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    Parallel liquid chromatography for analyzing combinatorial libraries of non-biological polymers
    21.
    发明授权
    Parallel liquid chromatography for analyzing combinatorial libraries of non-biological polymers 有权
    用于分析非生物聚合物组合文库的平行液相色谱

    公开(公告)号：US06461515B1

    公开(公告)日：2002-10-08

    申请号：US09728729

    申请日：2000-11-28

    申请人： Adam Safir ,  Miroslav Petro ,  Ralph B. Nielsen

    发明人： Adam Safir ,  Miroslav Petro ,  Ralph B. Nielsen

    IPC分类号： B01D1508

    CPC分类号： G01N35/1097 ,  B01D15/08 ,  B01D15/14 ,  B01D15/1871 ,  B01D15/1885 ,  B01J19/0046 ,  B01J19/26 ,  B01J2219/00274 ,  B01J2219/00585 ,  B01J2219/00587 ,  B01J2219/00707 ,  B01J2219/00722 ,  C40B40/14 ,  G01N15/0205 ,  G01N30/02 ,  G01N30/16 ,  G01N30/24 ,  G01N30/30 ,  G01N30/461 ,  G01N30/466 ,  G01N30/54 ,  G01N30/6052 ,  G01N30/88 ,  G01N33/44 ,  G01N35/085 ,  G01N2015/0288 ,  G01N2015/0294 ,  G01N2030/324 ,  Y10T436/25 ,  B01D15/34

    摘要： A method is disclosed for characterizing non-biological polymers using liquid chromatography that is particularly useful in polymer research programs. The method includes the steps of providing a library of four or more non-biological polymer samples, with each of the four or more polymer samples being polymerization product mixtures that result from polymerization reactions that are varied with respect to a factor affecting polymerization. Each of the four or more polymer samples resides in the reaction vessel in which they were formed. The method further includes sampling first and second polymer samples from the reaction vessels in which they were formed, supplying a mobile phase in parallel through each of a first chromatographic column and a second chromatographic column of a liquid chromatography system, injecting the first and second polymer samples into the mobile phase of the first and second chromatographic columns, respectively, simultaneously separating at least one sample component of the injected first and second samples from other sample components thereof in the respective chromatographic columns, and detecting a property of at least one of the separated sample components of each of the first and second samples.

    摘要翻译： 公开了一种用于表征非生物聚合物的方法，该方法在聚合物研究程序中特别有用。 该方法包括以下步骤：提供四种或更多种非生物聚合物样品的文库，其中四种或更多种聚合物样品中的每一种都是由相对于影响聚合的因素而变化的聚合反应产生的聚合产物混合物。 四个或更多个聚合物样品中的每一个驻留在形成它们的反应容器中。 该方法还包括从其形成的反应容器中取样第一和第二聚合物样品，通过液相色谱系统的第一色谱柱和第二色谱柱中的每一个并行供应流动相，将第一和第二聚合物 样品分别进入第一和第二色谱柱的流动相，同时将注入的第一和第二样品的至少一个样品组分与其它样品组分在各色谱柱中分离，并检测至少一种 分离出第一和第二样品的样品成分。