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81.发明授权公开(公告)号：US08114807B2
公开(公告)日：2012-02-14
申请号：US12718319
申请日：2010-03-05
CPC分类号： C07C5/10 , C07C29/17 , C07C45/62 , C07C205/06 , H01F1/01
摘要： An intermetallic magnetic compound of iron oxide and palladium with a nanometer particle size is disclosed, together with a method of making magnetic nanoparticles that include an intermetallic bond between palladium and iron-oxide. Additionally, a method is disclosed of catalyzing an organic reaction by contacting the organic reagents with an intermetallic magnetic compound of iron oxide and palladium that has nanometer particle size in an amount sufficient to catalyze the organic reaction.
摘要翻译： 公开了一种具有纳米粒度的氧化铁和钯的金属间磁性化合物，以及制备包括钯和氧化铁之间的金属间键的磁性纳米颗粒的方法。 另外，公开了通过使有机试剂与氧化铁和钯的金属间磁性化合物接触来催化有机反应的方法，该化合物具有足以催化有机反应的量的纳米粒径。
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82.发明申请公开(公告)号：US20110084035A1
公开(公告)日：2011-04-14
申请号：US12970017
申请日：2010-12-16
申请人： Robert N. Revesz
发明人： Robert N. Revesz
IPC分类号： B01D35/00
CPC分类号： G01N1/40 , B01L3/50255 , B01L2300/0803 , B01L2300/1866 , B01L2400/0478 , G01N1/4044 , G01N1/44 , G01N22/00 , Y10T436/25
摘要： A filtration method and associated apparatus are disclosed for improving the separation yield of matrix based compositions. The method includes the steps of positioning a matrix based composition that includes at least some liquid in a filter vessel and applying a moderate over-pressure to the composition upstream of the filter to accelerate the movement of liquid through the filter. The associated apparatus includes a funnel support, a funnel resting in the funnel support, a filter cup resting in the funnel opposite the funnel support, an over-pressure cap for engaging the filter cup opposite the funnel, and a source of pressurized gas in communication with the over-pressure cap for supplying a moderate over pressure to the filter cup for accelerating the movement of solvent through the filter cup and the funnel.
摘要翻译： 公开了一种用于改进基于基质的组合物的分离收率的过滤方法和相关设备。 该方法包括以下步骤：将基于基质的组合物定位在过滤器容器中，至少包括一些液体，并在过滤器上游施加适度的超压，以加速液体通过过滤器的运动。 相关联的装置包括漏斗支撑件，漏斗支撑件中的漏斗，与漏斗支架相对的漏斗中的过滤杯，与漏斗对接的过滤杯的过压帽以及与漏斗相对的加压气体源 其中过压帽用于向过滤杯提供适度的过压，以加速溶剂通过过滤杯和漏斗的运动。
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公开(公告)号：US07820951B2
公开(公告)日：2010-10-26
申请号：US11852480
申请日：2007-09-10
IPC分类号： H05B6/68
CPC分类号： H05B6/806 , B01J3/03 , B01J19/126 , B01J2219/0027 , B01J2219/00283 , B01J2219/00335 , B01J2219/00495 , B01J2219/0059 , B01J2219/1233 , B01J2219/1254 , B01J2219/1263 , B01J2219/1284 , H05B6/705 , H05B6/708 , Y10T436/25
摘要： An instrument for carrying out controlled microwave assisted chemical processes, and that is particularly useful for handling relatively small samples. The instrument includes a microwave-transparent reaction vessel with an open mouth, a pressure-resistant seal on the mouth of the vessel, and a needle, portions of which penetrate the seal with a first end of the needle and provide fluid communication into the vessel. A pressure transducer is at the opposite end of the needle and in fluid communication with the interior of the vessel through the needle. The instrument defines a pressure control flow path from a portion of the needle outside of the vessel to a fluid port, the flow path being in communication with the needle, the interior of the vessel and the transducer. A controllable pressure release valve for the flow path is associated with the port.
