Process for preparing organic carboxylic acid
    3.
    发明授权
    Process for preparing organic carboxylic acid 失效
    制备有机羧酸的方法

    公开(公告)号:US5576458A

    公开(公告)日:1996-11-19

    申请号:US407612

    申请日:1995-03-21

    摘要: In the production step, alcohol is reacted with carbon monoxide in a reaction solvent in the presence of a rhodium-containing solid catalyst obtained by immobilizing rhodium in an insoluble carrier (I) containing a pyridine ring in its resin structure and an alkyl iodide containing an alkyl group of 1 to 5 carbon atoms, to produce a reaction product having a water content of 0.5 to 10% by weight; and in the subsequent removing step, an organic carboxylic acid is separated and recovered from the reaction product, and the recovered organic carboxylic acid is contacted with an insoluble carrier (II) containing a pyridine ring in its resin structure, to remove an iodide contained in the organic carboxylic acid.

    摘要翻译: 在制造工序中,使醇与反应溶剂中的一氧化碳反应,在含有固体催化剂的铑固体催化剂的存在下,将铑固定在其树脂结构中含有吡啶环的不溶性载体(I)中, 1〜5个碳原子的烷基,得到含水率为0.5〜10重量%的反应产物; 在随后的除去步骤中,将有机羧酸从反应产物中分离回收,回收的有机羧酸与其树脂结构中含有吡啶环的不溶性载体(II)接触,除去 有机羧酸。

    Supported rhodium catalyst, method of preparing same and process of
producing acetic acid by methanol carbonylation using same
    4.
    发明授权
    Supported rhodium catalyst, method of preparing same and process of producing acetic acid by methanol carbonylation using same 失效
    负载型铑催化剂,其制备方法和使用甲醇羰基化生产乙酸的方法

    公开(公告)号:US5364963A

    公开(公告)日:1994-11-15

    申请号:US169639

    申请日:1993-12-20

    摘要: A methanol carbonylation catalyst includes a rhodium complex supported on a porous, cross-linked vinylpyridine resin, wherein the vinylpyridine resin has a cross-linking degree of 30-60%, a pore volume of 0.1-0.4 ml/g and an average pore diameter of 20-100 nm. The catalyst may be prepared by contacting the pyridine ring-containing resin with an aqueous solution containing rhodium ion and then contacting the resulting rhodium ion-carrying resin with carbon monoxide and an alkyl iodide in an organic solvent to convert the rhodium ion to a rhodium complex bound to the resin. Acetic acid is produced by reacting carbon monoxide with methanol at a temperature of 140.degree.-250.degree. C. and a partial pressure of carbon monoxide of 7-30 kg/cm.sup.2 in the presence of an alkyl iodide and the above catalyst.

    摘要翻译: 甲醇羰基化催化剂包括负载在多孔交联乙烯基吡啶树脂上的铑络合物,其中乙烯基吡啶树脂的交联度为30-60%,孔体积为0.1-0.4ml / g,平均孔径 为20-100nm。 催化剂可以通过使含吡啶环的树脂与含有铑离子的水溶液接触,然后使所得的含铑离子的树脂与一氧化碳和烷基碘在有机溶剂中接触来将铑离子转化成铑络合物 结合树脂。 在烷基碘和上述催化剂的存在下,一氧化碳与甲醇在140〜250℃的温度和一氧化碳分压为7〜30kg / cm 2下反应生成乙酸。

    Solar energy collecting system
    6.
    发明授权
    Solar energy collecting system 失效
    太阳能收集系统

    公开(公告)号:US4285333A

    公开(公告)日:1981-08-25

    申请号:US20583

    申请日:1979-03-14

    摘要: In a solar energy collecting system which comprises a primary closed circuit including a solar energy collector, a heat exchanger, a carrier fluid receiver tank, and a circulating pump and a secondary closed circuit including a utilization means and engaged with the primary closed circuit through the heat exchanger, a heat carrier used in the primary closed circuit is a fluid capable of evaporating at low temperature under low pressure and the control of the primary closed circuit is performed according to a surface temperature of the solar energy collector, a temperature of the carrier emanating from the collector and/or a pressure of the carrier in the primary closed circuit.

    摘要翻译: 在包括太阳能收集器,热交换器,载体流体接收罐和循环泵的主闭路的太阳能收集系统中,以及包括利用装置的二次闭合回路,并通过所述主闭合回路 热交换器中,主闭路中使用的热载体是能够在低压下在低压下蒸发的流体,并且根据太阳能集热器的表面温度,主要闭合回路的控制,载体的温度 从集电器发出和/或在主闭路中的载体的压力。

    Garnet polycrystalline film for magneto-optical recording medium
    8.
    发明授权
    Garnet polycrystalline film for magneto-optical recording medium 失效
    用于磁光记录介质的石榴石多晶膜

    公开(公告)号:US5501913A

    公开(公告)日:1996-03-26

    申请号:US791653

    申请日:1991-11-13

    摘要: A garnet polycrystalline film for a magneto-optical recording medium including at least two layers of polycrystalline garnet represented by Bi.sub.x R.sub.3-x M.sub.Y Fe.sub.5-Y O.sub.12, where 0.ltoreq.X.ltoreq.3, 0 Y.ltoreq.5, R represents one or more rare earth elements containing yttrium, and M represents Ga, Al or In, wherein crystal lattice constants of these adjacent two layers are different from each other by .+-.0.3% or more, and an average crystal grain diameter of one of the layers is smaller than that of the other layer and 1 .mu.m or less, and a magneto-optical recording disk using this garnet polycrystalline film.

    摘要翻译: 一种用于磁光记录介质的石榴石多晶膜,其包括由BixR3-xMYFe5-YO12表示的至少两层多晶石榴石,其中0≤X= 3,0Y = 5,R表示一个或多个 含有钇的稀土元素,M表示Ga,Al或In,其中这些相邻两层的晶格常数彼此不同,为+/- 0.3%以上,其中一层的平均晶粒直径为 小于另一层的1μm以下,以及使用该石榴石多晶膜的磁光记录盘。

    Transfer of flux onto electrodes and production of bumps on electrodes
    10.
    发明授权
    Transfer of flux onto electrodes and production of bumps on electrodes 失效
    将焊剂转移到电极上并在电极上产生凸块

    公开(公告)号:US5899376A

    公开(公告)日:1999-05-04

    申请号:US677392

    申请日:1996-07-09

    IPC分类号: B23K1/20 H05K3/34

    摘要: A process of transferring a flux on electrodes of a semiconductor chip, a film carrier, or a substrate, the process comprising: using a transfer apparatus including a transfer baseplate having protrusions corresponding to said electrodes; dipping the tips of the protrusions of the transfer baseplate in a flux bath to cause the flux to stick to the tips; then aligning the protrusions of the transfer baseplate with the electrodes; and transferring the stuck flux onto the electrodes from the tips.

    摘要翻译: 一种在半导体芯片,薄膜载体或基板的电极上传送磁通的方法,该方法包括:使用包括具有对应于所述电极的突起的转印基板的转印装置; 将转移基板的突起的尖端浸入助熔剂槽中以使焊剂粘附到尖端; 然后将转印基板的突起与电极对准; 并将粘附的助焊剂从尖端转移到电极上。