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1.发明申请公开(公告)号：US20180094475A1
公开(公告)日：2018-04-05
申请号：US15722581
申请日：2017-10-02
发明人： Takashi NAITO , Kei YOSHIMURA , Yuji HASHIBA , Shinichi TACHIZONO , Takuya AOYAGI , Tatsuya MIYAKE
CPC分类号： E06B3/66342 , C03C3/122 , C03C8/02 , C03C8/14 , C03C8/18 , C03C8/20 , C03C8/24 , C03C2207/00 , E06B3/6612 , E06B3/6733 , E06B3/6736 , E06B3/677 , E06B3/6775 , Y02A30/25 , Y02B80/24
摘要： Provided are a vacuum heat insulating member which includes: a first substrate; a second substrate; and a sealing part disposed between the first substrate and the second substrate, in which an internal space is formed by surrounding by the first substrate, the second substrate and the sealing part, and in which the sealing part includes a glass phase and a metal phase, the metal phase being disposed on a side of the internal space of the glass phase. Thus, in the vacuum heat insulating member, an amount of a gas released from the glass phase to the internal space can be decreased and a high heat insulating property can be kept.
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2.发明申请LEAD-FREE LOW-MELTING GLASS COMPOSITION, LOW-TEMPERATURE SEALING GLASS FRIT, LOW-TEMPERATURE SEALING GLASS PASTE, CONDUCTIVE MATERIAL, AND CONDUCTIVE GLASS PASTE CONTAINING GLASS COMPOSITION, AND GLASS-SEALED COMPONENT AND ELECTRIC/ELECTRONIC COMPONENT PREPARED USING THE SAME 有权无铅低熔点玻璃组合物，低温密封玻璃纤维，低温密封玻璃胶，导电材料和导电玻璃包含玻璃组合物，以及使用其制备的玻璃密封组件和电/电子组件公开(公告)号：US20160229737A1
公开(公告)日：2016-08-11
申请号：US14834386
申请日：2015-08-24
发明人： Takashi NAITO , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA , Takuya AOYAGI , Taigo ONODERA , Tatsuya MIYAKE
IPC分类号： C03C8/24 , H05K1/11 , H01L31/0224 , H01L31/0216 , H01L51/52 , C03B23/203 , H01L41/053 , H03H9/19 , H03H9/10 , C03C8/02 , C03C8/08 , C09D5/24 , H05K1/09 , H01B1/14
CPC分类号： C03C8/24 , C03B23/203 , C03C3/122 , C03C3/14 , C03C3/21 , C03C8/02 , C03C8/08 , C03C8/14 , C03C8/16 , C03C8/18 , C09D5/24 , H01B1/14 , H01L31/02168 , H01L31/022425 , H01L31/068 , H01L41/053 , H01L51/5246 , H01L2224/16225 , H01L2924/16152 , H03H3/02 , H03H9/1014 , H03H9/19 , H05K1/092 , H05K2203/1126 , Y02E10/547
摘要： An Ag2O—V2O5—TeO2 lead-free low-melting glass composition that is prevented or restrained from crystallization by heating so as to soften and flow more satisfactorily at a low temperature contains a principal component which includes a vanadium oxide, a tellurium oxide and a silver oxide; a secondary component which includes at least one selected from the group consisting of BaO, WO3 and P2O5; and an additional component which includes at least one selected from the group consisting of oxides of elements in Group 13 of periodic table. A total component of the principal component is 85 mole percent or more in terms of V2O5, TeO2 and Ag2O. Contents of TeO2 and Ag2O each is 1 to 2 times as much as a content of V2O5. A content of the secondary component is 0 to 13 mole percent. A content of the additional component is 0.1 to 3.0 mole percent.
