area density of the plurality of threading dislocations in the main surface is more than or equal to 50 cm−2. A value obtained by dividing an area density of the annular defect when viewed from the direction perpendicular to the main surface by the area density of the plurality of threading dislocations in the main surface is more than or equal to 0.00002 and less than or equal to 0.004.
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公开(公告)号:US20180274129A1
公开(公告)日:2018-09-27
申请号:US15989373
申请日:2018-05-25
发明人: Tsubasa HONKE , Kyoko OKITA
IPC分类号: C30B33/12 , C09K3/14 , C09G1/02 , C01B32/956 , B24B37/04 , B08B3/08 , C30B29/36 , H01L21/02 , H01L21/306 , H01L29/04 , H01L29/16 , C30B33/10
CPC分类号: C30B33/12 , B08B3/08 , B24B37/00 , B24B37/044 , C01B32/956 , C09G1/02 , C09K3/1409 , C09K3/1463 , C30B29/36 , C30B33/10 , H01L21/02024 , H01L21/02052 , H01L21/30625 , H01L29/045 , H01L29/1608 , H01L29/34 , H01L29/78 , H01L29/861
摘要: A silicon carbide substrate is composed of silicon carbide, and when a main surface thereof is etched with chlorine gas, the overall length of linear etch-pit groups observed in the main surface is equal to or less than the diameter of the substrate.
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14.
公开(公告)号:US20160155808A1
公开(公告)日:2016-06-02
申请号:US15017235
申请日:2016-02-05
发明人: Tsubasa HONKE , Kyoko OKITA , Tomohiro KAWASE , Tsutomu HORI
CPC分类号: H01L29/1608 , C30B23/00 , C30B23/002 , C30B23/025 , C30B23/066 , C30B29/36 , H01L29/045 , Y10T428/21
摘要: Quality of a silicon carbide single crystal is improved. A crucible having first and second sides is prepared. A solid source material for growing silicon carbide with a sublimation method is arranged on the first side. A seed crystal made of silicon carbide is arranged on the second side. The crucible is arranged in a heat insulating container. The heat insulating container has an opening facing the second side. The crucible is heated such that the solid source material sublimes. A temperature on the second side is measured through the opening in the heat insulating container. The opening has a tapered inner surface narrowed toward the outside of the heat insulating container.
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公开(公告)号:US20140030892A1
公开(公告)日:2014-01-30
申请号:US13915107
申请日:2013-06-11
发明人: Tsubasa HONKE , Kyoko OKITA
IPC分类号: H01L21/04
CPC分类号: H01L21/0445 , C30B23/00 , C30B29/36 , C30B33/12 , H01L21/02019 , H01L21/02024 , H01L21/3065 , H01L29/1608
摘要: A method for manufacturing a silicon carbide substrate includes the steps of: preparing an ingot made of silicon carbide; obtaining a silicon carbide substrate by cutting the ingot prepared; etching a silicon surface of the silicon carbide substrate; and polishing the etching surface of the silicon carbide substrate after etching the silicon carbide substrate. The step of etching a silicon surface of the silicon carbide substrate includes the step of removing silicon atoms, which form the silicon carbide, from an etching region using chlorine gas, the etching region including the etching main surface of the silicon carbide substrate.
摘要翻译: 一种制造碳化硅基板的方法包括以下步骤:制备由碳化硅制成的铸块; 通过切割制备的锭获得碳化硅衬底; 蚀刻碳化硅衬底的硅表面; 并在蚀刻碳化硅衬底之后研磨碳化硅衬底的蚀刻表面。 蚀刻碳化硅衬底的硅表面的步骤包括从蚀刻区域使用氯气去除形成碳化硅的硅原子的步骤,该蚀刻区域包括碳化硅衬底的蚀刻主表面。
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公开(公告)号:US20220403550A1
公开(公告)日:2022-12-22
申请号:US17780355
申请日:2020-11-12
发明人: Kyoko OKITA , Tsubasa HONKE , Shunsaku UETA
摘要: A ratio obtained by dividing a number of pits by a number of screw dislocations is equal to or smaller than 1%. The first main surface has a surface roughness equal to or smaller than 0.15 nm. An absolute value of a difference between the first wave number and the second wave number is equal to or smaller than 0.2 cm−1, and an absolute value of a difference between the first full width at half maximum and the second full width at half maximum is equal to or smaller than 0.25 cm−1.
