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    Method for preparing a supported ruthenium catalyst
    101.
    发明授权
    Method for preparing a supported ruthenium catalyst 有权
    负载型钌催化剂的制备方法

    公开(公告)号：US09499402B2

    公开(公告)日：2016-11-22

    申请号：US14118301

    申请日：2012-05-15

    申请人： Debasish Chakraborty

    发明人： Debasish Chakraborty

    IPC分类号： C01B3/08 ,  H01M8/06 ,  B01J21/04 ,  B01J23/46 ,  B01J23/58 ,  B01J23/63 ,  B01J23/644 ,  B01J35/00 ,  B01J35/10 ,  B01J37/02 ,  B01J37/08 ,  C01B3/04

    CPC分类号： C01B3/08 ,  B01J21/04 ,  B01J23/46 ,  B01J23/462 ,  B01J23/58 ,  B01J23/63 ,  B01J23/644 ,  B01J23/6447 ,  B01J35/00 ,  B01J35/0013 ,  B01J35/002 ,  B01J35/10 ,  B01J35/1009 ,  B01J35/1014 ,  B01J35/1019 ,  B01J35/1038 ,  B01J35/1042 ,  B01J37/02 ,  B01J37/0203 ,  B01J37/0211 ,  B01J37/0221 ,  B01J37/08 ,  C01B3/047 ,  H01M8/0606 ,  Y02E60/324 ,  Y02E60/364 ,  Y02E60/50

    摘要： In a method of preparing a ruthenium-containing catalyst on a non-conductive metal oxide support comprises dissolving one or more ruthenium precursor compounds in an liquid organic polyol, combining the thus obtained solution with (a) nano-powder(s) of one or more metal oxides in a ratio of moles metal oxide(s) to moles ruthenium atoms in the one or more ruthenium precursor compounds of about 0:1 to about 6:1, the metal oxide nano-powder(s) having a surface area of from about 5 to about 300 m2/g and a point of zero charge (PZC) of pH 5.5 or higher, agitating the thus obtained mixture, adding pre-shaped alumina support pellets to the agitated mixture, which is than heated at a temperature of about 50° C. to the boiling point of the organic polyol, until the reaction is finished, cooling the mixture and combining it with an aqueous solution of NaNO3 and/or KNO3, agitating the resultant mixture, separating the solvent and the solids, and drying the thus obtained solid pellets of alumina, or alumina and the metal oxide(s) of the nano-powder(s) coated with ruthenium and an additional amount Na and/or K ions. Also disclosed is the supported ruthenium-containing catalyst obtainable by the method and the use thereof in decomposing ammonia into nitrogen and oxygen.

    摘要翻译： 在非导电性金属氧化物载体上制备含钌催化剂的方法包括将一种或多种钌前体化合物溶解在液体有机多元醇中，将由此获得的溶液与（a）一种或多种纳米粉末组合， 一种或多种钌前体化合物中的金属氧化物与一种或多种钌前体化合物中钌原子摩尔数的摩尔比为大约0:1至大约6:1的金属氧化物，所述金属氧化物纳米粉末的表面积为 约5至约300m 2 / g和pH 5.5或更高的零电荷点（PZC），搅拌由此获得的混合物，将预形状的氧化铝载体颗粒加入到搅拌的混合物中，该混合物在温度为 约50℃至有机多元醇的沸点，直到反应完成，冷却混合物并将其与NaNO 3和/或KNO 3的水溶液混合，搅拌所得混合物，分离溶剂和固体，和 干燥由此获得的氧化铝固体颗粒， 或氧化铝和涂覆有钌的纳米粉末和额外量的Na和/或K离子的金属氧化物。 还公开了通过该方法获得的负载的含钌催化剂及其在将氨分解成氮和氧的用途。

    Catalyst for oxygenate synthesis and method for manufacturing same, device for manufacturing oxygenate, and method for manufacturing oxygenate
    103.
    发明授权
    Catalyst for oxygenate synthesis and method for manufacturing same, device for manufacturing oxygenate, and method for manufacturing oxygenate 有权
    含氧化合物合成催化剂及其制造方法，含氧化合物的制造装置以及含氧化合物的制造方法