摘要翻译： 通过加热而防止或抑制结晶以便在低温下更令人满意地软化和流动的Ag 2 O-V 2 O 5 -TeO 2无铅低熔点玻璃组合物包含主成分，其包含氧化钒，氧化碲和 氧化银 第二组分，其包括选自BaO，WO 3和P 2 O 5中的至少一种; 和另外的组分，其包括选自元素周期表第13族元素的氧化物中的至少一种。 主成分的总成分以V 2 O 5，TeO 2和Ag 2 O计为85摩尔％以上。 TeO2和Ag2O的含量分别为V2O5含量的1〜2倍。 次要成分的含量为0〜13摩尔％。 附加成分的含量为0.1〜3.0摩尔％。
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3.发明申请公开(公告)号：US20170301883A1
公开(公告)日：2017-10-19
申请号：US15635893
申请日：2017-06-28
发明人： Takashi NAITO , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA , Motomune KODAMA , Masanori MIYAGI , Takuya AOYAGI , Yuichi SAWAI , Tadashi FUJIEDA , Takeshi TSUKAMOTO , Hajime MURAKAMI
IPC分类号： H01L51/52 , H01L51/00 , C09J101/28 , C09J11/04 , C09J101/18 , H01L51/44 , H01G9/20 , C08K3/00
CPC分类号： H01L51/5246 , B32B3/06 , B32B7/14 , B32B17/06 , B32B17/10018 , B32B17/10119 , B32B17/10788 , B32B37/12 , B32B37/18 , B32B38/0008 , B32B38/0036 , B32B38/164 , B32B2038/168 , B32B2250/03 , B32B2255/20 , B32B2255/26 , B32B2307/412 , B32B2457/12 , B32B2457/206 , C08K3/013 , C08K3/22 , C08K2003/2258 , C08K2003/2265 , C08K2201/008 , C09J11/04 , C09J101/18 , C09J101/28 , H01G9/20 , H01G9/2077 , H01L23/295 , H01L51/0034 , H01L51/0096 , H01L51/448 , H01L2924/0002 , H01M14/00 , H05B33/04 , Y02E10/542 , Y02E10/549 , Y10T428/239 , H01L2924/00
摘要： An electronic component has an organic member between two transparent substrates, in which outer peripheral portions of the two transparent substrates are bonded by a sealing material containing low melting glass. The low melting glass contains vanadium oxide, tellurium oxide, iron oxide and phosphoric acid, and satisfies the following relations (1) and (2) in terms of oxides. The sealing material is formed of a sealing material paste which contains the low melting glass, a resin binder and a solvent, the low melting glass containing vanadium oxide, tellurium oxide, iron oxide and phosphoric acid, and satisfies the following relations (1) and (2) in terms of the oxides. Thereby, thermal damages to an organic element or an organic material contained in the electronic component can be reduced and an electronic component having a glass bonding layer of high reliability can be produced efficiently. V2O5+TeO2+Fe2O3+P2O5≧90 (mass %) (1) V2O5>TeO2>Fe2O3>P2O5 (mass %) (2)
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公开(公告)号：US20170253522A1
公开(公告)日：2017-09-07
申请号：US15598674
申请日：2017-05-18
发明人： Takashi NAITO , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA , Takuya AOYAGI , Taigo ONODERA , Tatsuya MIYAKE
CPC分类号： C03C8/24 , C03B23/203 , C03C3/122 , C03C3/14 , C03C3/21 , C03C8/02 , C03C8/08 , C03C8/14 , C03C8/16 , C03C8/18 , C09D5/24 , H01B1/14 , H01L31/02168 , H01L31/022425 , H01L31/068 , H01L41/053 , H01L51/5246 , H01L2224/16225 , H01L2924/16152 , H03H3/02 , H03H9/1014 , H03H9/19 , H05K1/092 , H05K2203/1126 , Y02E10/547
摘要： An Ag2O—V2O5—TeO2 lead-free low-melting glass composition that is prevented or restrained from crystallization by heating so as to soften and flow more satisfactorily at a low temperature contains a principal component which includes a vanadium oxide, a tellurium oxide and a silver oxide; a secondary component which includes at least one selected from the group consisting of BaO, WO3 and P2O5; and an additional component which includes at least one selected from the group consisting of oxides of elements in Group 13 of periodic table. A total component of the principal component is 85 mole percent or more in terms of V2O5, TeO2 and Ag2O. Contents of TeO2 and Ag2O each is 1 to 2 times as much as a content of V2O5. A content of the secondary component is 0 to 13 mole percent. A content of the additional component is 0.1 to 3.0 mole percent.
