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    High pressure parallel reactor with individually sealable vessels
    71.
    发明申请
    High pressure parallel reactor with individually sealable vessels 有权
    具有单独密封容器的高压并联反应器

    公开(公告)号：US20030202911A1

    公开(公告)日：2003-10-30

    申请号：US10317315

    申请日：2002-12-12

    Applicant: Symyx Technologies, Inc.

    Inventor： Lynn Van Erden ,  William H. Chandler JR.

    IPC: B01J019/00

    CPC classification number: B01J3/04 ,  B01J19/0046 ,  B01J2219/00283 ,  B01J2219/00308 ,  B01J2219/00313 ,  B01J2219/00315 ,  B01J2219/00335 ,  B01J2219/00477 ,  B01J2219/00585 ,  B01J2219/00601 ,  B01J2219/0072 ,  B01J2219/00745 ,  B01J2219/00747 ,  C40B30/08 ,  C40B40/18 ,  C40B60/14 ,  Y10T436/25

    Abstract: An apparatus and method for synthesis and screening of materials are disclosed. According to one aspect of the present invention, a parallel batch reactor for effecting chemical reactions includes a pressure chamber, an inlet port, two or more reaction vessels within the pressure chamber, and a reaction vessel cover. The inlet port is in fluid communication with the pressure chamber, and pressurizes the pressure chamber from an external pressure source. Each of the two or more reaction vessels are in isolatable fluid communication with the pressure chamber such that during a first pressurizing stage of operation, each of the two or more reaction vessels can be simultaneously pressurized through common fluid communication with the pressure chamber. In addition, during at least a second reaction stage of operation, each of the two or more pressurized reaction vessels can be isolated from each other by positioning the reaction vessel cover appropriately.

    Abstract translation: 公开了一种合成和筛选材料的装置和方法。 根据本发明的一个方面，用于实现化学反应的并行批量反应器包括压力室，入口，压力室内的两个或更多个反应容器和反应容器盖。 入口与压力室流体连通，并从外部压力源对压力室加压。 两个或更多个反应容器中的每一个与压力室可分离流体连通，使得在操作的第一加压阶段期间，两个或更多个反应容器中的每一个可以通过与压力室的常见流体连通同时加压。 此外，在操作的至少第二反应阶段中，通过适当地定位反应容器盖，可以将两个或更多个加压反应容器中的每一个彼此隔离。

    Microreactor
    73.
    发明申请
    Microreactor 审中-公开
    微反应器

    公开(公告)号：US20030175168A1

    公开(公告)日：2003-09-18

    申请号：US10367167

    申请日：2003-02-14

    Inventor： Mark Peter Timothy Gilligan ,  Philip James Homewood ,  Rowland Whiffin

    IPC: B01J019/00

    CPC classification number: B01J19/0093 ,  B01J2219/00783 ,  B01J2219/00835 ,  B01J2219/00889 ,  B01J2219/0095 ,  B01J2219/00959 ,  B01J2219/00975 ,  B01J2219/00977

    Abstract: A method of optimising a reaction in a microreactor. Two reaction fluids A, B as supplied to a microchannel 6 and their relative proportions are varied in a controlled manner. A sensor 13 monitors a reaction characteristic and determines the relative proportion of the fluids which optimises the yield of the reaction product. The total flow rate can also be varied at the optimum relative proportion in order to determine the maximum overall flow rate at which completion of the reactions still occurs.

    Abstract translation: 一种在微反应器中优化反应的方法。 提供给微通道6的两个反应流体A，B及其相对比例以受控的方式变化。 传感器13监测反应特性，并确定优化反应产物收率的流体的相对比例。 总流速也可以以最佳相对比例变化，以确定仍然发生反应完成的最大总流速。

    Coking and carburization resistant iron aluminides for hydrocarbon cracking
    77.
    发明申请
    Coking and carburization resistant iron aluminides for hydrocarbon cracking 有权
    用于碳氢化合物开裂的焦化和渗碳的铁铝化物

    公开(公告)号：US20020187091A1

    公开(公告)日：2002-12-12

    申请号：US09876917

    申请日：2001-06-11

    Inventor： Seetharama C. Deevi

    IPC: B01J019/00

    CPC classification number: B01J19/02 ,  B01J8/067 ,  B01J19/0026 ,  B01J23/06 ,  B01J2219/00247 ,  B01J2219/0236 ,  B01J2219/024 ,  C10G9/203 ,  C10G11/00 ,  C23C4/16 ,  C23C24/08 ,  C23C26/00 ,  C23C28/00 ,  C23C28/023 ,  Y10S585/92

    Abstract: A cracking tube includes a lining of a fouling resistant and corrosion resistant iron aluminide alloy. The iron aluminide alloy can include 14-32 wt. % Al, at least 2 vol. % transition metal oxides, 0.003 to 0.020 wt. % B, 0.2 to 2.0 wt. % Mo, 0.05 to 1.0 wt. % Zr, 0.2 to 2.0 wt. %Ti, 0.10 to 1.0 wt. % La, 0.05 to 0.2 wt. % C., balance Fe, and optionallynull1 wt. % Cr, and the coefficient of thermal expansion of the iron aluminide alloy is substantially the same as the coefficient of thermal expansion over the temperature range of ambient to about 1200null C. of an outer metal layer. A cracking tube utilizing the iron aluminide alloy can be formed from powders of the iron aluminide alloy by consolidation methods including cold isostatic pressing (CIP), hot isostatic pressing (HIP), reaction synthesis, spraying techniques, or co-extrusion with a second material of the cracking tube.

