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    Method of preparing a molecular sieve composition
    41.
    发明授权
    Method of preparing a molecular sieve composition 有权
    制备分子筛组合物的方法

    公开(公告)号：US07829062B2

    公开(公告)日：2010-11-09

    申请号：US11698500

    申请日：2007-01-26

    Applicant: Wenyih Frank Lai ,  Robert Ellis Kay

    Inventor： Wenyih Frank Lai ,  Robert Ellis Kay

    IPC: C01B39/02

    CPC classification number: B01J29/70 ,  B01J29/04 ,  B01J29/06 ,  B01J29/7007 ,  B01J29/7038 ,  B01J29/80 ,  B01J37/0009 ,  B01J37/031 ,  B01J2229/12 ,  B01J2229/20 ,  B01J2229/62 ,  B01J2229/64 ,  C01B39/023 ,  C01B39/04 ,  C01B39/48 ,  C07C2/66 ,  C07C2529/70 ,  C07C2529/80 ,  Y02P20/52 ,  C07C15/085

    Abstract: A method of preparing a crystalline molecular sieve is provided, which method comprises (a) providing a reaction mixture comprising at least one source of ions of tetravalent element Y, at least one source of alkali metal hydroxide, water, optionally at least one seed crystal, and optionally at least one source of ions of trivalent element X, said reaction mixture having the following mole composition: Y:X2 =10 to infinity OH−:Y =0.001 to 2 M+:Y =0.001 to 2 wherein M is an alkali metal and the amount of water is at least sufficient to permit extrusion of said reaction mixture; (b) extruding said reaction mixture to form a pre-formed extrudate; and (c) crystallizing said pre-formed extrudate under vapor phase conditions in a reactor to form said crystalline molecular sieve whereby excess alkali metal hydroxide is removed from the pre-formed extrudate during crystallization. The crystalline molecular sieve product is useful as catalyst in hydrocarbon conversion processes.

    Abstract translation: 提供一种制备结晶分子筛的方法，该方法包括（a）提供包含至少一种四价元素Y的离子源，至少一种碱金属氢氧化物源，水，任选至少一种晶种的离子的反应混合物 和任选的至少一种三价元素X的离子源，所述反应混合物具有以下摩尔组成：Y：X2 = 10至无穷远OH-：Y = 0.001至2M +：Y = 0.001至2其中M为碱 金属和水的量至少足以允许所述反应混合物的挤出; （b）挤出所述反应混合物以形成预成型的挤出物; 和（c）在气相条件下在反应器中使所述预形成的挤出物结晶以形成所述结晶分子筛，从而在结晶期间从预形成的挤出物中除去过量的碱金属氢氧化物。 结晶分子筛产物可用作烃转化过程中的催化剂。

    Process for Preparing Nano Size Zeolites
    42.
    发明申请
    Process for Preparing Nano Size Zeolites 审中-公开
    制备纳米尺寸沸石的方法

    公开(公告)号：US20100260664A1

    公开(公告)日：2010-10-14

    申请号：US12822353

    申请日：2010-06-24

    Applicant: Richard R. Willis ,  Dorothy E. Kuechl ,  Annabelle I. Benin

    Inventor： Richard R. Willis ,  Dorothy E. Kuechl ,  Annabelle I. Benin

    IPC: C01B39/02

    CPC classification number: C01B39/04 ,  C01B39/24

    Abstract: A process has been developed to synthesize various zeolites with nano size crystals. The process involves forming an aluminosilicate initiator which exhibits the Tyndall effect and contains no appreciable filterable solids. This initiator is then mixed with a clear solution comprising reactive sources of Al, Si, M and R plus water. M is an alkali or alkaline earth metal while R is an organoammonium compound. The resultant reaction mixture is reacted at a temperature and for a time sufficient to produce a zeolite such as zeolite Y with average crystallite size less than 500 nm or preferably less than 300 nm.

