Methods of plugging wells
    72.
    发明授权
    Methods of plugging wells 失效
    堵井方法

    公开(公告)号:US06488089B1

    公开(公告)日:2002-12-03

    申请号:US09918997

    申请日:2001-07-31

    IPC分类号: E21B3300

    摘要: Methods of forming one or more plugs in a well bore are provided. The methods basically comprise the steps of dropping into the well bore a cementitious material which will delayedly react with water therein to form an impermeable solid and which has been formed into agglomerates of sufficient weight to sink through the water and other fluids and materials in the well bore. The agglomerates are dropped in a quantity sufficient to form a mass of the agglomerates in the well bore. Thereafter, the mass of agglomerates is allowed to react with the water in the well bore and set into an impermeable solid plug therein.

    摘要翻译: 提供了在井眼中形成一个或多个塞子的方法。 该方法基本上包括以下步骤:将井眼中的水与其延迟反应形成不渗透的固体,并且已经形成为足够重的聚集体以沉入井中的水和井中的其它流体和材料的水泥质材料 孔。 附聚物以足以在井眼中形成团块的量的量被滴下。 此后,允许附聚物的质量与井眼中的水反应并在其中设置为不渗透的固体塞子。

    Low sintering temperature cordierite batch and cordierite ceramic produced therefrom
    73.
    发明授权
    Low sintering temperature cordierite batch and cordierite ceramic produced therefrom 失效
    低烧结温度由其生产的堇青石和堇青石陶瓷

    公开(公告)号:US06391813B1

    公开(公告)日:2002-05-21

    申请号:US09473376

    申请日:1999-12-28

    申请人: Gregory A. Merkel

    发明人: Gregory A. Merkel

    IPC分类号: C04B35195

    摘要: The invention is directed at sintered ceramic articles exhibiting a primary crystalline phase of cordierite and an analytical oxide composition, in weight percent, of 44-53% SiO2, 30-38 Al2O3, 11-16% MgO and 0.05 to 10% of a metal oxide. The ceramic article exhibits a coefficient of thermal expansion in at least one direction no greater than about 15.0×10−7° C. over the temperature range of about 25° C. to about 800° C. The sum of the weight percentages of residual mullite, corundum, and spinel, as measured by X-ray diffractometry of the crushed and powdered body, is not greater than 15%. Furthermore, the invention discloses a method of producing the aforementioned ceramic body, comprising (a) selecting a raw material batch mixture for forming the cordierite ceramic body, comprising two or more compounds which serve as an alumina source, a silica source and a magnesia source, and at least one metal oxide source in an amount to result in the cordierite body comprising, on an analytical oxide basis, in weight percent, between about 0.05-10% of the metal oxide; (b) adding an organic binder system to the inorganic mixture and forming the mixture into a green body; (c) drying the green body and thereafter firing the green body at a time and at a temperature no greater than about 1300° C. to result in sintered ceramic body. Preferred metal oxide sources include the oxides or oxide-forming compounds of the metals selected from the group consisting of molybdenum, tungsten, bismuth, copper, yttrium, lanthanide metals and boron.

    摘要翻译: 本发明涉及显示堇青石的主结晶相和分析氧化物组合物的烧结陶瓷制品,其重量百分比为44-53%SiO 2,30-38 Al 2 O 3,11-16%MgO和0.05至10%的金属 氧化物。 在约25℃至约800℃的温度范围内,陶瓷制品在至少一个方向上显示不大于约15.0×10-7℃的热膨胀系数。残余莫来石的重量百分比之和 ,刚玉和尖晶石,通过粉碎和粉碎体的X射线衍射测量,不大于15%。 此外,本发明公开了一种制造上述陶瓷体的方法,包括(a)选择用于形成堇青石陶瓷体的原料分批混合物,其包含两种或更多种用作氧化铝源的化合物,二氧化硅源和氧化镁源 ,并且导致堇青石体的量的至少一种金属氧化物源以分析氧化物为基准,以重量百分比计包含约0.05-10%的金属氧化物;(b)将有机粘合剂体系加入到 无机混合物并将混合物形成生坯;(c)干燥生坯,然后在不大于约1300℃的温度下煅烧生坯以产生烧结陶瓷体。优选的金属氧化物源 包括选自钼,钨,铋,铜,钇,镧系元素金属和硼中的金属的氧化物或氧化物形成化合物。