    Abstract translation: 裂解管包括防结垢和耐腐蚀的铁铝化合物的衬里。 铁铝化合物可以包括14-32wt。 ％Al，至少2体积％ ％过渡金属氧化物，0.003至0.020重量％ ％B，0.2〜2.0重量％ ％Mo，0.05〜1.0重量％ ％Zr，0.2〜2.0重量％ ％Ti，0.10〜1.0wt。 ％La，0.05〜0.2wt。 ％C，余量为Fe，任选地<= 1wt。 ％Cr，并且铁铝化合物合金的热膨胀系数与外部金属层的环境温度至约1200℃的温度范围内的热膨胀系数基本相同。 使用铁铝化物合金的裂解管可以通过包括冷等静压（CIP），热等静压（HIP），反应合成，喷涂技术或与第二材料共挤出的固结方法由铁铝化物合金的粉末形成 的裂化管。

    Gelatinous wood preservative
    78.
    发明申请
    Gelatinous wood preservative 失效
    凝胶木防腐剂

    公开(公告)号：US20020172614A1

    公开(公告)日：2002-11-21

    申请号：US09818487

    申请日：2001-03-27

    Inventor： David J. Ostby ,  Michael J. Maloney

    IPC: A61L011/00 ,  B01J019/00

    CPC classification number: E01B9/28 ,  B27K3/0264 ,  B27K3/12 ,  B27K3/20 ,  B27K3/30 ,  E01B31/20

    Abstract: The general purpose of this invention is to provide an improved apparatus and method of preserving the vulnerable area of a railroad cross tie near the interface of the tie and the tie plate. To attain this purpose the invention provides a thin preservative-bearing gelatinous material that is placed between the cross tie and the tie plate either at the time of the original laying of rail or during any subsequent relaying. No extra equipment is needed and only a negligible amount of labor is required to simply place the gelatinous material on the adzed surface of the cross tie prior to the mounting or remounting of the rail. The presence of the gelatinous material poses absolutely no resistance to the subsequent driving of the spikes into the tie and is thin enough so as not to pose any rail alignment problems. The use of the gelatinous material relies on the moisture found under the tie plate to leach the active ingredients out of the material and help diffuse them throughout the adjacent section of wood. In addition, the unloading and loading of the tie plate by the passing of a train forces moisture into and out of the gelatinous material to further promote the leaching action. The inert components of the gelatinous material are completely biodegradable and will not pose an environmental problem at the end of the material's service life.

    Abstract translation: 本发明的总体目的是提供一种改进的装置和方法，其保持靠近接头和连接板的界面处的铁路十字架的易损区域。 为了实现这个目的，本发明提供了一种薄的防腐剂的凝胶状材料，其在原始铺设轨道时或在任何后续的中继期间放置在十字架和连接板之间。 在安装或重新安装轨道之前，不需要额外的设备，只需要少量的人力来简单地将凝胶状材料放置在十字架的加固表面上。 凝胶状材料的存在对于随后将扎带驱动到扎带中是绝对没有阻力的，并且足够薄以便不引起任何轨道对准问题。 凝胶状材料的使用依赖于在连接板下面发现的水分，将活性成分从材料中浸出，并帮助它们扩散到木材的相邻部分。 此外，通过列车的卸载和装载连接板将使潮湿进入和流出凝胶状材料以进一步促进浸出作用。 凝胶状材料的惰性成分是完全可生物降解的，在材料使用寿命结束时不会造成环境问题。

    Sequential injection liquid-liquid extraction
    80.
    发明申请
    Sequential injection liquid-liquid extraction 失效
    顺序注射液 - 液萃取

    公开(公告)号：US20020106319A1

    公开(公告)日：2002-08-08

    申请号：US09773464

    申请日：2001-02-02

    Inventor： Duane K. Wolcott

    IPC: B01J019/00

    CPC classification number: G01N1/34 ,  G01N2001/4061 ,  G01N2030/009 ,  Y10T436/117497 ,  Y10T436/118339 ,  Y10T436/255

    Abstract: Apparatus and method for sequential injection liquid-liquid extraction analysis. Under the control of a bidirectional precision pump, a stream-selection valve, and a microprocessor, a series of liquid zones is built up in a holding/mixing coil. The liquid zones are transferred from the holding/mixing coil to a separation cell. After phase separation into an extract and a raffinate, the extract is withdrawn from the separation cell and sent to a detector, which determines the amount of a component which was extracted from a sample by an extraction solvent. The principal advantages of this automated technology are elimination of the need for dynamic phase separation; on-line pre-extraction chemical conditioning; a substantial reduction in solvent, reagent, and sample usage; and a similar substantial reduction in waste generation.

    Abstract translation: 连续注射液 - 液萃取分析装置及方法。 在双向精密泵，流量选择阀和微处理器的控制下，在保持/混合盘管中建立了一系列液体区域。 液体区域从保持/混合盘管转移到分离单元。 在分离成萃取液和萃余液之后，将萃取物从分离池中取出并送至检测器，检测器确定通过萃取溶剂从样品中提取的组分的量。 这种自动化技术的主要优点是消除了动态相分离的需要; 在线预提取化学调理; 溶剂，试剂和样品用量大幅减少; 并大大减少了废物的产生。

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