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84.发明授权公开(公告)号：US07816633B2
公开(公告)日：2010-10-19
申请号：US11853102
申请日：2007-09-11
CPC分类号： H05B6/806 , B01J19/0046 , B01J19/126 , B01J2219/00162 , B01J2219/002 , B01J2219/00231 , B01J2219/0024 , B01J2219/00283 , B01J2219/0034 , B01J2219/00353 , B01J2219/00477 , B01J2219/00495 , B01J2219/00601 , B01J2219/00689 , B01J2219/00691 , B01J2219/0869 , B01J2219/1215 , B01J2219/1239 , B01J2219/1275 , C40B60/14 , H05B6/6408
摘要： A method and associated instrument are disclosed for increasing the sequential rate at which a series of microwave assisted chemical reactions that potentially generate high pressure can be carried out. The method includes the steps of opening a pressure-resistant valve on a microwave-transparent pressure-resistant vessel to define a unpressurized pathway through the valve into the vessel, inserting a tube through the pathway in the valve and into the vessel, transferring at least one composition into the vessel through the tube, removing the tube from the vessel and from the pathway in the valve, closing the valve to seal the vessel against pressure release, and exposing the vessel and its contents to microwave radiation. The instrument includes a source of microwave radiation, a cavity in microwave communication with the source, an attenuator that forms at least a portion of the cavity, a pressure-resistant microwave-transparent reaction vessel having portions in the cavity and portions in the attenuator, a pressure-resistant valve on the mouth of the vessel, a reciprocating tube for passing through the valve and into the vessel when the valve is open, and means for mechanically inserting and retracting the tube through the valve and into the vessel when the vessel is in the cavity and the attenuator.
摘要翻译： 公开了一种方法和相关联的仪器，用于增加可以进行可能产生高压的一系列微波辅助化学反应的顺序速率。 该方法包括以下步骤：在微波透明耐压容器上打开耐压阀，以限定通过阀进入容器的非加压路径，将管穿过阀中的通道插入容器中，至少转移 一个组合物通过管子进入容器，从容器中取出管子并从阀门中的通道中取出管子，关闭阀门以密封容器以抵抗压力释放，并将容器及其内容物暴露于微波辐射。 仪器包括微波辐射源，与源极微波连通的空腔，形成空腔的至少一部分的衰减器，具有空腔中的部分和衰减器中的部分的耐压微波透明反应容器， 容器口上的耐压阀，当阀打开时通过阀门并进入容器的往复式管，以及用于当管是容器时通过阀机械地插入和收回管并进入容器的装置 在腔和衰减器中。
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公开(公告)号：US20100048865A1
公开(公告)日：2010-02-25
申请号：US12549445
申请日：2009-08-28
CPC分类号： B01J19/126 , B01J19/087 , B01J2219/0871 , B01J2219/0879 , B01J2219/1206 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , B01J2219/1221 , B01J2219/1254 , B01J2219/126 , B01J2219/1272 , B01J2219/1293 , C07K1/045 , C07K1/063 , C07K5/08 , C07K7/06
摘要： An instrument and method for accelerating the solid phase synthesis of peptides are disclosed. The method includes the steps of deprotecting a protected first amino acid linked to a solid phase resin by admixing the protected linked acid with a deprotecting solution in a microwave transparent vessel while irradiating the admixed acid and solution with microwaves, activating a second amino acid, coupling the second amino acid to the first acid while irradiating the composition in the same vessel with microwaves, and cleaving the linked peptide from the solid phase resin by admixing the linked peptide with a cleaving composition in the same vessel while irradiating the composition with microwaves.