    Method of forming and shaping plasticized mixtures and the green bodies made therefrom
    74.
    发明授权
    Method of forming and shaping plasticized mixtures and the green bodies made therefrom 失效
    塑化混合物和由其制成的生坯体的形成和成型方法

    公开(公告)号:US06372033B1

    公开(公告)日:2002-04-16

    申请号:US09503625

    申请日:2000-02-11

    IPC分类号: C08L8900

    摘要: Powder mixtures and a method of forming and shaping the mixtures. The method involves compounding the components of powder materials, binder, solvent for the binder, surfactant, and non-solvent with respect to at least the binder, the solvent, and the powder materials. The non-solvent is lower in viscosity than the binder combined with the solvent. The solvent is present in an amount that is less than the amount that would be present otherwise. The components are mixed and plasticized, and shaped to form a green body. The choice of components results in improved wet green strength in the green body. The method is especially useful for extrusion processing of aqueous binder systems such as water and cellulose ethers and hydrophobic non-solvents, to form structures such as honeycombs. In the body, the ratio, upon subsequent firing, of the isostatic strength to the A-axis strength is at least about 20% higher than in bodies made without the mixture composition of the invention. A honeycomb body having a ratio of the isostatic strength to the A-axis strength of at least about 0.33 upon firing.

    摘要翻译: 粉末混合物和形成和成型混合物的方法。 该方法包括将至少粘合剂,溶剂和粉末材料的粉末材料,粘合剂,粘合剂,表面活性剂和非溶剂的溶剂的组分混合。 非溶剂的粘度低于与溶剂结合的粘合剂。 溶剂的存在量小于否则会存在的量。 将组分混合并塑化,并成形以形成生坯。 组分的选择导致生坯中湿绿色强度的提高。 该方法特别适用于水性粘合剂体系如水和纤维素醚和疏水性非溶剂的挤出加工,以形成结构如蜂窝。 在身体中,随后的烧制中的等静压强度与A轴强度的比例比不用本发明的混合物组合物制造的体积高至少约20%。 具有等离子强度与A轴强度的比例在焙烧时为至少约0.33的蜂窝体。

    High strength/high surface area alumina ceramics
    75.
    发明授权
    High strength/high surface area alumina ceramics 失效
    高强度/高表面积氧化铝陶瓷

    公开(公告)号:US06365259B1

    公开(公告)日:2002-04-02

    申请号:US09467741

    申请日:1999-12-20

    IPC分类号: B32B312

    摘要: Ceramic honeycombs incorporating cell walls of a sintered alumina material providing controlled pore size distribution in combination with high BET surface area and flexural (MOR) strength are formed by the extrusion, drying and firing of plasticized alumina powder batches containing major proportions of anhydrous, high-surface-area gamma alumina powders dispersed with selected acids; low combined drying and firing shrinkages provide strong, crack-free bodies of high surface area and strength.

    摘要翻译: 通过挤出,干燥和焙烧含有主要比例的无水高岭石的增塑的氧化铝粉末组合物,形成了结合高BET值表面积和弯曲(MOR)强度而提供受控孔径分布的烧结氧化铝材料的细胞壁的陶瓷蜂窝体, 用选择的酸分散的表面积γ氧化铝粉末; 低组合干燥和烧结收缩提供强大的,无裂纹的高表面积和强度的物体。

    Fabrication of ultra low thermal expansion cordierite structures
    77.
    发明申请
    Fabrication of ultra low thermal expansion cordierite structures 审中-公开
    超低热膨胀堇青石结构的制造