    公开(公告)号：US09272267B2

    公开(公告)日：2016-03-01

    申请号：US14237427

    申请日：2012-08-22

    申请人： Toshihito Miyama

    发明人： Toshihito Miyama

    IPC分类号： B01J31/00 ,  B01J23/00 ,  B01J23/656 ,  C07C29/158 ,  C07C45/49 ,  B01J37/02 ,  B01J21/14

    CPC分类号： B01J23/6562 ,  B01J21/14 ,  B01J37/02 ,  B01J37/0207 ,  B01J37/0242 ,  C07C29/158 ,  C07C45/49 ,  Y02E50/18 ,  Y02P20/52 ,  C07C31/08 ,  C07C47/06

    摘要： The present invention relates to a catalyst for oxygenate synthesis for synthesizing an oxygenate from a mixed gas containing hydrogen and carbon monoxide, the catalyst for oxygenate synthesis containing: a component (A): rhodium, a component (B): manganese, a component (C): an alkali metal, and a component (D): a component (D1), component (D2) or component (D3), wherein the component (D1) is one or more substances selected from the group consisting of titanium, vanadium and chromium, the component (D2) is an element belonging to group 13 of the periodic table, and the component (D3) is one or more substances selected from the group consisting of magnesium and lanthanoids. According to the present invention, an oxygenate can be synthesized efficiently from a mixed gas containing hydrogen and carbon monoxide.

    摘要翻译： 本发明涉及一种用于从含氢和一氧化碳的混合气体中合成含氧化合物的含氧化合物催化剂，含氧合成催化剂含有：组分（A）：铑，组分（B）：锰，组分（ C）：碱金属和组分（D）：组分（D1），组分（D2）或组分（D3），其中组分（D1）是一种或多种选自钛，钒 和组分（D2）是属于周期表第13族的元素，组分（D3）是一种或多种选自镁和镧系元素的物质。 根据本发明，可以从含有氢和一氧化碳的混合气体中有效地合成含氧化合物。

    Method for producing hydrorefining catalyst
    109.
    发明授权
    Method for producing hydrorefining catalyst 有权
    加氢精制催化剂的制造方法

    公开(公告)号：US07427578B2

    公开(公告)日：2008-09-23

    申请号：US10525841

    申请日：2003-08-29

    申请人： Yoshiki Iwata

    发明人： Yoshiki Iwata

    IPC分类号： B01J27/00 ,  B01J27/188 ,  B01J27/19

    CPC分类号： C10G45/08 ,  B01J23/88 ,  B01J23/882 ,  B01J23/883 ,  B01J27/1853 ,  B01J27/19 ,  B01J35/002 ,  B01J35/1014 ,  B01J35/1019 ,  B01J35/1038 ,  B01J35/1061 ,  B01J37/02

    摘要： A method for producing a hydrorefining catalyst includes the step of preparing a carrying solution containing molybdenum, phosphorus, and cobalt or nickel and bringing a carrier composed of an inorganic porous oxide into contact with the carrying solution. A molar ratio of molybdenum with respect to phosphorus in the carrying solution is 2.5 to 7.0, a molar ratio of a total of molybdenum, cobalt, and nickel with respect to phosphorus is 3.5 to 9.0, and a molar ratio of molybdenum with respect to a total of cobalt and nickel is 1.9 to 2.8. pH of the carrying solution is 2 to 5, and a Raman spectroscopy spectrum of the carrying solution has a peak top between 965 cm−1 and 975 cm−1. The catalyst obtained by this method is excellent in desulfurizing activity.

    摘要翻译： 制备加氢精制催化剂的方法包括制备含有钼，磷和钴或镍的载体溶液并使由无机多孔氧化物构成的载体与载体溶液接触的步骤。 在载体溶液中，钼相对于磷的摩尔比为2.5〜7.0，相对于磷，钼，钴和镍的总摩尔比为3.5〜9.0，钼相对于 钴和镍的总量为1.9至2.8。 载体溶液的pH为2至5，载体溶液的拉曼光谱谱具有在965cm -1至975cm -1之间的峰顶。 通过该方法获得的催化剂具有优异的脱硫活性。