摘要翻译： 公开了用于促进肽的固相合成的仪器和方法。 该方法包括以下步骤：通过将受保护的连接酸与去保护溶液混合在微波透明容器中，同时用微波照射混合的酸和溶液，活化第二个氨基酸，偶联 同时用微波在同一容器中照射组合物的第二个氨基酸，并且通过将相连的肽与裂解组合物在同一容器中混合同时用微波照射组合物来将固定相树脂切断连接的肽。
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86.发明申请公开(公告)号：US20080267841A1
公开(公告)日：2008-10-30
申请号：US12146511
申请日：2008-06-26
申请人： Edward Earl King
发明人： Edward Earl King
CPC分类号： H05B6/806 , B01J19/126 , B01J2219/00051 , B01J2219/00162 , B01J2219/1206 , B01J2219/1215 , B01J2219/126 , B01J2219/1269 , B01J2219/1275 , B01J2219/1278 , B01J2219/1281 , B01J2219/1284 , B01J2219/1293
摘要： An instrument and associated method are disclosed for conducting microwave assisted chemical reactions. The instrument includes a microwave cavity, preferably a closed microwave cavity, for conducting microwave assisted chemical reactions, and a source for applying microwave radiation within the cavity and to a vessel and its contents. The instrument also includes an illumination source for illuminating the vessel and its contents, as well as means for visually observing the vessel and its contents, an infrared detector for monitoring the temperature of the vessel and its contents, and means for preventing the illumination source from saturating the infrared detector, thereby enabling concurrent visual observation and infrared monitoring.
摘要翻译： 公开了用于进行微波辅助化学反应的仪器和相关方法。 仪器包括用于进行微波辅助化学反应的微波腔，优选封闭的微波腔，以及用于在空腔内以及容器及其内容物施加微波辐射的源。 仪器还包括用于照明容器及其内容物的照明源，以及用于目视观察容器及其内容物的装置，用于监测容器及其内容物的温度的红外检测器，以及用于防止照明源 使红外线检测器饱和，从而实现视觉观察和红外监测。
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87.发明授权公开(公告)号：US07307248B2
公开(公告)日：2007-12-11
申请号：US10707376
申请日：2003-12-09
CPC分类号： H05B6/806 , B01J19/0046 , B01J19/126 , B01J2219/00162 , B01J2219/002 , B01J2219/00231 , B01J2219/0024 , B01J2219/00283 , B01J2219/0034 , B01J2219/00353 , B01J2219/00477 , B01J2219/00495 , B01J2219/00601 , B01J2219/00689 , B01J2219/00691 , B01J2219/0869 , B01J2219/1215 , B01J2219/1239 , B01J2219/1275 , C40B60/14 , H05B6/6408
摘要： A method and associated instrument are disclosed for increasing the sequential rate at which a series of microwave assisted chemical reactions that potentially generate high pressure can be carried out.
摘要翻译： 公开了一种方法和相关联的仪器，用于增加可以进行可能产生高压的一系列微波辅助化学反应的顺序速率。
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公开(公告)号：US07220591B2
公开(公告)日：2007-05-22
申请号：US10852621
申请日：2004-05-24
申请人： Michael J. Collins , Edward E. King
发明人： Michael J. Collins , Edward E. King
CPC分类号： G01R33/44 , G01N24/081 , G01N24/085 , Y10T436/24
摘要： A method and apparatus for rapidly and accurately determining the fat and oil content of a sample using microwave drying and NMR analysis is disclosed. The method and apparatus incorporate a low mass, porous, hydrophilic and lipophilic sample pad that ensures that the entire sample is subjected to NMR analysis. The method and apparatus according to the invention are suitable for rapidly determining the fat and oil content of samples collected during a production process and for process or quality control.
