Solder/polymer composite paste and method
    1.
    发明授权
    Solder/polymer composite paste and method 失效
    焊剂/聚合物复合材料和方法

    公开(公告)号:US5062896A

    公开(公告)日:1991-11-05

    申请号:US502090

    申请日:1990-03-30

    摘要: An improved solder/polymer fluxless composite paste interconnection material having a low reflow temperature to form electrical contacts having good bonding strength and low contact resistance. The present pastes comprise a major proportion of a meltable metal alloy powder filler, free of noble metals and preferably free of lead, a minor proportion of a solution of a temperature-stable thermoplastic polymer having a softening temperature above the melting temperature of the metal powder filler in a volatile solvent which evaporates during reflow, and a minor proportion of a fluxing agent having a boiling point lower than the reflow temperature of the composition and higher than the melting point of the eutectic alloy powder filler. An oxide-free, partially coalesced metal alloy connection is obtained, which is polymer strengthened and reworkable at a low reflow temperature, per se, or in the presence of polymer solvent.

    摘要翻译: 具有低回流温度的改进的焊料/聚合物无焊剂复合糊剂互连材料,以形成具有良好的接合强度和低接触电阻的电触点。 本发明的糊料主要包括不含贵金属,优选不含铅的可熔融金属合金粉末填料的主要部分,较小比例的软化温度高于金属粉末的熔融温度的温度稳定的热塑性聚合物溶液 在回流时蒸发的挥发性溶剂中的填料,以及沸点低于组合物的回流温度并且高于共晶合金粉末填料的熔点的助熔剂的一小部分。 获得无氧化物,部分聚结的金属合金连接,其在低回流温度下或在聚合物溶剂的存在下聚合物增强并可再加工。

    DIRECT DETECTION OF LOCALIZED MODULATION OF ION CONCENTRATION ON AN ELECTRODE-ELECTROLYTE INTERFACE
    2.
    发明申请
    DIRECT DETECTION OF LOCALIZED MODULATION OF ION CONCENTRATION ON AN ELECTRODE-ELECTROLYTE INTERFACE 有权
    直接检测离子浓度在电极电解质界面上的局部化调节

    公开(公告)号:US20090316157A1

    公开(公告)日:2009-12-24

    申请号:US12131647

    申请日:2008-06-02

    IPC分类号: G01B9/02 C25B9/00

    CPC分类号: G01N21/45 C25D21/12 G01N21/21

    摘要: The present invention directly measures localized electrochemical processes on a planar electrode using differential interferometry. The ionic charge accumulation at the electrode-electrolyte interface may be directly measured by using differential interferometry as a function of magnitude and frequency (for example, 2-50 kHz) of an external potential applied on an electrode. Methods in accordance with the present invention probe the ion dynamics confined to the electrical double layer. An electric field is applied using a pure AC potential and a superposition of AC and DC-ramp potential to measure ion concentration and detect redox processes.

    摘要翻译: 本发明使用差分干涉法直接测量平面电极上的局部电化学过程。 可以通过使用差分干涉测量作为施加在电极上的外部电位的幅度和频率(例如2-50kHz)的函数来直接测量电极 - 电解质界面处的离子电荷累积。 根据本发明的方法探测限于电双层的离子动力学。 使用纯AC电位和AC和DC-ramp电位的叠加来施加电场以测量离子浓度并检测氧化还原过程。

    Micro goniometer for scanning probe microscopy
    4.
    发明授权
    Micro goniometer for scanning probe microscopy 失效
    用于扫描探针显微镜的微测角仪

    公开(公告)号:US06552339B1

    公开(公告)日:2003-04-22

    申请号:US09572209

    申请日:2000-05-17

    IPC分类号: G01N2300

    摘要: A goniometer for performing scanning probe microscopy on a substrate surface is disclosed. The goniometer has a cantilever, having a cantilevered end and a supported end and a tip disposed at the cantilevered end of the cantilever. The goniometer also has a block disposed at the supported end of the cantilever. The block has at least one pair of piezoelectric layers, a pair of electrodes disposed about each individual piezoelectric layer such that varying a potential difference applied between the individual electrodes of a pair of electrodes causes the corresponding piezoelectric layer to deform, and a first insulating material disposed between the individual electrodes for insulating the individual electrodes from each other. The individual piezoelectric layers are deformed at different rates resulting in a deformity of the block and tilting of the cantilever and tip connected therewith. Also disclosed are methods of using the goniometer of the present invention to measure the interactive forces between two molecular structures using a scanning probe microscope equipped with a goniometer of the present invention.