    Abstract translation: 已经开发了一种合成具有纳米尺寸晶体的各种沸石的方法。 该方法包括形成具有廷德尔效应的硅铝酸盐引发剂，并且不含有明显的可过滤固体。 然后将该引发剂与包含Al，Si，M和R反应水的水的澄清溶液混合。 M是碱金属或碱土金属，而R是有机铵化合物。 所得反应混合物在足以产生平均微晶尺寸小于500nm或优选小于300nm的沸石Y沸石的温度和时间下反应。

    Process for Preparing a Zeolite-Containing Film
    43.
    发明申请
    Process for Preparing a Zeolite-Containing Film 审中-公开
    制备含沸石膜的方法

    公开(公告)号：US20080248328A1

    公开(公告)日：2008-10-09

    申请号：US12060480

    申请日：2008-04-01

    Applicant: Yoshitaka Hamada ,  Masaru Sasago ,  Hideo Nakagawa

    Inventor： Yoshitaka Hamada ,  Masaru Sasago ,  Hideo Nakagawa

    IPC: B32B9/00 ,  B05D3/02 ,  B05D5/12

    CPC classification number: H01L21/31695 ,  C01B33/141 ,  C01B33/145 ,  C01B39/04 ,  C23C18/1212 ,  C23C18/122 ,  C23C18/127 ,  H01L21/02126 ,  H01L21/02203 ,  H01L21/02216 ,  H01L21/02282 ,  H01L21/02337

    Abstract: The invention provides a preparation process of a zeolite-containing film which can raise a zeolite component therein, control the physical properties of the surface, and provide a highly smooth film. The process for preparing a zeolite-containing film has a step of forming a precursor film containing an amorphous silicon oxide portion and a zeolite-like recurring portion by using a material having an amorphous silicon oxide portion and a material having a zeolite-like recurring portion; and a dry gel conversion step of heating the precursor film in the presence of water vapor in order to grow the zeolite-like recurring portion. In this process, the material having an amorphous silicon oxide portion and/or the material having a zeolite-like recurring portion contain(s) a silicon atom bonded to the carbon atom of an organic group containing at least one carbon group.

    Abstract translation: 本发明提供了一种含沸石的膜的制备方法，其可以在其中提高沸石组分，控制表面的物理性能，并提供高度光滑的膜。 制备含沸石的膜的方法具有通过使用具有非晶氧化硅部分的材料和具有沸石状重复部分的材料形成含有非晶氧化硅部分和沸石状重复部分的前体膜的步骤 ; 以及干燥凝胶转化步骤，在水蒸气存在下加热前体膜，以生长沸石状重复部分。 在该方法中，具有无定形氧化硅部分的材料和/或具有沸石状重复部分的材料含有与含有至少一个碳原子的有机基团的碳原子键合的硅原子。

    Zeolite formed product, zeolite laminate intermediate, zeolite laminate composite and method for their preparation
    47.
    发明申请
    Zeolite formed product, zeolite laminate intermediate, zeolite laminate composite and method for their preparation 有权
    沸石成型产品，沸石层压板中间体，沸石层压复合材料及其制备方法

    公开(公告)号：US20070014717A1

    公开(公告)日：2007-01-18

    申请号：US11521008

    申请日：2006-09-14

    Applicant: Toshihiro Tomita ,  Shinji Nakamura

    Inventor： Toshihiro Tomita ,  Shinji Nakamura

    IPC: B01J29/06 ,  C01B39/00

    CPC classification number: C01B39/04 ,  B01D53/228 ,  B01D71/028 ,  B01D2323/12 ,  B01J29/035 ,  B01J29/06 ,  B01J35/065 ,  C01B37/02 ,  Y10S423/22

    Abstract: There are provided methods for producing a zeolite layered composite, methods for producing a zeolite shaped body and methods for producing a zeolite layered intermediate body. In one aspect, there is provided a method for producing a zeolite layered composite, comprising layering a template-containing zeolite membrane having a composition the same as or similar to that of a zeolite shaped body of a completely crystallized zeolite composed of tetrapropylammonium ion (TPA) and silica sol in a mixing ratio (TPA/SiO2) of 0.015 to 0.08 by mole and containing a template therein on the zeolite shaped body, and simultaneously removing the template from the zeolite membrane and the zeolite shaped body by calcining the resulting layered product to obtain a zeolite layered composite comprising the zeolite shaped body and the zeolite membrane layered thereon.

