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11.
公开(公告)号:US09006651B2
公开(公告)日:2015-04-14
申请号:US14029368
申请日:2013-09-17
Applicant: FEI Company
Inventor: Jeffrey Blackwood , Stacey Stone
CPC classification number: G01N1/28 , G01N1/06 , G01N1/08 , G01N1/32 , G01N23/04 , H01J37/06 , H01J37/18 , H01J37/20 , H01J37/26 , H01J37/28 , H01J37/3056 , H01J2237/063 , H01J2237/182 , H01J2237/204 , H01J2237/208 , H01J2237/2802 , H01J2237/31745 , H01J2237/31749
Abstract: An improved method and apparatus for S/TEM sample preparation and analysis. Preferred embodiments of the present invention provide improved methods for TEM sample creation, especially for small geometry (
Abstract translation: 一种用于S / TEM样品制备和分析的改进方法和装置。 本发明的优选实施例提供用于TEM样品制备的改进方法,特别是对于小几何(<100nm厚)TEM薄片。 新颖的样品结构和铣削图案的新颖应用允许产生薄至50nm的S / TEM样品,而没有显着的弯曲或翘曲。 本发明的优选实施方案提供了部分或全部自动化TEM样品制备的方法,使TEM样品的创建和分析过程减少劳动密集度,并提高TEM分析的产量和再现性。
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公开(公告)号:US20180301319A1
公开(公告)日:2018-10-18
申请号:US16012888
申请日:2018-06-20
Applicant: FEI Company
Inventor: Stacey Stone , Sang Hoon Lee , Jeffrey Blackwood , Michael Schmidt , Hyun Hwa Kim
IPC: H01J37/317 , H01J37/305
Abstract: A method for analyzing a sample with a charged particle beam including directing the beam toward the sample surface; milling the surface to expose a second surface in the sample in which the end of the second surface distal to ion source is milled to a greater depth relative to a reference depth than the end of the first surface proximal to ion source; directing the charged particle beam toward the second surface to form one or more images of the second surface; forming images of the cross sections of the multiple adjacent features of interest by detecting the interaction of the electron beam with the second surface; assembling the images of the cross section into a three-dimensional model of one or more of the features of interest. A method for forming an improved fiducial and determining the depth of an exposed feature in a nanoscale three-dimensional structure is presented.
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公开(公告)号:US10026590B2
公开(公告)日:2018-07-17
申请号:US14758466
申请日:2013-12-30
Applicant: FEI Company
Inventor: Stacey Stone , Sang Hoon Lee , Jeffrey Blackwood , Michael Schmidt , Hyun Hwa Kim
IPC: H01J37/317 , H01J37/305
Abstract: A method for analyzing a sample with a charged particle beam including directing the beam toward the sample surface; milling the surface to expose a second surface in the sample in which the end of the second surface distal to ion source is milled to a greater depth relative to a reference depth than the end of the first surface proximal to ion source; directing the charged particle beam toward the second surface to form one or more images of the second surface; forming images of the cross sections of the multiple adjacent features of interest by detecting the interaction of the electron beam with the second surface; assembling the images of the cross section into a three-dimensional model of one or more of the features of interest. A method for forming an improved fiducial and determining the depth of an exposed feature in a nanoscale three-dimensional structure is presented.
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公开(公告)号:US09696372B2
公开(公告)日:2017-07-04
申请号:US14432712
申请日:2013-10-04
Applicant: FEI Company
Inventor: Jeffrey Blackwood , Sang Hoon Lee , Michael Schmidt , Stacey Stone , Karey Holland
IPC: G01R31/305 , G01R31/265 , G01N1/28 , H01L21/66 , G01N1/32 , H01J37/30 , H01J37/153 , G01R31/307 , G01R31/28 , G01R31/312
CPC classification number: G01R31/2653 , G01N1/286 , G01N1/32 , G01R31/2808 , G01R31/2898 , G01R31/307 , G01R31/312 , H01J37/153 , H01J37/3005 , H01J2237/208 , H01J2237/24564 , H01J2237/2817 , H01J2237/31749 , H01L22/14 , H01L2924/0002 , H01L2924/00
Abstract: Multiple planes within the sample are exposed from a single perspective for contact by an electrical probe. The sample can be milled at a non-orthogonal angle to expose different layers as sloped surfaces. The sloped edges of multiple, parallel conductor planes provide access to the multiple levels from above. The planes can be accessed, for example, for contacting with an electrical probe for applying or sensing a voltage. The level of an exposed layer to be contacted can be identified, for example, by counting down the exposed layers from the sample surface, since the non-orthogonal mill makes all layers visible from above. Alternatively, the sample can be milled orthogonally to the surface, and then tilted and/or rotated to provide access to multiple levels of the device. The milling is preferably performed away from the region of interest, to provide electrical access to the region while minimizing damage to the region.