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公开(公告)号:US20220220637A1
公开(公告)日:2022-07-14
申请号:US17611138
申请日:2020-03-19
发明人: Tsubasa HONKE , Kyoko OKITA
摘要: A silicon carbide substrate has a first main surface, a second main surface, and a chamfered portion. The second main surface is opposite to the first main surface. The chamfered portion is contiguous to each of the first main surface and the second main surface. The silicon carbide substrate has a maximum diameter of 150 mm or more. A surface manganese concentration in the chamfered portion is 1×1011 atoms/cm2 or less.
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18.
公开(公告)号:US20220085172A1
公开(公告)日:2022-03-17
申请号:US17420416
申请日:2019-09-26
发明人: Tsubasa HONKE , Kyoko OKITA
摘要: A recycle wafer of silicon carbide has a silicon carbide substrate and a first silicon carbide layer. The silicon carbide substrate has a first main surface and a second main surface opposite to the first main surface. The first silicon carbide layer is in contact with the first main surface. The silicon carbide substrate includes a substrate region that is within 10 μm from the first main surface toward the second main surface. In a direction perpendicular to the first main surface, a value obtained by subtracting a value that is three times a standard deviation of a nitrogen concentration in the substrate region from an average value of the nitrogen concentration in the substrate region is greater than a minimum value of a nitrogen concentration in the first silicon carbide layer.
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公开(公告)号:US20180033703A1
公开(公告)日:2018-02-01
申请号:US15552863
申请日:2016-01-21
发明人: Tsubasa HONKE , Kyoko OKITA
IPC分类号: H01L21/66 , C23C14/34 , C23C14/58 , C30B29/36 , B24C1/08 , C30B33/02 , H01L21/027 , H01L21/306 , H01L29/66 , C23C14/06 , C30B25/20
CPC分类号: H01L22/20 , B24C1/08 , C23C14/0682 , C23C14/185 , C23C14/34 , C23C14/5806 , C23C16/325 , C30B25/186 , C30B25/20 , C30B29/36 , C30B31/20 , C30B33/02 , H01L21/02013 , H01L21/02024 , H01L21/027 , H01L21/265 , H01L21/304 , H01L21/30625 , H01L22/12 , H01L29/045 , H01L29/1608 , H01L29/66053 , H01L29/66068 , H01L29/7395 , H01L29/7802 , H01L29/8083 , H01L29/872
摘要: A silicon carbide single crystal substrate includes a first main surface and a second main surface opposite to the first main surface. The first main surface includes a central square region and an outer square region. When viewed in a thickness direction, each of the central square region and the outer square region has a side having a length of 15 mm. The first main surface has a maximum diameter of not less than 100 mm. The silicon carbide single crystal substrate has a TTV of not more than 5 μm. A value obtained by dividing a LTIR in the central square region by a LTV in the central square region is not less than 0.8 and not more than 1.2. A value obtained by dividing a LTV in the outer square region by the LTV in the central square region is not less than 1 and not more than 3.
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20.
公开(公告)号:US20170335489A1
公开(公告)日:2017-11-23
申请号:US15527121
申请日:2015-11-04
发明人: Tsubasa HONKE , Kyoko OKITA
IPC分类号: C30B33/12 , H01L29/04 , H01L21/306 , H01L21/02 , C30B29/36 , C01B32/956 , C09K3/14 , C09G1/02 , B24B37/04 , B08B3/08 , H01L29/16 , C30B33/10
CPC分类号: C30B33/12 , B08B3/08 , B24B37/00 , B24B37/044 , C01B32/956 , C09G1/02 , C09K3/1409 , C09K3/1463 , C30B29/36 , C30B33/10 , H01L21/02024 , H01L21/02052 , H01L21/30625 , H01L29/045 , H01L29/1608 , H01L29/34 , H01L29/78 , H01L29/861
摘要: A silicon carbide substrate is composed of silicon carbide, and when a main surface thereof is etched with chlorine gas, the overall length of linear etch-pit groups observed in the main surface is equal to or less than the diameter of the substrate.
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