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    Method of producing a cyclohexenone oxime ether lithium salt, products which can be obtained using this method, the use thereof and corresponding plant protection agents
    26.
    发明授权
    Method of producing a cyclohexenone oxime ether lithium salt, products which can be obtained using this method, the use thereof and corresponding plant protection agents 失效
    制备环己烯酮肟醚锂盐的方法，可以使用该方法得到的产物，其用途和相应的植物保护剂

    公开(公告)号：US06989453B2

    公开(公告)日：2006-01-24

    申请号：US10380107

    申请日：2001-09-12

    申请人： Volker Maywald ,  Reiner Kober ,  Frank Heimann ,  Klaus Oberdorf ,  Albrecht Harreus ,  Norbert Götz ,  Marcus Vossen

    发明人： Volker Maywald ,  Reiner Kober ,  Frank Heimann ,  Klaus Oberdorf ,  Albrecht Harreus ,  Norbert Götz ,  Marcus Vossen

    IPC分类号： C07D335/00

    CPC分类号： C07D335/02

    摘要： A process for preparing 2-{1-[2-(4-chlorophenoxy)propoxyimino]-butyl}-3-hydroxy-5-(tetrahydrothiopyran-3-yl)cyclohex-2-enone lithium salt by reacting the corresponding acid 2-{1-[2-(4-chlorophenoxy)-propoxyimino]butyl}-3-hydroxy-5-(tetrahydrothiopyran-3-yl)-cyclohex-2-enone and lithium hydroxide and the isolation of the lithium salt are described. Here, it is advantageous to use a solvent mixture which comprises methanol and at least one aromatic hydrocarbon and to remove at least some of the solvent prior to the isolation. It is particularly preferred to dissolve the acid in an aromatic hydrocarbon, preferably toluene, and to use a methanolic lithium hydroxide solution.The product, which can be obtained in a more efficient manner by this process, furthermore has considerable advantages with respect to formulation.

    摘要翻译： 通过使相应的酸2-（1-（2-氯苯氧基）丙氧基亚氨基] - 丁基} -3-羟基-5-（四氢噻喃-3-基）环己-2-烯酮锂盐 描述了{1- [2-（4-氯苯氧基） - 丙氧基亚氨基]丁基} -3-羟基-5-（四氢噻喃-3-基） - 环己-2-烯酮和氢氧化锂并分离了锂盐。 这里，使用包含甲醇和至少一种芳烃的溶剂混合物是有利的，并且在分离之前除去至少一些溶剂。 特别优选将酸溶解在芳族烃，优选甲苯中，并使用甲醇氢氧化锂溶液。 通过该方法可以以更有效的方式获得的产品在制剂方面还具有相当大的优点。