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公开(公告)号:US20150330877A1
公开(公告)日:2015-11-19
申请号:US14758150
申请日:2013-12-30
Applicant: FEI COMPANY
Inventor: Michael Schmidt , Jeffrey Blackwood , Stacey Stone , Sang Hoon Lee , Ronald Kelley , Trevan Landin
IPC: G01N1/32 , H01L21/3065
CPC classification number: G01N1/32 , G01N1/28 , H01L21/30655
Abstract: A method and apparatus is provided for preparing samples for observation in a charged particle beam system in a manner that reduces or prevents artifacts. An ion beam mills exposes a cross section of the work piece using a bulk mill process. A deposition precursor gas is directed to the sample surface while a small amount of material is removed from the exposed cross section face, the deposition precursor producing a more uniform cross section. Embodiments are useful for preparing cross sections for SEM observation of samples having layers of materials of different hardnesses. Embodiments are useful for preparation of thin TEM samples.
Abstract translation: 提供了一种方法和装置,用于以减少或防止伪影的方式制备用于在带电粒子束系统中观察的样品。 离子束研磨机使用大量研磨工艺暴露工件的横截面。 沉积前体气体被引导到样品表面,同时少量的材料从暴露的横截面去除,沉积前体产生更均匀的横截面。 实施例对于制备具有不同硬度的材料层的样品的SEM观察的截面是有用的。 实施例可用于制备薄TEM样品。
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公开(公告)号:US09111720B2
公开(公告)日:2015-08-18
申请号:US14572626
申请日:2014-12-16
Applicant: FEI Company
Inventor: Ronald Kelley , Michael Moriarty , Stacey Stone , Jeffrey Blackwood
IPC: G01N23/00 , H01J37/305 , C23C14/30
CPC classification number: H01J37/3053 , B05D3/044 , C23C14/30 , G01N1/286 , G01N1/32 , G01N2001/2886 , H01J37/265 , H01J37/3056 , H01J2237/31745 , H01J2237/3348 , H01L21/02318
Abstract: A method and apparatus is provided for preparing samples for observation in a charged particle beam system in a manner that reduces or prevents artifacts. Material is deposited onto the sample using charged particle beam deposition just before or during the final milling, which results in an artifact-free surface. Embodiments are useful for preparing cross sections for SEM observation of samples having layers of materials of different hardnesses. Embodiments are useful for preparation of thin TEM samples.
Abstract translation: 提供了一种方法和装置,用于以减少或防止伪影的方式制备用于在带电粒子束系统中观察的样品。 在最终研磨之前或期间,使用带电粒子束沉积将材料沉积到样品上,这导致无伪影的表面。 实施例对于制备具有不同硬度的材料层的样品的SEM观察的截面是有用的。 实施例可用于制备薄TEM样品。
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公开(公告)号:US08912490B2
公开(公告)日:2014-12-16
申请号:US14081947
申请日:2013-11-15
Applicant: FEI Company
Inventor: Ronald Kelley , Michael Moriarty , Stacey Stone , Jeffrey Blackwood
IPC: G01N23/00 , B05D3/04 , H01J37/305 , H01L21/02 , G01N1/28
CPC classification number: H01J37/3053 , B05D3/044 , C23C14/30 , G01N1/286 , G01N1/32 , G01N2001/2886 , H01J37/265 , H01J37/3056 , H01J2237/31745 , H01J2237/3348 , H01L21/02318
Abstract: A method and apparatus is provided for preparing samples for observation in a charged particle beam system in a manner that reduces or prevents artifacts. Material is deposited onto the sample using charged particle beam deposition just before or during the final milling, which results in an artifact-free surface. Embodiments are useful for preparing cross sections for SEM observation of samples having layers of materials of different hardnesses. Embodiments are useful for preparation of thin TEM samples.
