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    Superabrasive particle synthesis with controlled placement of crystalline seeds
    21.
    发明授权
    Superabrasive particle synthesis with controlled placement of crystalline seeds 失效
    超级磨料颗粒合成，控制放置晶种

    公开(公告)号：US07368013B2

    公开(公告)日：2008-05-06

    申请号：US11175017

    申请日：2005-07-05

    Applicant: Chien-Min Sung

    Inventor： Chien-Min Sung

    IPC: C30B29/04

    CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B01J2203/0685 ,  B22F2005/001 ,  B22F2999/00 ,  B23D61/18 ,  B23D65/00 ,  B23P15/28 ,  B24D3/08 ,  B24D7/066 ,  B24D18/00 ,  B24D99/005 ,  B24D2203/00 ,  C04B35/52 ,  C09K3/1409 ,  C09K3/1445 ,  C22C1/051 ,  C22C26/00 ,  C22C2204/00 ,  E21B10/5676 ,  Y10T428/2991 ,  B22F2207/03 ,  B22F1/0011 ,  B22F3/004 ,  B22F2003/1046

    Abstract: An improved method for synthesizing superabrasive particles provides high quality industrial superabrasive particles with high yield and a narrow size distribution. The synthesis method can include forming a growth precursor of a substantially homogeneous mixture of raw material and catalyst material or layers of raw material and metal catalyst. The growth precursor can have a layer of adhesive over at least a portion thereof. A plurality of crystalline seeds can be placed in a predetermined pattern on the layer of adhesive. The growth precursor can be maintained at a temperature and pressure at which the superabrasive crystal is thermodynamically stable for a time sufficient for a desired degree of growth. Advantageously, the patterned placement of crystalline seeds and disclosed processes allow for production of various morphologies of synthetic diamonds, including octahedral and cubic diamonds, and improved growth conditions generally. As a result, the grown superabrasive particles typically have a high yield of high quality particles and a narrow distribution of particle sizes.

    Abstract translation: 合成超级磨料颗粒的改进方法提供高产率和窄尺寸分布的高质量工业超研磨颗粒。 合成方法可以包括形成原料和催化剂材料或原料和金属催化剂层的基本上均匀的混合物的生长前体。 生长前体可在其至少一部分上具有一层粘合剂。 多个结晶种子可以以预定图案放置在粘合剂层上。 生长前体可以保持在超磨料晶体在热力学稳定的温度和压力下达足以达到所需生长程度的时间。 有利地，结晶晶种的图案化布置和所公开的方法允许生产合成金刚石的各种形态，包括八面体和立方晶体，以及通常改善的生长条件。 结果，生长的超级磨料颗粒通常具有高产率的高质量颗粒和窄的粒度分布。

    High pressure superabrasive particle synthesis
    22.
    发明申请
    High pressure superabrasive particle synthesis 审中-公开
    高压超磨料颗粒合成

    公开(公告)号：US20070295267A1

    公开(公告)日：2007-12-27

    申请号：US11818894

    申请日：2007-06-14

    Applicant: Chien-Min Sung

    Inventor： Chien-Min Sung

    IPC: C30B19/02

    CPC classification number: E21B10/5676 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B01J2203/0685 ,  B22F2005/001 ,  B22F2999/00 ,  B23D61/18 ,  B23D65/00 ,  B23P15/28 ,  B24D3/08 ,  B24D7/066 ,  B24D18/00 ,  B24D99/005 ,  B24D2203/00 ,  C22C1/051 ,  C22C26/00 ,  C22C2204/00 ,  B22F2207/03 ,  B22F1/0011 ,  B22F3/004 ,  B22F2003/1046

    Abstract: An improved method for controlling nucleation sites during superabrasive particle synthesis can provide high quality industrial superabrasive particles with high yield and a narrow size distribution. The synthesis method can include forming a raw material layer, forming a particulate catalyst layer adjacent the raw material layer, and placing crystalline seeds in a predetermined pattern at least partially in the catalyst layer or raw material layer to form a growth precursor. Alternatively, the raw material and catalyst material can be mixed to form a particulate crystal growth layer and then placing the crystalline seeds in a predetermined pattern in the growth layer. Preferably, seeds can be substantially surrounded by catalyst material. The growth precursor can be maintained at a temperature and pressure at which the superabrasive crystal is thermodynamically stable for a time sufficient for a desired degree of growth. The crystalline seeds can be placed in a predetermined pattern using a template, a transfer sheet, vacuum chuck or similar techniques. The superabrasive particles grown using the described methods typically have a high yield of high quality industrial particles and a narrow distribution of particle sizes.

    Abstract translation: 在超磨料颗粒合成中控制成核位置的改进方法可以提供高产率和窄尺寸分布的高质量工业超研磨颗粒。 合成方法可以包括形成原料层，在原料层附近形成颗粒催化剂层，并将至少部分地将结晶晶种至少部分地放置在催化剂层或原料层中以形成生长前体。 或者，可以将原料和催化剂材料混合以形成颗粒状晶体生长层，然后将结晶种子以预定图案放置在生长层中。 优选地，种子可以被催化剂材料基本包围。 生长前体可以保持在超磨料晶体在热力学稳定的温度和压力下达足以达到所需生长程度的时间。 结晶种子可以使用模板，转印片，真空吸盘或类似技术以预定图案放置。 使用所述方法生长的超级磨料颗粒通常具有高产率的高质量工业颗粒和窄粒度分布。

    High pressure split die and associated methods
    24.
    发明授权
    High pressure split die and associated methods 有权
    高压分模和相关方法