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5.发明申请HEAT-INSULATING MEMBER, LOW-MELTING GLASS COMPOSITION, AND SEALING MATERIAL PASTE 审中-公开绝热部件，低熔点玻璃组合物和密封材料公开(公告)号：US20160297706A1
公开(公告)日：2016-10-13
申请号：US15036721
申请日：2014-11-28
发明人： Takashi NAITO , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA , Takuya AOYAGI , Motomune KODAMA , Taigo ONODERA , Tadashi FUJIEDA
CPC分类号： C03C8/24 , C03C3/0745 , C03C3/145 , C03C3/16 , C03C3/21 , C03C8/08 , C03C8/20 , C03C8/245 , C03C27/10 , C03C2207/00 , E06B3/6612 , E06B3/66304 , E06B3/6715 , E06B3/6775 , Y02A30/25 , Y02B80/24
摘要： There is disclosed a heat-insulating member including a pair of substrates and an airtight sealing part, in which the airtight sealing part is formed in an outer peripheral part between the pair of substrates to form a space between the pair of substrates, the space being in a vacuum or reduced pressure state, a sealing material that forms the airtight sealing part includes a low-melting glass, and the low-melting glass contains a vanadium oxide, barium oxide, phosphorus oxide, and tungsten oxide, in which the following two relational expressions are satisfied in terms of oxide contents: V2O5+BaO+P2O5+WO3≧90 and V2O5>BaO>P2O5>WO3 (wherein unit: mol %). Thereby, influence on environmental impact can be reduced and maintenance of airtightness and an improvement in acid resistance can be achieved.
摘要翻译： 公开了一种绝热构件，其包括一对基板和气密密封部分，其中气密密封部分形成在该对基板之间的外周部分中，以在一对基板之间形成空间，空间为 在真空或减压状态下，形成气密密封部分的密封材料包括低熔点玻璃，低熔点玻璃含有氧化钒，氧化钡，氧化磷和氧化钨，其中以下两种 关于氧化物含量满足关系式：V2O5 + BaO + P2O5 +WO3≥90，V2O5> BaO> P2O5> WO3（其中单位：mol％）。 从而可以降低对环境影响的影响，并且可以实现气密性的维持和耐酸性的提高。
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公开(公告)号：US20190217574A1
公开(公告)日：2019-07-18
申请号：US16248085
申请日：2019-01-15
发明人： Takashi NAITO , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA , Taigo ONODERA , Tatsuya MIYAKE , Akitoyo KONNO
CPC分类号： B32B7/025 , B23K35/3601 , B32B7/12 , B32B17/10036 , B32B17/10119 , B32B17/10871 , B32B2264/105 , B32B2264/107 , B32B2307/206 , B32B2405/00 , C09J1/00 , C09J2203/326 , C09J2400/14
摘要： There is provided a bonding article comprising: an electrical insulating substrate; a first adhesion layer laminated on one surface of the electrical insulating substrate; and a second adhesion layer laminated on the other surface of the electrical insulating substrate. Both the first adhesion layer and the second adhesion layer include a low-melting-point lead-free glass containing vanadium oxide and tellurium oxide as chemical constituents and having a softening point of 360° C. or lower. And, when contours of the first adhesion layer, the electrical insulating substrate, and the second adhesion layer are projected parallel to one another along the lamination direction, the contour of the first adhesion layer is located inside the contour of the second adhesion layer.
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公开(公告)号：US20170203997A1
公开(公告)日：2017-07-20
申请号：US15408090
申请日：2017-01-17
发明人： Tatsuya MIYAKE , Takashi NAITO , Takuya AOYAGI , Eiichi OGIWARA , Akihito IWAI , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA
CPC分类号： C03C3/21 , B23K35/262 , C03C3/122 , C03C27/06 , C03C27/08 , C22C13/00 , E06B3/6612 , E06B3/66304 , E06B3/67334 , E06B3/6775 , Y02A30/25 , Y02B80/22 , Y02B80/24
摘要： An object of the present invention is to provide a multi-layer glass with high degree of vacuum and high mass productivity. In order to achieve the object, the multi-layer glass according to the present invention includes a first glass substrate, a second glass substrate disposed facing the first glass substrate with a space therebetween, a sealing portion, which contains a glass composition and is disposed in a peripheral edge portion of the space between the first glass substrate and the second glass substrate, and column members disposed between the first glass substrate and the second glass substrate, wherein the column member is made of a metal or alloy, and a melting point of the metal or alloy is higher than a softening point of the glass composition and is lower than or equal to a temperature 20° C. higher than a flow point of the glass composition.
