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    Method of making M41S family molecular sieve
    123.
    发明授权
    Method of making M41S family molecular sieve 有权
    制作M41S系列分子筛的方法

    公开(公告)号：US09365430B2

    公开(公告)日：2016-06-14

    申请号：US12738050

    申请日：2008-07-30

    申请人： Wenyih Frank Lai ,  Robert Ellis Kay ,  Stephen John McCarthy

    发明人： Wenyih Frank Lai ,  Robert Ellis Kay ,  Stephen John McCarthy

    IPC分类号： C01B37/00 ,  C01B39/00 ,  B01J29/54 ,  C01B37/02 ,  B01J29/83 ,  B01J29/76 ,  C01B39/54 ,  B01J29/84 ,  B01J29/03 ,  B01J29/85 ,  B01J29/04 ,  C01B39/48 ,  B01J29/70 ,  B01J29/82 ,  C01B37/04 ,  C01B37/06 ,  C01B37/08

    CPC分类号： C01B37/02 ,  B01J29/0308 ,  B01J29/0333 ,  B01J29/041 ,  B01J29/044 ,  B01J29/70 ,  B01J29/76 ,  B01J29/82 ,  B01J29/83 ,  B01J29/84 ,  B01J29/85 ,  B01J2229/42 ,  C01B37/005 ,  C01B37/04 ,  C01B37/06 ,  C01B37/065 ,  C01B37/08 ,  C01B39/48 ,  C01B39/54

    摘要： This disclosure relates to a novel method of making and recovering M41S family molecular sieve materials using synthesis mixtures having high solids-content and without a purification step. The solids-content, for example, is in a range from about 20 wt. % to 50 wt. %. The method also includes the step of mixing at least a portion of the M41S made with another material to form a composition, wherein the amount of said material to be mixed with said M41S product is such that said composition having less than 10 wt. % free fluid. The material mixed with the M41S made includes metal oxides, metal nitrides, metal carbides and mixtures thereof, as well as absorptive material capable of absorbing mother liquor and selected from the group consisting of carbon silica, alumina, titania, zirconia and mixtures thereof. The amount of the wastewater generated by this novel method is reduced by at least 50% to as much as 100% as comparing with conventional method of making M41S materials. By reducing and/or eliminating at least a portion of the wastewater generated in the synthesis product, the new method reduces cost of making of M41S materials and provides a more environmentally-friendly synthesis product.

    摘要翻译： 本公开涉及使用具有高固体含量并且没有纯化步骤的合成混合物制备和回收M41S家族分子筛材料的新方法。 固体含量例如在约20wt。 ％至50重量％ ％。 该方法还包括将至少一部分与另一种材料制成的M41S混合以形成组合物的步骤，其中与所述M41S产品混合的所述材料的量使得所述组合物的含量小于10wt。 ％自由流体。 与M41S混合的材料包括金属氧化物，金属氮化物，金属碳化物及其混合物，以及能够吸收母液并且选自碳二氧化硅，氧化铝，二氧化钛，氧化锆及其混合物的吸收材料。 与传统的制备M41S材料的方法相比，这种新方法产生的废水量减少至少50％至多达100％。 通过减少和/或消除在合成产物中产生的至少一部分废水，新方法降低了M41S材料的制造成本并提供了更环保的合成产品。

    Process for aryl-aryl carbon to carbon bond formation by arylation of aryl halide or an aromatic compound
    130.
    发明申请
    Process for aryl-aryl carbon to carbon bond formation by arylation of aryl halide or an aromatic compound 审中-公开
    通过芳基卤化物或芳族化合物的芳基化形成芳基 - 芳基碳与碳键的方法

    公开(公告)号：US20050227863A1

    公开(公告)日：2005-10-13

    申请号：US10814860

    申请日：2004-03-31

    申请人： Vasant Choudhary ,  Rani Jha

    发明人： Vasant Choudhary ,  Rani Jha

    IPC分类号： B01J21/16 ,  B01J23/26 ,  B01J23/83 ,  B01J27/06 ,  B01J27/132 ,  B01J27/187 ,  B01J29/03 ,  B01J29/035 ,  B01J29/70 ,  B01J29/83 ,  B01J37/22 ,  B01J37/24 ,  C07C2/86

    CPC分类号： B01J37/24 ,  B01J21/16 ,  B01J23/26 ,  B01J23/83 ,  B01J27/132 ,  B01J29/0308 ,  B01J29/035 ,  B01J29/7007 ,  B01J29/83 ,  B01J37/22 ,  C07C2/861 ,  C07C2523/745 ,  Y02P20/588 ,  C07C15/16

    摘要： A solid catalyst, consisting of partially halogenated metal oxide or mixed metal oxide or zeolite or zeolite-like solid, represented by a general formula: X(a)/PbMOc(OH)d wherein, X is halogen element selected from F, Cl, Br and I; P is phosphorous element; M is at least one metallic element selected from alkaline earth metals, rare earth metals, group IIIa metals, non-noble transition metals, Sn, Sb, Bi, Si, thorium and uranium; O is oxygen; H is hydrogen; a is the concentration of halogen element X present in the catalyst in the range from 0.01 wt % to 50 wt %; b is the mole ratio of P to M in the range from zero to 1.0; c and d are the number of oxygen and OH groups, respectively, required to satisfy the valence requirement of the metallic and non-metallic elements (M and P); and the ratio of d to c in the range from zero to about 1.0, with or without any catalyst support, useful for the Friedel-Crafts reactions and also its method of preparation are disclosed.

    摘要翻译： 由以下通式表示的部分卤化金属氧化物或混合金属氧化物或沸石或类似沸石的固体组成的固体催化剂：<？in-line-formula description =“In-Line Formulas”end =“lead”？> α（in）-in-line-formula description =“In-line Formulas”end =“尾”→其中，X是选自F，Cl，Br和I的卤素元素; P是磷元素; M是选自碱土金属，稀土金属，IIIa族金属，非贵金属过渡金属，Sn，Sb，Bi，Si，钍和铀中的至少一种金属元素; O是氧; H是氢; a是催化剂中存在的卤素元素X的浓度在0.01重量％至50重量％的范围内; b是P与M的摩尔比在0至1.0的范围内; c和d分别是满足金属和非金属元素（M和P）的化合价要求所需的氧和OH基数; 并且公开了对于Friedel-Crafts反应可用的有或没有任何催化剂载体的d至c在0至约1.0的范围内的比率，以及其制备方法。