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公开(公告)号:US09336985B2
公开(公告)日:2016-05-10
申请号:US14684825
申请日:2015-04-13
Applicant: FEI Company
Inventor: Jeffrey Blackwood , Stacey Stone
IPC: H01J37/28 , H01J37/18 , H01J37/20 , H01J37/06 , G01N23/04 , G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , H01J37/305 , H01J37/26
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
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公开(公告)号:US20150260784A1
公开(公告)日:2015-09-17
申请号:US14432712
申请日:2013-10-04
Applicant: FEI COMPANY
Inventor: Jeffrey Blackwood , Sang Hoon Lee , Michael Schmidt , Stacey Stone , Karey Holland
IPC: G01R31/265 , H01J37/153
CPC classification number: G01R31/2653 , G01N1/286 , G01N1/32 , G01R31/2808 , G01R31/2898 , G01R31/307 , G01R31/312 , H01J37/153 , H01J37/3005 , H01J2237/208 , H01J2237/24564 , H01J2237/2817 , H01J2237/31749 , H01L22/14 , H01L2924/0002 , H01L2924/00
Abstract: Multiple planes within the sample are exposed from a single perspective for contact by an electrical probe. The sample can be milled at a non-orthogonal angle to expose different layers as sloped surfaces. The sloped edges of multiple, parallel conductor planes provide access to the multiple levels from above. The planes can be accessed, for example, for contacting with an electrical probe for applying or sensing a voltage. The level of an exposed layer to be contacted can be identified, for example, by counting down the exposed layers from the sample surface, since the non-orthogonal mill makes all layers visible from above. Alternatively, the sample can be milled orthogonally to the surface, and then tilted and/or rotated to provide access to multiple levels of the device. The milling is preferably performed away from the region of interest, to provide electrical access to the region while minimizing damage to the region.
Abstract translation: 样品中的多个平面从单个角度暴露出来,用于通过电探针进行接触。 样品可以以非正交角度研磨,以将不同的层暴露于倾斜的表面。 多个平行导体平面的倾斜边缘可从上方进入多个层次。 例如,可以访问平面,以便与用于施加或感测电压的电探针接触。 可以例如通过从样品表面倒下暴露的层来鉴定待接触的暴露层的水平,因为非正交磨机使得所有层从上方可见。 或者,样品可以与表面正交地研磨,然后倾斜和/或旋转以提供对该装置的多个级别的访问。 铣削优选地远离感兴趣的区域进行,以提供对该区域的电通路,同时使对该区域的损害最小化。
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23.
公开(公告)号:US20150102009A1
公开(公告)日:2015-04-16
申请号:US14514199
申请日:2014-10-14
Applicant: FEI Company
Inventor: Michael Moriarty , Stacey Stone , Jeffrey Blackwood
CPC classification number: G01N1/32 , G01N1/286 , G01N2001/2886 , H01J37/02 , H01J37/3056 , H01J2237/20 , H01J2237/2802 , H01J2237/31745 , H01L21/02318
Abstract: A method and apparatus for preparing thin TEM samples in a manner that reduces or prevents bending and curtaining is realized. Embodiments of the present invention deposit material onto the face of a TEM sample during the process of preparing the sample. In some embodiments, the material can be deposited on a sample face that has already been thinned before the opposite face is thinned, which can serve to reinforce the structural integrity of the sample and refill areas that have been over-thinned due to a curtaining phenomena. In other embodiments, material can also be deposited onto the face being milled, which can serve to reduce or eliminate curtaining on the sample face.
Abstract translation: 实现了以减少或防止弯曲和卷曲的方式制备薄TEM样品的方法和装置。 在制备样品的过程中,本发明的实施方案将材料沉积在TEM样品的表面上。 在一些实施例中,材料可以沉积在样品面上,该样品表面在相对面变薄之前已经变薄,这可以用于增强样品的结构完整性并且由于存在现象而已经被过度稀释的区域 。 在其他实施例中,材料也可以沉积到被研磨的面上,这可以用于减少或消除样品面上的绘制。
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24.
公开(公告)号:US09006651B2
公开(公告)日:2015-04-14
申请号:US14029368
申请日:2013-09-17
Applicant: FEI Company
Inventor: Jeffrey Blackwood , Stacey Stone
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
Abstract translation: 一种用于S / TEM样品制备和分析的改进方法和装置。 本发明的优选实施例提供用于TEM样品制备的改进方法,特别是对于小几何(<100nm厚)TEM薄片。 新颖的样品结构和铣削图案的新颖应用允许产生薄至50nm的S / TEM样品,而没有显着的弯曲或翘曲。 本发明的优选实施方案提供了部分或全部自动化TEM样品制备的方法,使TEM样品的创建和分析过程减少劳动密集度,并提高TEM分析的产量和再现性。
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公开(公告)号:US11315756B2
公开(公告)日:2022-04-26
申请号:US16012888
申请日:2018-06-20
Applicant: FEI Company
Inventor: Stacey Stone , Sang Hoon Lee , Jeffrey Blackwood , Michael Schmidt , Hyun Hwa Kim
IPC: H01J37/317 , H01J37/305
Abstract: A method for analyzing a sample with a charged particle beam including directing the beam toward the sample surface; milling the surface to expose a second surface in the sample in which the end of the second surface distal to ion source is milled to a greater depth relative to a reference depth than the end of the first surface proximal to ion source; directing the charged particle beam toward the second surface to form one or more images of the second surface; forming images of the cross sections of the multiple adjacent features of interest by detecting the interaction of the electron beam with the second surface; assembling the images of the cross section into a three-dimensional model of one or more of the features of interest. A method for forming an improved fiducial and determining the depth of an exposed feature in a nanoscale three-dimensional structure is presented.