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8.发明申请LEAD-FREE LOW-MELTING GLASS COMPOSITION, LOW-TEMPERATURE SEALING GLASS FRIT, LOW-TEMPERATURE SEALING GLASS PASTE, CONDUCTIVE MATERIAL, AND CONDUCTIVE GLASS PASTE CONTAINING GLASS COMPOSITION, AND GLASS-SEALED COMPONENT AND ELECTRIC/ELECTRONIC COMPONENT PREPARED USING THE SAME 有权无铅低熔点玻璃组合物，低温密封玻璃纤维，低温密封玻璃胶，导电材料和导电玻璃包含玻璃组合物，以及使用其制备的玻璃密封组件和电/电子组件公开(公告)号：US20160060158A1
公开(公告)日：2016-03-03
申请号：US14838786
申请日：2015-08-28
发明人： Takashi NAITO , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA , Taigo ONODERA , Takuya AOYAGI , Tatsuya MIYAKE
摘要： Disclosed is an Ag2O—V2O5—TeO2 lead-free low-melting glass composition that is prevented or restrained from crystallization so as to soften and flow more satisfactorily at a low temperature. This lead-free low-melting glass composition contains a principal component; and an additional component. The principal component includes a vanadium oxide, a tellurium oxide and a silver oxide. The additional component includes at least one selected from the group consisting of yttrium oxide and lanthanoid oxides. A content of the additional component is 0.1 to 3.0 mole percent in terms of oxide. The additional component preferably contains at least one selected from Y2O3, La2O3, CeO2, Er2O3, and Yb2O3 in a content of 0.1 to 2.0 mole percent in terms of oxide. The additional component particularly effectively contains at least one of Y2O3 and La2O3 in a total content of 0.1 to 1.0 mole percent.
摘要翻译： 公开了一种防止或抑制结晶的Ag 2 O-V 2 O 5 -TeO 2无铅低熔点玻璃组合物，以便在低温下更令人满意地软化和流动。 该无铅低熔点玻璃组合物含有主成分; 和一个附加组件。 主要成分包括氧化钒，氧化碲和氧化银。 附加组分包括选自氧化钇和镧系氧化物中的至少一种。 附加成分的含量以氧化物计为0.1〜3.0摩尔％。 另外的成分优选含有以氧化物计为0.1〜2.0摩尔％的Y2O3，La2O3，CeO2，Er2O3，Yb2O3中的至少一种。 另外的组分特别有效地含有总量为0.1至1.0摩尔％的Y 2 O 3和La 2 O 3中的至少一种。
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公开(公告)号：US20200165863A1
公开(公告)日：2020-05-28
申请号：US16695970
申请日：2019-11-26
发明人： Taigo ONODERA , Takashi NAITO , Tatsuya MIYAKE , Takuya AOYAGI , Shinichi TACHIZONO , Yuji HASHIBA , Takahiro IKABATA
摘要： There is provided a gas trapping material and vacuum heat insulation equipment where the gas trapping material can be activated in a sealing step of the vacuum heat insulation equipment, and production efficiency can be enhanced by maintaining a high gas trapping characteristic even when a gas is released in a baking step or in a sealing step under an air atmosphere. The gas trapping material contains porous metal oxide and silver particles having an average particle size of 0.5 nm to 100 nm inclusive.
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公开(公告)号：US20180111218A1
公开(公告)日：2018-04-26
申请号：US15567862
申请日：2016-04-22
发明人： Takashi NAITO , Shinichi TACHIZONO , Kei YOSHIMURA , Yuji HASHIBA , Kiyomi NAKAMURA , Taigo ONODERA , Takuya AOYAGI , Tatsuya MIYAKE
CPC分类号： B23K11/16 , B22F7/064 , B23K1/0004 , B23K11/11 , B23K11/18 , B23K35/0244 , B23K35/262 , B23K35/286 , B23K35/3006 , B23K35/3013 , B23K35/302 , B23K35/3033 , B23K35/36 , B23K35/3601 , B23K35/3602 , B23K35/361 , C22C1/05 , H01B1/023 , H01B1/026 , H01R4/029 , H01R43/0214
摘要： It is an objective of the invention to provide a conductive joint article exhibiting electrical joinability comparable to that of solder joining of easy-to-solder joinable metals even when a joined member of the conductive joint article is made of a hard-to-solder joinable metal. There is provided a conductive joint article with conductive joined members electrically joined via a joining layer, at least one of the joined members being made of a hard-to-solder joinable metal. The joining layer comprises an oxide glass phase and a conductive metal phase. The oxide glass phase includes vanadium as a major constituent and at least one of phosphorus, barium and tungsten as an accessory constituent, and has a glass transition point of 390° C. or less. And, connection resistance between the joined members exhibits less than 1×10−5 Ω/mm2.
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