    公开(公告)号:US20020010073A1

    公开(公告)日:2002-01-24

    申请号:US09872414

    申请日:2001-05-31

    IPC分类号: C04B035/195 C04B033/32

    摘要: Disclosed is sintered ceramic article that exhibits a primary crystalline phase of cordierite and analytical oxide composition, in weight percent, of 49-53% SiO2, 33-38% Al2O3, 12-16% MgO and exhibits a coefficient of thermal expansion no greater than about 4.0null10null7/null C. over the temperature range of about 25null C. to about 800null C. and a transverse-I ratio of not less than about 0.92. Also disclosed is a method for producing a sintered cordierite ceramic article involving preparing a plasticizable raw material, comprising a magnesium source, a SiO2-forming source and an additional component of either: (a) a clay-free, Al2O3-forming source having a surface area of greater than about 5 m2/g; or, (b) a clay and Al2O3-forming source combination wherein the clay comprises no greater than about 30%, by weight, of the total inorganic mixture, and the Al2O3-forming source exhibits a surface area of greater than about 40 m2/g. The mixture is formed into a green body substrate of the desired configuration and subsequently dried and fired for a time and at temperature sufficient to form a structure having the aforementioned CTE and I-ratio properties.

    摘要翻译: 公开了烧结陶瓷制品,其显示堇青石的主结晶相和分析氧化物组合物,其重量百分比为49-53%SiO 2,33-38%Al 2 O 3,12-16%MgO,并且显示出不大于 在约25℃至约800℃的温度范围内为约4.0×10 -7 /℃,横I比不小于约0.92。 还公开了一种生产堇青石烧结体烧结体的方法,其包括制备可塑性原料,包括镁源,形成SiO 2的源和另外的组分:(a)不含粘土的Al 2 O 3形成源,其具有 表面积大于约5m2 / g; 或(b)粘土和Al 2 O 3形成源组合,其中粘土占总无机混合物的不大于约30重量%,并且Al 2 O 3形成源的表面积大于约40m 2 / G。 将混合物形成为所需构型的生坯基材,随后干燥并焙烧一段时间并在足以形成具有上述CTE和I比率性质的结构的温度下进行烧制。

    Method of forming and shaping plasticized mixtures
    80.
    发明授权
    Method of forming and shaping plasticized mixtures 失效
    塑化混合物的形成和成型方法

    公开(公告)号:US6080345A

    公开(公告)日:2000-06-27

    申请号:US116144

    申请日:1998-07-15

    摘要: Powder mixtures and a method of forming and shaping the mixtures. The method involves compounding the components of powder materials, binder, solvent for the binder, surfactant, and non-solvent with respect to at least the binder, the solvent, and the powder materials. The non-solvent is lower in viscosity than the binder combined with the solvent. The solvent is present in an amount that is less than the amount that would be present otherwise. The components are mixed and plasticized, and shaped to form a green body. The choice of components results in improved wet green strength in the green body. The method is especially useful for extrusion processing of aqueous binder systems such as water and cellulose ethers and hydrophobic non-solvents, to form structures such as honeycombs. In the body, the ratio, upon subsequent firing, of the isostatic strength to the A-axis strength is at least about 20% higher than in bodies made without the mixture composition of the invention. A honeycomb body having a ratio of the isostatic strength to the A-axis strength of at least about 0.33 upon firing.

    摘要翻译: 粉末混合物和形成和成型混合物的方法。 该方法包括将至少粘合剂,溶剂和粉末材料的粉末材料,粘合剂,粘合剂,表面活性剂和非溶剂的溶剂的组分混合。 非溶剂的粘度低于与溶剂结合的粘合剂。 溶剂的存在量小于否则会存在的量。 将组分混合并塑化,并成形以形成生坯。 组分的选择导致生坯中湿绿色强度的提高。 该方法特别适用于水性粘合剂体系如水和纤维素醚和疏水性非溶剂的挤出加工,以形成结构如蜂窝。 在身体中,随后的烧制中的等静压强度与A轴强度的比例比不用本发明的混合物组合物制造的体积高至少约20%。 具有等离子强度与A轴强度的比例在焙烧时为至少约0.33的蜂窝体。