摘要翻译： 公开了一种使用微波干燥和NMR分析快速准确地测定样品的油脂含量的方法和装置。 该方法和设备结合了低质量，多孔，亲水和亲脂性样品垫，确保整个样品进行NMR分析。 根据本发明的方法和设备适用于快速测定在生产过程中收集的样品的脂肪和油含量以及过程或质量控制。
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89.发明授权公开(公告)号：US07144739B2
公开(公告)日：2006-12-05
申请号：US10065851
申请日：2002-11-26
申请人： William E. Jennings
发明人： William E. Jennings
CPC分类号： G01N15/1456 , G01N1/44
摘要： A pressure-sealing, pressure-monitoring closure for non-invasively sealing a reaction vessel to a defined release pressure in microwave-assisted chemistry is disclosed. The closure includes a pressure-resistant, microwave-transparent reaction vessel, one portion of which defines a mouth, a flexible pressure-transmitting releasable cover assembly on the mouth of the vessel, a pressure transducer on the cover and external to the vessel for monitoring the pressure in the vessel as exerted against the flexible cover, and a clamp for urging the vessel, the cover and the transducer together under a defined force so that when the pressure in the vessel exceeds the defined force, the cover can flex and release the pressure from the vessel.
摘要翻译： 公开了一种用于在微波辅助化学中非侵入性密封反应容器至限定释放压力的压力密封压力监测封闭件。 封闭件包括耐压微波透明的反应容器，其一部分限定了一个口，容器口上的柔性压力传递的可释放的盖组件，盖上的压力传感器和用于监测的容器的外部 容器中对柔性盖施加的压力，以及用于在限定的力下将容器，盖和换能器一起推动的夹具，使得当容器中的压力超过限定的力时，盖可以弯曲并释放 来自船只的压力。
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公开(公告)号：US06926939B2
公开(公告)日：2005-08-09
申请号：US10064718
申请日：2002-08-09
IPC分类号： B01J3/04 , B01J19/02 , B01J19/12 , F16J13/02 , G01N1/44 , G01N35/00 , H05B6/64 , H05B6/80 , B32B1/08 , A61L2/12 , B01L9/00 , B01L11/00
CPC分类号： H05B6/806 , B01J3/048 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/0295 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , F16J13/02 , G01N1/44 , G01N2035/00405 , H05B6/6408 , Y10T428/131 , Y10T428/1314 , Y10T428/1321 , Y10T428/1366 , Y10T428/1369 , Y10T428/139 , Y10T428/1393
摘要： A self sealing vessel assembly for high pressure microwave assisted chemistry is disclosed. The vessel assembly includes a polymeric cylinder and a circular polymeric cap for the cylinder, the cylinder being closed at one end and open at the other end to receive the cap. The open end of the cylinder has a lip that is beveled inwardly from the open end, and the circular polymeric cap has a beveled lower edge that engages the beveled lip when the cap is place upon the polymericcylinder. For high pressure applications, a choke cylinder depends from the beveled lower edge of the cap, and has an outer diameter substantially the same as the inner diameter of the polymeric cylinder so that the choke provides a self sealing mechanism for the cylinder as pressure from a chemical reaction increases within the cylinder. A composite sleeve surrounds the polymeric cylinder, and includes at least one wound fabric layer in which the winding is selected from the group consisting of filaments and yarns. A supporting frame extends along the cylinder and across the lid and across the closed end of the cylinder, and prevents the lid from being displaced from the cylinder when pressure is generated inside of the vessel.
摘要翻译： 公开了一种用于高压微波辅助化学的自密封容器组件。 容器组件包括聚合物圆筒和用于圆柱体的圆形聚合物盖，所述圆筒在一端封闭并在另一端开口以接收盖。 圆柱体的开口端具有从开口端向内倾斜的唇缘，并且圆形聚合物盖具有斜面下边缘，当帽位于聚合圆筒上时，该下边缘接合倾斜的唇缘。 对于高压应用，阻塞气缸从盖的斜面下边缘取向，并且具有与聚合物圆筒的内径基本相同的外径，使得扼流圈为气缸提供自密封机构，作为来自 化学反应在气缸内增加。 复合套管围绕聚合物圆筒，并且包括至少一个缠绕织物层，其中绕组选自长丝和纱线。 支撑框架沿着圆柱体延伸并且横过盖子并且横过气缸的封闭端延伸，并且当在容器内部产生压力时防止盖子从气缸移位。
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