    公开(公告)号：US07128547B2

    公开(公告)日：2006-10-31

    申请号：US10757715

    申请日：2004-01-13

    Applicant: Chien-Min Sung

    Inventor： Chien-Min Sung

    IPC: B28B3/00

    CPC classification number: B01J3/065 ,  B01J3/067 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B30B11/004 ,  B30B11/007 ,  Y10T29/49826 ,  Y10T29/49863 ,  Y10T29/49998 ,  Y10T29/51

    Abstract: An improved high pressure apparatus can include a plurality of complementary die segments. The die segments can have inner surfaces which are shaped to form a die chamber upon assembly of the die segments. A pair of anvils can be oriented such that an anvil is at each end of the die chamber. To prevent the die segments from being forced apart during movement of the anvils, force members can be connected to the die segments. The force members can apply discrete forces to the die segments sufficient to retain the die segments in substantially fixed positions relative to each other during application of force by the pair of anvils. Using such a high pressure apparatus can achieve pressures as high as 10 GPa with improved useful die life and larger reaction volumes.

    Abstract translation: 改进的高压装置可以包括多个互补的模片段。 模具段可以具有内表面，其在模具段的组装时成形为形成模腔。 一对砧座可以被定向成使得砧座在模腔的每个端部。 为了防止模具段在砧座移动期间被迫分开，可以将力构件连接到模具段。 力构件可以向模具段施加离散的力，足以在由一对砧施加力期间将模具段保持在相对于彼此的基本上固定的位置。 使用这种高压装置可以实现高达10GPa的压力，并且具有改善的有用的模具寿命和较大的反应体积。

    Boron doped blue diamond and its production
    28.
    发明申请
    Boron doped blue diamond and its production 审中-公开
    硼掺杂蓝钻石及其生产

    公开(公告)号：US20040018137A1

    公开(公告)日：2004-01-29

    申请号：US10262784

    申请日：2002-10-02

    Applicant: GENERAL ELECTRIC COMPANY

    Inventor： Yue Meng

    IPC: C01B031/06

    CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685 ,  B01J2203/0695

    Abstract: A method for synthesizing boron doped diamond for improving the oxidation resistance of said diamond crystals includes forming a fully dense core (mixture) of graphite, catalyst/solvent metals, optional diamond seed crystals, and a source of boron. This mixture is subjected to diamond-formed high pressure/high temperature (HP/HT) conditions for a time adequate for forming diamond. The thus-formed diamond product is recovered to contain boron substituted into the diamond structure. The fully dense core is substantially devoid of air/nitrogen (N) content. In one embodiment, the boron amorphous B.

    Abstract translation: 用于合成硼掺杂金刚石以提高所述金刚石晶体的抗氧化性的方法包括形成石墨，催化剂/溶剂金属，任选的金刚石晶种和硼源的完全致密的核心（混合物）。 将该混合物经受金刚石形成的高压/高温（HP / HT）条件一段足以形成金刚石的时间。 回收如此形成的金刚石产品以含有被取代成金刚石结构的硼。 完全致密的核基本上没有空气/氮（N）含量。 在一个实施方案中，硼无定形B.

    Methods for forming artificial diamond
    30.
    发明授权
    Methods for forming artificial diamond 失效
    形成人造金刚石的方法

    公开(公告)号：US5462772A

    公开(公告)日：1995-10-31

    申请号：US30506

    申请日：1993-05-13

    Applicant: Jerome H. Lemelson

    Inventor： Jerome H. Lemelson

    IPC: B01J3/08 ,  B01J19/08 ,  B01J19/12 ,  B21C23/08 ,  B21C25/08 ,  B21D26/06 ,  B22D31/00 ,  B22F3/20 ,  B23D79/00 ,  B24B31/00 ,  B29C47/36 ,  B29C47/54 ,  B30B11/26 ,  B05D3/06

    CPC classification number: B29C47/54 ,  B01J19/081 ,  B01J19/121 ,  B01J3/08 ,  B21C23/085 ,  B21C25/08 ,  B21D26/06 ,  B22D31/00 ,  B22F3/20 ,  B23D79/005 ,  B24B31/00 ,  B29C47/36 ,  B30B11/26 ,  B01J2203/061 ,  B01J2203/0655 ,  B29C47/0009 ,  H05K2203/175

    Abstract: New and improved structures in tools subject to wear and attrition when engaging or engaged by work or material being worked on thereby. Synthetic diamond material is formed in situ on a select portion or portions of the surface of a hard substrate or tool support to define or cover the portion of the tool substrate adjacent the work operated on by the tool in a manner to provide a hard wear resistant work engaging surface or surfaces which offers substantially greater resistance to abrasion and frictional deterioration than the material of the substrate or tool base. In one form, the synthetic diamond material is formed on and welded to the surface of the substrate in a single operation involving the application of intense radiant energy beamed against particles of carbon which are converted to a solid synthetic diamond structure of defined shape directly against the solid substrate. In a particular form, the synthetic diamond material is formed with a cutting edge for the tool having substantially the hardness and wear resistance of diamond.

    Abstract translation: 由于工作或材料被接合或接合而受到磨损和磨损的工具中的新的和改进的结构。 合成金刚石材料原位形成在硬质基材或工具支架的表面的选择部分或部分上，以限定或覆盖与工具操作的工件相邻的工具基板的部分，以提供耐磨损 工作接合表面或表面，其提供比基底或工具基底的材料显着更大的耐磨性和摩擦变差性。 在一种形式中，合成金刚石材料在单一操作中形成并焊接到基板的表面上，该操作涉及施加强度辐射能量的辐射能量，所述强度辐射能量被发射到碳颗粒上，所述强度辐射能量直接转换成定义形状的固体合成金刚石结构 固体基质。 在特定形式中，合成金刚石材料形成有用于工具的切割刃，具有基本上具有金刚石的硬度和耐磨性。

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