    Abstract translation: 提供沸石层状复合体的制造方法，沸石成形体的制造方法以及沸石层叠体的制造方法。 一方面，提供了一种沸石层状复合体的制造方法，其特征在于，包括具有与四丙基铵离子（TPA）组成的完全结晶沸石的沸石成形体相同或相似的组成的含模板的沸石膜 ）和二氧化硅溶胶，其混合比（TPA / SiO 2/2）为0.015〜0.08摩尔，在沸石成形体上含有模板，同时从沸石膜和沸石中除去模板 通过煅烧所得到的层叠体以获得包含分层的沸石成形体和沸石膜的沸石层状复合体。

    Process for preparing a nanosized zeolitic material
    48.
    发明申请
    Process for preparing a nanosized zeolitic material 有权
    制备纳米沸石材料的方法

    公开(公告)号：US20060239906A1

    公开(公告)日：2006-10-26

    申请号：US11111871

    申请日：2005-04-22

    Applicant: Ulrich Mueller ,  Lian Ma ,  Xiao Feng-Shou ,  Xiaoyu Yang

    Inventor： Ulrich Mueller ,  Lian Ma ,  Xiao Feng-Shou ,  Xiaoyu Yang

    IPC: C01B39/04 ,  C01B33/36

    CPC classification number: C01B37/005 ,  C01B39/04 ,  C01B39/40 ,  C01B39/48 ,  Y10S423/22 ,  Y10S423/27

    Abstract: A process for preparing a zeolitic material, comprising (i) preparing a mixture comprising the at least one silicon containing precursor compound from which the zeolitic framework is formed, at least one pore forming agent, and at least one polymer which has an essentially spheroidal geometry in the mixture; (ii) crystallizing the zeolitic material from the mixture obtained in (i) to obtain the crystallized zeolitic material in its mother liquor.

    Abstract translation: 一种制备沸石材料的方法，包括（i）制备包含所述至少一种含硅的前体化合物的混合物，所述至少一种含有硅沸石骨架的前体化合物由其形成，至少一种成孔剂和至少一种具有基本上球形几何形状的聚合物 在混合物中 （ii）从（i）中获得的混合物中结晶沸石材料，得到其母液中的结晶沸石材料。

    Method of preventing crystalline intergrowth during the preparation of a crystalline material
    50.
    发明申请
    Method of preventing crystalline intergrowth during the preparation of a crystalline material 审中-公开
    在制备结晶材料期间防止结晶共生的方法

    公开(公告)号：US20050135998A1

    公开(公告)日：2005-06-23

    申请号：US10745747

    申请日：2003-12-23

    Applicant: Allen Burton ,  Stacey Zones

    Inventor： Allen Burton ,  Stacey Zones

    IPC: C01B37/00 ,  C01B39/04 ,  C01B39/48

    CPC classification number: C01B39/04 ,  C01B37/00 ,  C01B39/48

    Abstract: The present invention relates to a method of preventing the intergrowth of an undesired porous crystalline phase during the preparation of a desired porous crystalline material comprising (1) an oxide of a first tetravalent element to (2) an oxide of a trivalent element, pentavalent element, second tetravalent element different from said first tetravalent element or mixture thereof, the method comprising contacting under crystallization conditions sources of said oxides, a structure directing agent capable of forming the desired porous crystalline material, and an amine too large to fit in the pores of the undesired porous crystalline phase.

    Abstract translation: 本发明涉及一种在制备期望的多孔结晶材料期间防止不想要的多孔结晶相共生的方法，包括（1）第一四价元素的氧化物，（2）三价元素的氧化物，五价元素 不同于所述第一四价元素或其混合物的第二四价元素，所述方法包括在结晶条件下接触所述氧化物源，能够形成所需多孔结晶材料的结构导向剂，以及太大以适合于 不需要的多孔结晶相。

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