    摘要翻译: 公开了一种用于在衬底表面上执行扫描探针显微镜的测角器。 测角器具有悬臂,具有悬臂端和支撑端,以及设置在悬臂悬臂端的尖端。 测角器还具有设置在悬臂的支撑端处的块。 该块具有至少一对压电层,围绕每个单独的压电层设置的一对电极,使得改变施加在一对电极的各个电极之间的电势差导致相应的压电层变形,并且第一绝缘材料 设置在各个电极之间,用于使各个电极彼此绝缘。 单个压电层以不同的速率变形,导致块的变形和与其连接的悬臂和尖端的倾斜。 还公开了使用本发明的测角器的方法,使用配备有本发明的测角器的扫描探针显微镜来测量两个分子结构之间的相互作用力。

    Micro goniometer for scanning microscopy
    5.
    发明授权
    Micro goniometer for scanning microscopy 失效
    用于扫描显微镜的微测角仪

    公开(公告)号:US6100523A

    公开(公告)日:2000-08-08

    申请号:US960692

    申请日:1997-10-29

    摘要: A goniometer for performing scanning probe microscopy on a substrate surface is disclosed. The goniometer has a cantilever, having a cantilevered end and a supported end and a tip disposed at the cantilevered end of the cantilever. The goniometer also has a block disposed at the supported end of the cantilever. The block has at least one pair of piezoelectric layers, a pair of electrodes disposed about each individual piezoelectric layer such that varying a potential difference applied between the individual electrodes of a pair of electrodes causes the corresponding piezoelectric layer to deform, and a first insulating material disposed between the individual electrodes for insulating the individual electrodes from each other. The individual piezoelectric layers are deformed at different rates resulting in a deformity of the block and tilting of the cantilever and tip connected therewith. Also disclosed are methods of using the goniometer of the present invention to measure the interactive forces between two molecular structures using a scanning probe microscope equipped with a goniometer of the present invention.

    摘要翻译: 公开了一种用于在衬底表面上执行扫描探针显微镜的测角器。 测角器具有悬臂,具有悬臂端和支撑端,以及设置在悬臂悬臂端的尖端。 测角器还具有设置在悬臂的支撑端处的块。 该块具有至少一对压电层,围绕每个单独的压电层设置的一对电极,使得改变施加在一对电极的各个电极之间的电势差导致相应的压电层变形,并且第一绝缘材料 设置在各个电极之间,用于使各个电极彼此绝缘。 单个压电层以不同的速率变形,导致块的变形和与其连接的悬臂和尖端的倾斜。 还公开了使用本发明的测角器的方法,使用配备有本发明的测角器的扫描探针显微镜来测量两个分子结构之间的相互作用力。

    Morphological composite materials formed from different precursors
    7.
    发明授权
    Morphological composite materials formed from different precursors 失效
    形态复合材料由不同的前体形成

    公开(公告)号:US5288842A

    公开(公告)日:1994-02-22

    申请号:US647957

    申请日:1991-01-30

    摘要: A method of producing a multiphase polymer is disclosed whereby the phases have the same chemical structure but have different morphological states and thus different properties. This is achieved by forming a mixture of precursors of the polymer, at least one of the precursors having a reaction rate higher than the other precursor or precursors in the mixture. The precursor having the highest reaction rate is then converted to obtain a composite of a polymer and the precursors that are not polymerized. This mixture might also be formed by mixing a soluble polymer with its precursor. The polymer/precursor composite is processed to obtain the structure having different morphological states by either choosing the reaction conditions to convert the unconverted different morphological states by either choosing the reaction conditions to convert the unconverted precursors such that the obtained polymer differs in it morphology/ properties from the first obtained polymer or by applying stress to the composite and then converting the still unreacted precursor or precursors in the composite such that different morphological states are obtained.

    摘要翻译: 公开了制备多相聚合物的方法,其中相具有相同的化学结构,但具有不同的形态和因此具有不同的性质。 这通过形成聚合物的前体的混合物来实现,至少一种前体的反应速率高于混合物中的其它前体或前体。 然后将具有最高反应速率的前体转化成聚合物和未聚合的前体的复合物。 该混合物也可以通过将可溶性聚合物与其前体混合而形成。 通过选择反应条件以转化未转化的前体使得所得聚合物的形态/性质不同,通过选择反应条件以转化未转化的不同形态状态,处理聚合物/前体复合物以获得具有不同形态的结构 从第一获得的聚合物或通过对复合材料施加应力,然后转化复合材料中的未反应的前体或前体,使得获得不同的形态。