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公开(公告)号:US10825651B2
公开(公告)日:2020-11-03
申请号:US16410774
申请日:2019-05-13
Applicant: FEI Company
Inventor: Valerie Brogden , Jeffrey Blackwood , Michael Schmidt , Dhruti Trivedi , Richard J. Young , Thomas G. Miller , Brian Roberts Routh, Jr. , Stacey Stone , Todd Templeton
IPC: H01J37/302 , H01J37/31 , H01J37/304 , G01N1/28 , H01J37/28 , H01J37/285
Abstract: Techniques are described that facilitate automated extraction of lamellae and attaching the lamellae to sample grids for viewing on transmission electron microscopes. Some embodiments of the invention involve the use of machine vision to determine the positions of the lamella, the probe, and/or the TEM grid to guide the attachment of the probe to the lamella and the attachment of the lamella to the TEM grid. Techniques that facilitate the use of machine vision include shaping a probe tip so that its position can be readily recognized by image recognition software. Image subtraction techniques can be used to determine the position of the lamellae attached to the probe for moving the lamella to the TEM grid for attachment. In some embodiments, reference structures are milled on the probe or on the lamella to facilitate image recognition.
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公开(公告)号:US20190272975A1
公开(公告)日:2019-09-05
申请号:US16410774
申请日:2019-05-13
Applicant: FEI Company
Inventor: Valerie Brogden , Jeffrey Blackwood , Michael Schmidt , Dhruti Trivedi , Richard J. Young , Thomas G. Miller , Brian Roberts Routh, JR. , Stacey Stone , Todd Templeton
IPC: H01J37/302 , H01J37/285 , H01J37/31 , G01N1/28 , H01J37/28 , H01J37/304
Abstract: Techniques are described that facilitate automated extraction of lamellae and attaching the lamellae to sample grids for viewing on transmission electron microscopes. Some embodiments of the invention involve the use of machine vision to determine the positions of the lamella, the probe, and/or the TEM grid to guide the attachment of the probe to the lamella and the attachment of the lamella to the TEM grid. Techniques that facilitate the use of machine vision include shaping a probe tip so that its position can be readily recognized by image recognition software. Image subtraction techniques can be used to determine the position of the lamellae attached to the probe for moving the lamella to the TEM grid for attachment. In some embodiments, reference structures are milled on the probe or on the lamella to facilitate image recognition.
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公开(公告)号:US10340119B2
公开(公告)日:2019-07-02
申请号:US15464307
申请日:2017-03-20
Applicant: FEI Company
Inventor: Valerie Brogden , Jeffrey Blackwood , Michael Schmidt , Dhruti Trivedi , Richard J. Young , Thomas G. Miller , Brian Roberts Routh, Jr. , Stacey Stone , Todd Templeton
IPC: H01J37/302 , H01J37/31 , H01J37/28 , H01J37/304 , H01J37/285 , G01N1/28
Abstract: Techniques are described that facilitate automated extraction of lamellae and attaching the lamellae to sample grids for viewing on transmission electron microscopes. Some embodiments of the invention involve the use of machine vision to determine the positions of the lamella, the probe, and/or the TEM grid to guide the attachment of the probe to the lamella and the attachment of the lamella to the TEM grid. Techniques that facilitate the use of machine vision include shaping a probe tip so that its position can be readily recognized by image recognition software. Image subtraction techniques can be used to determine the position of the lamellae attached to the probe for moving the lamella to the TEM grid for attachment. In some embodiments, reference structures are milled on the probe or on the lamella to facilitate image recognition.
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29.
公开(公告)号:US20170250055A1
公开(公告)日:2017-08-31
申请号:US15595773
申请日:2017-05-15
Applicant: FEI Company
Inventor: Paul Keady , Brennan Peterson , Guus Das , Craig Matthew Henry , Larry Dworkin , Jeff Blackwood , Stacey Stone , Michael Schmidt
IPC: H01J37/305 , H01J37/20 , H01J37/28
CPC classification number: H01J37/3056 , C23C14/5833 , C23F1/02 , G01N1/32 , H01J37/20 , H01J37/28 , H01J37/3005 , H01J2237/024 , H01J2237/20207 , H01J2237/31745 , H01J2237/31749
Abstract: A method for TEM sample preparation and analysis that can be used in a FIB-SEM system without re-welds, unloads, user handling of the lamella, or a motorized flip stage. The method allows a dual beam FIB-SEM system with a typical tilt stage to be used to extract a sample to from a substrate, mount the sample onto a TEM sample holder capable of tilting, thin the sample using FIB milling, and rotate the sample so that the sample face is perpendicular to an electron column for STEM imaging.
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公开(公告)号:US09741536B2
公开(公告)日:2017-08-22
申请号:US14433354
申请日:2013-10-04
Applicant: FEI Company
Inventor: Sang Hoon Lee , Stacey Stone , Jeffrey Blackwood , Michael Schmidt
IPC: G01R23/02 , H01J37/305 , H01J37/28 , H01J37/317 , C23C14/46 , G01N1/32
CPC classification number: H01J37/3053 , C23C14/46 , G01N1/32 , H01J37/28 , H01J37/3056 , H01J37/3178 , H01J2237/3174 , H01J2237/31745 , H01J2237/31749
Abstract: Curtaining artifacts on high aspect ratio features are reduced by reducing the distance between a protective layer and feature of interest. For example, the ion beam can mill at an angle to the work piece surface to create a sloped surface. A protective layer is deposited onto the sloped surface, and the ion beam mills through the protective layer to expose the feature of interest for analysis. The sloped mill positions the protective layer close to the feature of interest to reduce curtaining.
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