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公开(公告)号:US10546719B2
公开(公告)日:2020-01-28
申请号:US15987847
申请日:2018-05-23
Applicant: FEI Company
Inventor: Noel Thomas Franco , Kenny Mani , Chad Rue , Joe Christian , Jeffrey Blackwood
IPC: H01J37/305 , H01L21/67 , H01L21/263 , H01L21/3065 , H01J37/22 , G01N1/44 , G01N1/28
Abstract: Method for preparing site-specific, plan-view lamellae from multilayered microelectronic devices. A focused ion beam that is directed, with an etch-assisting gas, toward an uppermost layer of a device removes at least that uppermost layer and thereby exposes an underlying layer over, or comprising, a target area from which the site-specific, plan-view lamella is to be prepared, wherein the focused ion beam is in a face-on orientation in removing the uppermost layer to expose the underlying layer. In a preferred embodiment, the etch-assisting gas comprises methyl nitroacetate. In alternative embodiments, the etch-assisting gas is methyl acetate, ethyl acetate, ethyl nitroacetate, propyl acetate, propyl nitroacetate, nitro ethyl acetate, methyl methoxyacetate, or methoxy acetylchloride.
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公开(公告)号:US09601313B2
公开(公告)日:2017-03-21
申请号:US14934837
申请日:2015-11-06
Applicant: FEI Company
Inventor: Valerie Brogden , Jeffrey Blackwood , Michael Schmidt , Dhruti Trivedi , Richard J. Young , Thomas G. Miller , Brian Roberts Routh, Jr. , Stacey Stone , Todd Templeton
IPC: H01J37/26 , H01J37/302 , H01J37/285 , H01J37/28 , H01J37/31
CPC classification number: H01J37/3023 , G01N1/286 , G01N2001/2873 , H01J37/28 , H01J37/285 , H01J37/3045 , H01J37/31 , H01J2237/208 , H01J2237/31745
Abstract: Techniques are described that facilitate automated extraction of lamellae and attaching the lamellae to sample grids for viewing on transmission electron microscopes. Some embodiments of the invention involve the use of machine vision to determine the positions of the lamella, the probe, and/or the TEM grid to guide the attachment of the probe to the lamella and the attachment of the lamella to the TEM grid. Techniques that facilitate the use of machine vision include shaping a probe tip so that its position can be readily recognized by image recognition software. Image subtraction techniques can be used to determine the position of the lamellae attached to the probe for moving the lamella to the TEM grid for attachment. In some embodiments, reference structures are milled on the probe or on the lamella to facilitate image recognition.
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公开(公告)号:US09412560B2
公开(公告)日:2016-08-09
申请号:US14432730
申请日:2013-10-07
Applicant: FEI Company
Inventor: Stacey Stone , Sang Hoon Lee , Jeffrey Blackwood , Michael Schmidt
IPC: H01J37/31 , G01N1/32 , H01J37/30 , G01N23/225 , H01J37/305
CPC classification number: H01J37/3005 , G01N1/32 , G01N23/2255 , G01N2223/104 , G01N2223/611 , H01J37/3007 , H01J37/3053 , H01J37/3056 , H01J37/31 , H01J2237/063 , H01J2237/08 , H01J2237/2813 , H01J2237/31732 , H01J2237/31745 , H01J2237/31749
Abstract: To reduce artifacts in a surface exposed by a focused ion beam for viewing, a trench is milled next to the region of interest, and the trench is filled to create a bulkhead. The ion beam is directed through the bulkhead to expose a portion of the region of interest for viewing. The trench is filled, for example, by charged particle beam-induced deposition. The trench is typically milled and filled from the top down, and then the ion beam is angled with respect to the sample surface to expose the region of interest.
Abstract translation: 为了减少由聚焦离子束暴露的表面中的人造物进行观察,在感兴趣区域旁边研磨沟槽,并且填充沟槽以形成隔板。 离子束被引导通过隔板以暴露感兴趣区域的一部分以供观察。 例如,通过带电粒子束诱导沉积来填充沟槽。 沟槽通常从顶部向下铣削和填充,然后离子束相对于样品表面成角度以暴露感兴趣区域。
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